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Resourceful Utilization of Ironmaking Waste: Synthesis of Ti5Si3 Alloy from Titanium-Bearing Blast Furnace Slag

ISIJ International 2025年第3期65卷 460-469页

作者： Pang, Zhongya Chen, Shun Jiang, Zhenqiang Han, Chenyang Yu, Xing Zheng, Kai Chen, Chaoyi Li, Guangshi Xu, Qian Zou, Xingli Lu, Xionggang State Key Laboratory of Advanced Special Steel Shanghai Key Laboratory of Advanced Ferrometallurgy School of Materials Science and Engineering Shanghai University 99 Shangda Road BaoShan District Shanghai200444 China School of Materials and Energy Engineering Guizhou Key Laboratory for Preparation of Light Metal Materials Guizhou Institute of Technology Doctor Road Dangwu Town GUI ‘an New District Guiyang550025 China School of Materials and Metallurgy Guizhou University 2708 South Section of Huaxi Avenue Guiyang550025 China

Titanium-bearing blast furnace slag (TBFS), a byproduct of ironmaking processes, has long been discarded as waste, resulting in the squandering of valuable resources such as titanium. The recovery and effective utilization of TBFS hold immense significance and importance. This study reports a direct electrolysis method for synthesizing Ti5Si3 alloy from a TBFS/SiO2 mixture in molten CaCl2 at 950°C. A comprehensive investigation was conducted into the phase and morphological evolution during the electrolysis process, along with an analysis of the migration behavior of impurities such as Ca and Al present in TBFS. The synthesized Ti5Si3 alloy powder was systematically characterized and analyzed using scanning electron microscopy, transmission electron microscopy, and other techniques. The results reveal that the electrolysis process encompasses electrochemical deoxidation, in-situ alloying, and self-purification. Furthermore, this study achieved further purification of the Ti5Si3 alloy through vacuum laser rapid melting, effectively volatilizing and removing the residual impurity elements, resulting in an increase in the purity of Ti5Si3 alloy from 96.8% to 98.6%. The resultant Ti5Si3 alloy exhibits excellent corrosion resistance in phosphate buffer solution. In summary, this work provides a crucial technical paradigm and scientific theoretical foundation for the resourceful and value-added utilization of ironmaking solid waste, specifically TBFS. © 2025 The Iron and Steel Institute of Japan.

关键词： Slags

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Proposal and Validation of Vector Hysteresis Operator Based on Microscopic Magnetization Mechanism 11th

Proposal and Validation of Vector Hysteresis Operator Based ...

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11th Frontier Academic Forum of Electrical engineering, FAFEE 2024

作者： Ma, Guang He, Chengxu Cheng, Ling Lu, Mengxue Duan, Nana State Key Laboratory of Advanced Power Transmission Technology Beijing102209 China School of Electrical Engineering Xi’an Jiaotong University Xi’an710049 China

ISBN: (纸本)9789819788118

In this paper, a new vector hysteresis operator is proposed based on the microscopic magnetization mechanism of magnetic materials. Firstly, the magnetization mechanism of magnetic materials is analyzed, and an ideal self-consistent crystal model is proposed. Then the vector hysteresis operator is proposed based on the principle of energy minimum stability, considering the magnetocrystalline anisotropy energy and magnetostatic energy of cubic crystal materials. Finally, the validity of vector hysteresis operator is verified by the comparison of the experimental and simulation results of the silicon steel samples under the alternating current magnetic field. The proposed new vector hysteresis operator is helpful to improve the accurate simulation of magnetic properties of magnetic materials, which is of great significance in engineering applications. © Beijing Paike Culture Commu. Co., Ltd. 2025.

关键词： Silicon steel

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Structure deformation of Ni-Fe-Se enables efficient oxygen evolution via RE atoms doping

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Rare Metals 2025年第1期44卷 336-348页

作者： Hong-Rui Zhao Cheng-Zong Yuan Cong-Hui Li Wen-Kai Zhao Fu-Ling Wu Lei Xin Hong Yin Shu-Feng Ye Xiao-Meng Zhang Yun-Fa Chen Jiangxi Province Research Institute of Rare Earths Ganjiang Innovation AcademyChinese Academy of SciencesGanzhou341119China School of Rare Earths University of Science and Technology of ChinaHefei230026China Key Laboratory of Hunan Province for Advanced Carbon-Based Functional Materials School of Chemistry and Chemical EngineeringHunan Institute of Science and TechnologyYueyang414006China State Key Laboratory of Multiphase Complex Systems Institute of Process EngineeringChinese Academy of SciencesBeijing100190China

The development of cost-effective and highly stable electrocatalysts for oxygen evolution reactions holds paramount importance in practical hydrogen ***,we present a novel self-supported electrode comprising Ce-doped Ni-Fe-Se nanosheets grown on carbon cloth(Ni-Fe-Ce-Se/CC).This electrode was synthesized through a selenylation process,utilizing Ni-Fe-Ce-layered double hydroxide/carbon cloth(Ni-Fe-Ce LDH/CC)as the ***,Ni-Fe-Ce-Se/CC electrode demonstrates remarkable performance,requiring a low overpotential of 300 mV to attain a current density of 100 mA·cm^(-2)under harsh alkaline ***,the electrode exhibits exceptional stability during continuous operation for 100 *** into the underlying mechanisms was gained through a combination of experimental results and density functional theory *** findings reveal that Ce doping induces crystal structure deformation in Ni-Fe-Se and enhances electron enrichment around Ni *** structural modification optimizes the adsorption energy of oxygen-based intermediates on the Ni-Fe-Se *** work offers a valuable strategy for regulating the electron transfer and adsorption capabilities of transition metal selenide electrocatalysts through RE atoms doping,opening new avenues for enhanced electrocatalytic performance.

关键词： Ce doping Structure deformation Ni-Fe-Se Electron transfer Oxygen evolution

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Proposal and Validation of the Vector Hysteresis Model Considering the Effect of Pressure 11th

Proposal and Validation of the Vector Hysteresis Model Consi...

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11th Frontier Academic Forum of Electrical engineering, FAFEE 2024

ISBN: (纸本)9789819788118

Magnetic materials will be affected by non-magnetic factors such as temperature, pressure and stress in actual working conditions, which will change the magnetic properties of magnetic materials, thus affecting the simulation results. A vector hysteresis model considering the effect of pressure is proposed in this paper. Firstly, based on the magnetization mechanism of ferromagnetic materials, a vector hysteresis operator is proposed, an energy calculation formula considering magnetostatic energy and anisotropic energy is proposed, and an octagonal star rule is proposed to determine the current magnetization state of ferromagnetic materials. Then the proposed model is modified considering the influence of pressure, and the different distribution functions under different pressures are proposed. Finally, the validity of the model is verified by comparing the experimental results with the simulation results. © Beijing Paike Culture Commu. Co., Ltd. 2025.

关键词： Distribution function Pressure effect Vector hysteresis model

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Effects of nuclear deformation and surface polarization on proton-emission half-lives

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Chinese Physics C 2025年第4期49卷 186-198页

作者： Hanlin Wang Zhen Wang Dong Bai Dongdong Ni Zhongzhou Ren School of Physics Science and Engineering Tongji UniversityShanghai 200092China College of Mechanics and Engineering Science Hohai UniversityNanjing 211100China Institute of Science and Technology for Deep Space Exploration Suzhou CampusNanjing UniversitySuzhou 215163China State Key Laboratory of Lunar and Planetary Sciences Macao University of Science and TechnologyMacao 999078China Key Laboratory of Advanced Micro-Structure Materials Ministry of EducationShanghai 200092China

Proton radioactivity is used to investigate the characteristics of unstable neutron-deficient nuclei beyond the proton *** on the tunneling of one proton through the potential barrier formed by Woods-Saxon plus expanded Coulomb potentials,the half-lives of various proton emitters are calculated using distorted wave Born *** particular,deformation and nuclear surface polarization are considered in our calculation,and their effects on proton-emission half-lives are *** analytic formula expressing the relationship between spectroscopic factors and deformation and polarization,which significantly reduces the deviations of calculated half-lives from experimental data,is proposed as ***,inspired by the new experimental results for the first proton emitter ever discovered,^(53)Co^(m)[*** et al.,***.14,5961(2023)],we calculate its two proton-emission branches and interpret the partial *** is noteworthy that this high-spin isomer has some particular characteristics,including diminutive spectroscopic factors and stronger daughter-proton interactions,that considerably enhance the effects of deformation and polarization.

关键词： proton emission proton dripline Gamow model

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Crystallographic micro-mechanism of faceted crack initiation in near-αtitanium alloy Ti6321 under room-temperature fatigue and dwell fatigue loadings

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材料科学技术（英文版） 2025年第2期205卷 109-126页

作者： Wenyuan Zhang Qiaonan Shu Jiangkun Fan Panpan Fan Xiangyi Xue Peng Jiang Minjie Lai Bing Tang Zhiqian Liao Hongchao Kou Jinshan Li State Key Laboratory of Solidification Processing Northwestern Polytechnical UniversityXi'an 710072China State Key Laboratory of Solidification Processing Northwestern Polytechnical UniversityXi'an 710072China National & Local Joint Engineering Research Center for Precision Thermoforming Technology of Advanced Metal Materials Xi'an 710072China Chongqing Innovation Center Northwestern Polytechnical UniversityChongqing 401135China Luoyang Ship Material Research Institute Luoyang 471000China

Crack initiation mechanism of dwell fatigue has always been a key problem in rationalizing the dwell effect,and it is not completely understood *** study conducted stress-controlled low-cycle fatigue and dwell fatigue tests on Ti-6Al-3Nb-2Zr-1Mo alloy with bimodal microstructure to reveal its microstruc-tural characteristics and crack initiation *** study demonstrated that the faceted primaryα nodules located near the specimen surface acted as crack initiation sites during both fatigue and dwell fatigue *** trace analysis revealed that faceted cracking occurred at(0001)basal plane with the maximum Schmid factor value through a special cracking mode referred to as(0001)twist boundary *** criteria of parameters C1 and C2 were proposed based on experimental observation and molecular dynamics simulations,which well identify candidates for(0001)twist boundary crack *** demonstrated that grain pairs combining a moderately high Schmid factor for basal slip and a well-orientated Burgers vector in the out-of-surface plane was the preferable location for surface(0001)twist-boundary crack initiation,and grain pairs combining a high Schmid factor for basal slip and a high normal stress on basal plane are perfect candidates for subsurface *** on this,phenomeno-logical models are proposed to explain the surface(0001)twist-boundary cracking mechanism from the perspective of surface extrusion-intrusion-induced micro-notches.

关键词： Titanium alloy Dwell fatigue Facet Fatigue crack initiation Crystallographic orientation

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Study on the Characteristics and Mechanism of Discharge Degradation Products of Epoxy Resin Matrix in Composite Insulators Under Humid Air Environment 19th

Study on the Characteristics and Mechanism of Discharge Degr...

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19th Annual Conference of China Electrotechnical Society, ACCES 2024

作者： Zhiyu, Wan Dandan, Zhang Chao, Gao Ming, Lu Hui, Li Zhenbiao, Li Kexin, Shi School of Electrical and Electronic Engineering Huazhong University of Science and Technology Wuhan430074 China Ministry of Education Wuhan430074 China State Key Laboratory of Advanced Electromagnetic Engineering and Technology Huazhong University of Science and Technology Wuhan430074 China Henan Key Laboratory of Power Transmission Line Galloping Prevention and Control Technology State Grid Henan Electric Power Research Institute Zhengzhou450052 China Henan Jiuyu EPRI Electric Power Technology Co. Ltd. Zhengzhou450052 China

ISBN: (纸本)9789819613823

The degradation of the epoxy resin matrix in the core rods of composite insulators is the primary factor leading to decay-like deterioration and fracture accidents. Partial discharge in a humid environment is a critical trigger for this phenomenon. As an organic polymer, epoxy resin is prone to degradation under discharge, producing complex degradation products that can have secondary effects on surrounding materials, further accelerating the decay-like deterioration process. To optimize the formulation and manufacturing process of composite insulator materials and mitigate or even prevent decay-like fractures, it is crucial to study the discharge degradation products and mechanisms of the epoxy resin matrix. In this study, discharge experiments were conducted on anhydride-cured bisphenol A epoxy resin used in composite insulators within a closed humid environment. Changes in chemical functional groups of solid samples before and after discharge were analyzed from the high-frequency region to the fingerprint region. The main components and relative yields of liquid and gaseous discharge products were detected, and the primary reaction mechanisms during the discharge degradation process were thoroughly investigated. Results indicate that partial discharge in humid air induces instantaneous temperature rise and radical action, leading to epoxy resin degradation, generating alcohols and hydroxyl groups, which may increase the material’s hydration capacity and surface conductivity, thereby reducing electric field uniformity. Gaseous products such as methane, acetone, ethylene, and ethyl acetate produced by discharge pyrolysis may exacerbate stress at the core rod and sheath interface, increasing the risk of interfacial damage. Liquid products like nitric acid, carboxylic acids, and acetone may accelerate glass fiber fracture and sheath swelling. © Beijing Paike Culture Commu. Co., Ltd. 2025.

关键词： Partial discharges

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electromagnetic Functions Modulation of Recycled By-Products by Heterodimensional Structure

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Nano-Micro Letters 2025年第6期17卷 264-278页

作者： Ze Nan Wei Wei Zhenhua Lin Ruimei Yuan Miao Zhang Jincheng Zhang Jianyong Ouyang Jingjing Chang Hejun Li Yue Hao State Key Laboratory of Wide-Bandgap Semiconductor Devices and Integrated Technology School of MicroelectronicsXidian UniversityXi’an 710071People’s Republic of China State Key Laboratory of Solidification Processing Shaanxi Province Key Laboratory of Fiber Reinforced Light Composite MaterialsCarbon/Carbon Composites Research CenterNorthwestern Polytechnical UniversityXi’an 710072People’s Republic of China Advanced Interdisciplinary Research Center for Flexible Electronics Xidian UniversityXi’an 710071People’s Republic of China Department of Materials Science and Engineering National University of Singapore7 Engineering Drive 1Singapore 117574Singapore

One of the significant technological challenges in safeguarding electronic devices pertains to the modulation of electromagnetic(EM)wave jamming and the recycling of defensive *** synergistic effect of heterodimensional materials can effectively enable the manipulation of EM waves by altering the *** we propose a novel approach for upcycling by-products of silver nanowires that can fabricate shape-tunable aerogels which enable the modulation of its interaction with microwaves by heterodimensional structure of ***-product heterodimensionality was used to design EM-wave-jamming-dissipation structures and therefore two typical tunable aerogel forms were *** first tunable form was aerogel film,which shielded EM interference(EMI shielding effectiveness(EMI SE)>89 dB)and the second tunable form was foam,which performed dual EM functions(SE>30 dB&reflective loss(RL)<-35 dB,effective absorption bandwidth(EAB)>6.7 GHz).We show that secondary recycled aerogels retain nearly all of their EM protection properties,making this type of closed-loop cycle an appealing *** findings pave the way for the development of adaptive EM functions with nanoscale regulation in a green and closed-loop cycle,and they shed light on the fundamental understanding of microwave interactions with heterodimensional structures.

关键词： Silver nanowires electromagnetic shielding Microwave absorption Recycled aerogels

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Self-powered Smart Water Meter for Pipeline Flow Monitoring 5th

Self-powered Smart Water Meter for Pipeline Flow Monitoring

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5th International Conference on Vibration and Energy Harvesting Applications, VEH 2024

作者： Mei, Mingqi Wang, Zizhao Li, Yunfei Tang, Tianyi Liu, Huicong School of Mechanical and Electric Engineering Jiangsu Provincial Key Laboratory of Advanced Robotics Soochow University Suzhou215123 China State Key Laboratory of Robotics and System Harbin Institute of Technology Harbin150001 China

ISBN: (纸本)9789819611904

This paper presents the development of a water flow energy harvester (WFEH) designed to power smart water meters within residential piping systems. Utilizing the kinetic energy of flowing water, the device harnesses this energy and converts it into electricity via electromagnetic principles. The impeller's shape, quantity, and guide vane height at the inlet were simulated using computational fluid dynamics (CFD) software, comparing impeller rotational speeds under various simulation parameters to select the appropriate impeller configuration. Experimental data indicate that with an inlet water pressure of 0.12 MPa and an outlet pressure of 0.06 MPa, a single coil in the device generates a peak voltage of 3.6 V, with a peak power of 54.2 mW and a head loss of 6 m. The maximum head loss permitted in residential water pipes is 10 m. The energy generation module of the WFEH has been designed with a six-coil array, significantly enhancing its performance output. Theoretically, the output power of the WFEH is sufficient to meet the energy needs of smart water meters. Therefore, the WFEH holds potential for integration into urban water management systems, providing a stable energy supply for data collection and transmission, and contributing to the development of self-powered smart meters. © The Author(s), under exclusive license to Springer Nature Singapore Pte Ltd. 2025.

关键词： Water meters

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Regulating crystallization and retarding oxidation in Sn-Pb perovskite via 1D cation engineering for high performance all-perovskite tandem solar cells

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Journal of Energy Chemistry 2025年第1期100卷 646-652页

作者： Ranran Liu Xin Zheng Zaiwei Wang Miaomiao Zeng Chunxiang Lan Shaomin Yang Shangzhi Li Awen Wang Min Li Jing Guo Xuefei Weng Yaoguang Rong Xiong Li Michael Grätzel Center for Mesoscopic Solar Cells Wuhan National Laboratory for OptoelectronicsHuazhong University of Science and TechnologyWuhan 430074HubeiChina Institute of Technology for Carbon Neutrality Shenzhen Institute of Advanced TechnologyChinese Academy of SciencesShenzhen 518055GuangdongChina School of Chemistry Chemical Engineering and Life SciencesState Key Laboratory of Advanced Technology for Materials Synthesis and ProcessingWuhan University of Technology430070HubeiChina Suzhou Institute of Nano-Tech and Nano-Bionics(SINANO) Chinese Academy of SciencesSuzhou 215123JiangsuChina School of Physics and Optoelectronic Engineering Hainan UniversityHaikou 570228HainanChina

All-perovskite tandem solar cells have the potential to surpass the theoretical efficiency limit of single junction solar cells by reducing thermalization ***,the challenges encompass the oxidation of Sn^(2+)to Sn^(4+)and uncontrolled crystallization kinetics in Sn-Pb perovskites,leading to nonradiative recombination and compositional heterogeneity to decrease photovoltaic efficiency and operational ***,we introduced an ionic liquid additive,1-ethyl-3-methylimidazolium iodide (EMIMI) into Sn-Pb perovskite precursor to form low-dimensional Sn-rich/pure-Sn perovskites at grain boundaries,which mitigates oxidation of Sn^(2+)to Sn^(4+)and regulates the film-forming dynamics of Sn/Pb-based perovskite *** optimized single-junction Sn-Pb perovskite devices incorporating EMIMI achieved a high efficiency of 22.87%.Furthermore,combined with wide-bandgap perovskite sub-cells in tandem device,we demonstrate 2-terminal all-perovskite tandem solar cells with a power conversion efficiency of 28.34%,achieving improved operational stability.

关键词： All-perovskite tandem solar cells Sn-Pb perovskite 1D Regulated crystallization Antioxidation

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