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Charge regulation by ferromagnetic metal/LiF spin-polarized interface for high-performance Li metal anodes

Rare Metals 2024年第3期43卷 995-1005页

作者： Ming-Yang Feng Shuang Zhou Yi-Fang Zhang Ya-Ping Wang Chun-Yan Fu Jian-Wen Li Yuan-Lang Wan Zhi-Jia Zhang Yong Jiang An-Qiang Pan State Key Laboratory of Powder Metallurgy School of Materials Science and EngineeringCentral South UniversityChangsha410083China State Key Laboratory of Separation Membranes and Membrane Processes Tianjin Key Laboratory of Advanced Fibers and Energy StorageSchool of Material Science and EngineeringTiangong UniversityTianjin300387China School of Materials Science and Engineering Hebei University of TechnologyTianjin300130China

The interfacial characteristics of the Li metal anode(LMA)play a crucial role in its overall *** various materials being applied to modify the interface,a comprehensive understanding of their specific mechanisms remains to be ***,we have prepared carbon cloth(CC)frameworks with their surfaces modified using ferromagnetic metal/LiF heterogeneous films(T^(M)-LiF-CC)as the substrate for LMA,which exhibit superior electrochemical *** ferromagnetic Co as a representative example,our study demonstrates that the enhanced performance of Co-LiF-CC,compared to bare CC,is attributed to the spinpolarized interface contributed by the Co/LiF *** and LiF play individual roles in redistributing electrons and Li^(+)to promote homogeneous Li *** nanoparticles play a crucial role in generating strong surface capacitance by storing electrons in spin-split bands,while LiF,with low surface diffusion barriers,ensures fast transportation of Li^(+).The Co-LiF-CC@Li electrodes deliver long lives of 7400 and 3600 h at 1 and 2 mA·cm^(-2)in symmetric cells,respectively;moreover,they enable full batteries with high and durable capacities,particularly when the N/P ratios are low(3.3 or even 1.7).

关键词： Lithium metal anode Interfacial charge Ferromagnetic metal Lithium fluoride Spin polarization

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In situ observation of the electrochemical behavior of Li–CO_(2)/O_(2)batteries in an environmental transmission electron microscope

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Carbon Energy 2024年第4期6卷 244-255页

作者： Peng Jia Yunna Guo Dongliang Chen Jingming Yao Xuedong Zhang Jianguo Lu Yuqing Qiao Liqiang Zhang Hebei Key Laboratory of Applied Chemistry College of Environmental and Chemical EngineeringYanshan UniversityQinhuangdaoChina State Key Laboratory of Metastable Materials Science and Technology Clean Nano Energy CenterYanshan UniversityQinhuangdaoChina State Key Laboratory of Silicon and Advanced Semiconductor Materials School of Materials Science and EngineeringZhejiang UniversityHangzhouChina Key Laboratory of Low Dimensional Materials and Application Technology of Ministry of Education School of Materials Science and EngineeringXiangtan UniversityXiangtanChina

Li–CO_(2)/O_(2)batteries,a promising energy storage technology,not only provide ultrahigh discharge capacity but also capture CO_(2)and turn it into renewable *** electrochemical reaction pathways'ambiguity,however,creates a hurdle for their practical *** study used copper selenide(CuSe)nanosheets as the air cathode medium in an environmental transmission electron microscope to in situ study Li–CO_(2)/O_(2)(mix CO_(2)as well as O_(2)at a volume ratio of 1:1)and Li–O_(2)batteries as well as Li–CO_(2)*** discharge reactions take place successively in the Li–CO_(2)/O_(2)–CuSe nanobattery:(I)4Li^(+)+O_(2)+4e^(−)→2Li_(2)O;(II)Li_(2)O+CO_(2)→Li_(2)CO_(3).The charge reaction proceeded via(III)2Li_(2)CO_(3)→4Li^(+)+2CO_(2)+O_(2)+4e^(−).However,Li–O_(2)and Li–CO_(2)nanobatteries showed poor cycling stability,suggesting the difficulty in the direct decomposition of the discharge *** fluctuations of the Li–CO_(2)/O_(2)battery's electrochemistry were also shown to depend heavily on O_(2).The CuSe‐based Li–CO_(2)/O_(2)battery showed exceptional electrochemical *** Li^–CO_(2)/O_(2)battery offered a discharge capacity apex of 15,492 mAh g^(−1) and stable cycling 60 times at 100 mA g^(−1).Our research offers crucial insight into the electrochemical behavior of Li–CO_(2)/O_(2),Li–O_(2),and Li–CO_(2)nanobatteries,which may help the creation of high‐performance Li–CO_(2)/O_(2)batteries for energy storage applications.

关键词： CuSe nanosheets electrochemical reaction in situ environmental transmission electron microscopy Li-CO_(2)battery Li-CO_(2)/O_(2)battery Li-O_(2)battery

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Effect of Ni interlayer on microstructures and mechanical properties of 2205 duplex stainless steel joint by laser oscillating welding

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Journal of Iron and Steel Research International 2024年第10期31卷 2463-2474页

作者： Jing-wei Yang Xu-yang Liu Tao Li Lai-cai Chen Kai Yang Zong-ye Ding Jie Zhang Jian Qiao School of Mechatronic Engineering and Automation Foshan UniversityFoshan528000GuangdongChina Key Laboratory of Advanced Manufacturing Technology of the Ministry of Education Guizhou UniversityGuiyang550025GuizhouChina State Key Laboratory of Advanced Brazing Filler Metals&Technology Zhengzhou Research Institute of Mechanical Engineering Co.Ltd.Zhengzhou450001HenanChina China National United Engineering Laboratory for Advanced Bearing Tribology Henan University of Science and TechnologyLuoyang471023HenanChina School of Mechanical Engineering University of Science and Technology BeijingBeijing100083China

Laser oscillating welding of 2205 duplex stainless steel was performed using Ni interlayer as filler *** influence of stirring effect caused by laser oscillating and Ni addition in the behavior of molten pool and the microstructure evolution was *** results shows that Ni addition decreased the ratio of chromium equivalent and nickel equivalent in the molten pool and accelerated the austenitic *** austenite/ferrite ratio was regulated,and the precipitation of nitrides was suppressed in the weld *** stirring effect caused by the oscillating beam facilitated the uniform distribution of Ni elements within the molten pool,promoting the formation of the homogeneous microstructures in the weld *** increasing the thickness of Ni interlayer,both the dimension and the peak temperature of molten pool decrease,further increasing the cooling rate and refining the grain *** the thickness of Ni interlayer was 50μm,the austenite/ferrite ratio in the weld seam was close to 1:1,and the grain size reached the minimum *** tensile strength and ductility of the welded joint using Ni interlayer with thickness were 774 MPa and 25%,respectively,significantly improving the mechanical properties of 2205 duplex stainless steel joint welded without Ni addition.

关键词： 2205 duplex stainless steel Ni interlayer Laser welding Microstructure Mechanical property

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Characterization and degradation of β-Sn particles in thermal aged Pb-rich solder joint for low-temperature co-fired ceramic(LTCC)applications

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Rare Metals 2024年第10期43卷 5346-5361页

作者： Jin-Hong Liu Zhe Zhu Qiang-Qiang Nie Jun-Fu Liu Peng He Shu-Ye Zhang State Key Laboratory of Advanced Welding and Joining Harbin Institute of TechnologyHarbin 150001China Anhui Key Laboratory of Microsystem East China Research Institute of MicroelectronicsHefei 230088China School of Materials Science and Engineering Hefei University of TechnologyHefei 230009China

High-lead solder joints are still playing an indispensable role in military and space ***,in-depth characterization of high-lead solder joints and the underlying degradation mechanisms remain *** research first performed aging tests on Sn10Pb90 solder joints,the shear strength at room and elevated temperatures gradually reduced,and the resistance ***,a two-layered Ni-Sn intermetallic compound(IMC)structure was identified using transmission electron microscopy(TEM),which could be attributed to the change of Sn content in the ***,the internal annealing twin of a Sn particle was discovered,which could be attributed to creeping induced by thermal expansion coefficient(CTE)difference between Sn and *** analysis of partial and whole annealing twins was conducted through high-resolution TEM(HRTEM).Finally,four degradation mechanisms were *** of the IMC layer would result in increased brittleness and *** particle coarsening,apart from diminishing the ductility and toughness of the solder joint,it would also accelerate the creeping rate by weakening the phase boundary *** voids and cracks induced by phase boundary sliding,wedgeshaped cracking and pore-shaped cracking were discovered and their formation was *** importantly,the consumption of Sn resulted in a depletion of wettable layer,leading to the formation of Pb streams and isolated IMC islands,also known as the spalling and delamination of *** diffusion followed a spiral path,which was mutually influenced by orientation misfit and concentration gradient.A technique to prevent cracking was *** research is expected to provide significant technical references for high-lead solder joints.

关键词： High-lead solder joints Aging TEM characterization Degradation mechanisms Properties

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Optimal Voyage Scheduling of Battery-Swapping Based Inland All-Electric Ship Fleet Considering Environmental Factors and Time-of-Use Electricity Price 9

Optimal Voyage Scheduling of Battery-Swapping Based Inland A...

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9th Asia Conference on Power and Electrical engineering, ACPEE 2024

作者： Yang, Shenglong Ma, Fan Sun, Haishun Sun, Lin State Key Laboratory of Advanced Electromagnetic Engineering and Technology Wuhan China Huazhong University of Science and Technology State Key Laboratory of Advanced Electromagnetic Engineering and Technology Wuhan China Naval University of Engineering National Key Laboratory of Electromagnetic Energy Wuhan China

ISBN: (纸本)9798350309638

Inland all-electric ship is receiving more and more attention due to its advantages in terms of low carbon, energy conservation, and flexibility in operation mode. However, its extensive promotion and application are held back by various problems such as long charging time, high cost of energy supplement, environmental factors, etc. In addition, the complexity of the electric ship fleet also poses a challenge to its optimal operation. Hence, an optimal voyage scheduling model of the inland all-electric ship fleet, with departure time and speed of each ship as the decision variables, is firstly established to minimize the total battery-swapping cost and the total waiting time in this paper. Based on the battery-swapping mode, the model takes environmental factors and time-of-use electricity prices into account. Second, adaptive particle swarm optimization is used to solve the proposed model, and the comparative analysis is made. Finally, an all-electric ship fleet operating in the Yangtze River is selected as a study case, and the simulation results show that the proposed model can effectively reduce the total battery-swapping cost and the total waiting time. © 2024 IEEE.

关键词： Ships

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Self-Powered Piezo-Supercapacitors Based on ZnO@Mo-Fe-MnO_(2)Nanoarrays

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Energy & Environmental Materials 2024年第4期7卷 304-314页

作者： Luo Sun Zhiguo Ye Xinyuan Peng Shaojie Zhuang Duosheng Li Zhong Jin School of Materials Science and Engineering Nanchang Hangkong University696#FengHeNan RoadNanchang 330063China State Key Laboratory of Coordination Chemistry MOE Key Laboratory of Mesoscopic ChemistryMOE Key Laboratory of High Performance Polymer Materials and TechnologyJiangsu Key Laboratory of Advanced Organic MaterialsSchool of Chemistry and Chemical EngineeringNanjing UniversityNanjing 210023China

The development of self-charging supercapacitor power cells(SCSPCs)has profound implications for smart electronic devices used in different ***,we epitaxially electrodeposited Mo-and Fe-codoped MnO_(2)films on piezoelectric ZnO nanoarrays(NAs)grown on the flexible carbon cloth(denoted ZnO@Mo-Fe-MnO_(2)NAs).A self-charging supercapacitor power cell device was assembled with the Mo-and Fe-codoped MnO_(2)nanoarray electrode and poly(vinylidenefluoride-co-trifluoroethylene)(PVDF-Trfe)piezoelectric film doped with BaTiO_(3)(BTO)and carbon nanotubes(CNTs)(denoted PVDF-Trfe/CNTs/BTO).The self-charging supercapacitor power cell device exhibited an energy density of 30μWh cm^(-2)with a high power density of 40 mW cm^(-2)and delivered an excellent self-charging performance of 363 mV(10 N)driven by both the piezoelectric ZnO nanoarrays and the poly(vinylidenefluoride-co-trifluoroethylene)piezoelectric film doped with BaTiO_(3)and carbon *** intriguingly,the device could also be self-charged by 184 mV due to residual stress alone and showed excellent energy conversion efficiency and low self-discharge *** work illustrates for the first time the self-charging mechanism involving electrolyte ion migration driven by both electrodes and films.A comprehensive analysis strongly confirmed the important contribution of the piezoelectric ZnO nanoarrays in the self-charging process of the self-charging supercapacitor power cell *** work provides novel directions and insights for the development of selfcharging supercapacitor power cells.

关键词： MnO_(2) piezoelectric self-charging supercapacitors ZnO nanoarray

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In situ construction of Cu(Ⅰ)-Cu(Ⅱ) pairs for efficient electrocatalytic nitrate reduction reaction to ammonia

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Journal of Energy Chemistry 2025年第1期100卷 106-113页

作者： Muyun Zheng Yuchi Wan Leping Yang Shen Ao Wangyang Fu Zhengjun Zhang Zheng-Hong Huang Tao Ling Feiyu Kang Ruitao Lv State Key Laboratory of New Ceramics and Fine Processing School of Materials Science and EngineeringTsinghua UniversityBeijing 100084China Institute of New Energy Materials and Engineering School of Materials Science and EngineeringFuzhou UniversityFuzhou 350108FujianChina Key Laboratory of Advanced Materials(MOE) School of Materials Science and EngineeringTsinghua UniversityBeijing 100084China Key Laboratory for Advanced Ceramics and Machining Technology of Ministry of Education Tianjin Key Laboratory of Composite and Functional MaterialsSchool of Materials Science and EngineeringTianjin UniversityTianjin 300072China

Electrocatalytic nitrate reduction reaction (NO_(3)-RR) to ammonia under ambient conditions is expected to be a green process for ammonia synthesis and alleviate water pollution *** report a CuO nanoparticles incorporated on nitrogen-doped porous carbon (CuO@NC) catalyst for NO_(3)-*** of Cu(Ⅱ) is reduced to Cu(Ⅰ) during the NO_(3)-RR process to construct Cu(Ⅰ)-Cu(Ⅱ) pairs,confirmed by in situ X-ray photoelectron spectroscopy (XPS) and Raman *** functional theory (DFT) calculations indicated that the formation of Cu(Ⅰ) could provide a reaction path with smaller energy barrier for NO_(3)-RR,while Cu(Ⅱ) effectively suppressed the competition of hydrogen evolution reaction (HER).As a result,CuO@NC catalyst achieved a Faradaic efficiency of 84.2% at -0.49 V versus reversible hydrogen electrode (RHE),and a NH_(3)yield rate of 17.2 mg h^(-1)mg^(-1)*** -0.79 V ***,higher than the HaberBosch process (<3.4 g h^(-1)g^(-1)cat.).This work may open a new avenue for effective NO_(3)-RR by modulating oxidation states.

关键词： Ammonia synthesis Cu oxidation state Electrochemistry Nitrate reduction In situ XPS

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Design and fabrication of bipolar plates for PEM water electrolyser

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Journal of Materials Science & technology 2023年第15期146卷 19-41页

作者： Xiejing Luo Chenhao Ren Jie Song Hong Luo Kui Xiao Dawei Zhang Junjie Hao Zhanfeng Deng Chaofang Dong Xiaogang Li Beijing Advanced Innovation Center for Materials Genome Engineering Key Laboratory for Corrosion and Protection(MOE)Beijing 100083China Institute for Advanced Materials and Technology University of Science and Technology BeijingBeijing 100083China State Key Laboratory of Advanced Power Transmission Technology State Grid Smart Grid Research Institute Co.Ltd.Beijing 102209China

Hydrogen energy,whether in generation plants or utilization facilities,plays a decisive role in the mission to achieve net-zero greenhouse gas emissions,all to minimize *** growing demand for clean energy carrier steadily accelerates the development of hydrogen production processes,and therein proton exchange membrane(PEM)water electrolysis is deemed a promising long-term strategy for hydrogen preparation and *** review retrospects recent developments and applications of bipolar plates(BPs)as key components in PEM fuel cells and water *** main content includes multifaceted challenges in the R&D or fabrication of BPs and potential future trends have also been *** details cover the BPs matrix(metallic materials and carbon composites)and the surface coating types(metal and compound coatings,carbon-based coatings,and polymer coatings),as well as the influence of flow field design for mass ***-term development and feasible researches of BPs are *** in the following aspects:(1)Structural and functional integration of components,such as material fabrication and flow field geometry optimization using 3D printing technology;(2)Introduction of environment-friendly renewable energy for hydrogen production;(3)Research on hydrogen energy reversible systems;(4)Composition optimization of surface coatings based on computational materials science and(5)systematic design expected to evolve into the next generation of BPs.

关键词： PEM water electrolyser Bipolar plates Corrosion Coatings Interfacial contact resistance

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Plasma characteristics and material erosion mechanism in multi-channel wire electrical discharge machining

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Chinese Journal of Aeronautics 2024年第10期37卷 508-525页

作者： Guokang SU Chuanyun ZHANG Junfei LI Xiaolei CHEN Guixian LIU Yongjun ZHANG State Key Laboratory of Precision Electronic Manufacturing Technology and Equipment Guangdong University of TechnologyGuangzhou 510006China Guangdong Key Laboratory of Advanced Manufacturing Technology of Marine Energy Equipment Guangdong University of TechnologyGuangzhou 510006China Guangzhou Key Laboratory of Nontraditional Machining Technology and Equipment Guangdong University of TechnologyGuangzhou 510006China School of Mechanical Engineering Xi’an Technological UniversityXi’an 710021China

Multi-channel wire electrical discharge machining(MC-WEDM)is an advanced and high-efficiency machining technology,but its material erosion mechanism remains *** this study,dual-channel wire electrical discharge machining was utilized as a case study to investigate the impact of the plunging current on both the plasma characteristics and material erosion under complex discharge *** analysis was conducted on the charged particles in the plasma,revealing that the plunging current can influence the trajectory of the plasma by modifying the selfmagnetic *** particle tracking method was employed to simulate the motion of electrons,revealing that in MC-WEDM,electrons exhibited a larger and more uniform *** evolution of the plasma within a single-pulse discharge was observed using high-speed photography technology,and the discharge signals collected from different channels were *** was observed that the plasma in MC-WEDM experienced more intense back-and-forth sweeping on the workpiece surface,facilitating the ejection of molten metal from the molten *** oscillating plasma exhibits a larger processing area and a more uniform distribution of energy,resulting in the formation of larger and shallower discharge ***,the influence of the amplitude and time point of the plunging current on the volume and area of the discharge craters was ***,MC-WEDM significantly reduced the occurrence of holes and micro-cracks and exhibited a thinner recast layer in the continuous discharge experiment.

关键词： Multi-channel WEDM Discharge observation Plunging current Plasma characteristics Material erosion Discharge crater

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Fatigue Crack Initiation and Propagation Dominated by Crystallographic Factors in TiB/near α-Ti Composite

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Acta Metallurgica Sinica(English Letters) 2024年第5期37卷 763-776页

作者： Fanchao Meng Rui Zhang Shuai Wang Fengbo Sun Run Chen Lujun Huang Lin Geng School of Materials Science and Engineering Harbin Institute of TechnologyHarbin 150001China Waikato Centre for Advanced Materials and Manufacturing School of EngineeringUniversity of WaikatoHamilton 3240New Zealand State Key Laboratory of Advanced Welding and Joining Harbin Institute of TechnologyHarbin 150001China

Discontinuously reinforced titanium matrix composites(DRTMCs)with a network structure have been extensively researched due to their superior combination of strength and ***,their fatigue performance has remained *** order to elucidate the fatigue behavior of DRTMCs,a tension-tension fatigue test was performed on a TiB/nearα-Ti composite with network *** results showed that the variability of fatigue lifetime increased as the stress level *** analysis indicated that fatigue crack initiation was associated with facet formation,while the subsequent propagation was hindered by the network structure comprising TiB whiskers and *** characterization further revealed that facets formed due to a combination of shear and normal *** reduction in fatigue lifetime was attributed to an increase in the effective slip length,which was influenced by the orientation of grains near the crack-initiation sites toward basal slip in the life-limiting *** in situ observation suggested that the crack initiation was facilitated by both basal and prismatic slip ofα-Ti as well as fracture of *** propagation was found to be associated with basal and prismatic slip systems with high Schmid factors,regardless of whether the crack was intergranular or intragranular.

关键词： Titanium matrix composite TiBw Fatigue lifetime variability Crack initiation Crack propagation

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