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Surface chemistry of electrode materials toward improving electrolyte-wettability:A method review

InfoMat 2024年第11期6卷 31-65页

作者： Lei Zhao Yuanyou Peng Peiyao Dou Yuan Li Tianqi He Fen Ran State Key Laboratory of Advanced Processing and Recycling of Non-ferrous Metals Department of Polymeric Materials Science and EngineeringSchool of Materials Science and EngineeringLanzhou University of TechnologyLanzhouthe People's Republic of China

The electrolyte-wettability at electrode material/electrolyte interface is a criticalfactor that governs the fundamental mechanisms of electrochemical reactionefficiency and kinetics of electrode materials in practical electrochemicalenergy storage. Therefore, the design and construction of electrode materialsurfaces with improved electrolyte-wettability has been demonstrated to beimportant to optimize electrochemical energy storage performance of electrodematerial. Here, we comprehensively summarize advanced strategies and keyprogresses in surface chemical modification for enhancing electrolytewettabilityof electrode materials, including polar atom doping by post treatment,introducing functional groups, grafting molecular brushes, and surfacecoating by in situ reaction. Specifically, the basic principles, characteristics,and challenges of these surface chemical strategies for improving electrolytewettabilityof electrode materials are discussed in detail. Finally, the potentialresearch directions regarding the surface chemical strategies and advancedcharacterization techniques for electrolyte-wettability in the future are *** review not only insights into the surface chemical strategies forimproving electrolyte-wettability of electrode materials, but also provides strategicguidance for the electrolyte-wettability modification and optimization ofelectrode materials in pursuing high-performance electrochemical energy storagedevices.

关键词： chemical modification electrochemical energy storage electrode materials electrode/electrolyte Interface surface chemistry

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Titanium nitrides as novel reactants for in-situ synthesis of TiB_(2)-based composites with improved properties

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Journal of Materials Science & technology 2023年第14期145卷 48-55页

作者： Ji Zou Huayue Liang Jingjing Liu Weimin Wang Fan Zhang Wei Ji Zhengyi Fu State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of TechnologyWuhan 430070China Hubei Longzhong Laboratory Xiangyang 441000China School of Materials Science and Engineering Wuhan University of TechnologyWuhan 430070China

A novel in-situ reactive approach based on the reactions among TiN,aluminum and boron has been developed to synthesize TiB_(2)-based composites including TiB_(2)-h BN(TB)and TiB_(2)-h BN-AlN(TBA).Fully dense ceramics with fine-grained microstructure were successfully obtained via spark plasma sintering at 1850℃/60 MPa/5 *** analysis suggests h BN flakes were homogenously distributed in the TiB_(2)*** AlN,however,they were elongated into plate-like grains during sintering,in which lots of defects in terms of stacking faults and twinning structures were *** mechanical and thermophysical properties of as-sintered ceramics were comprehensively investigated and ***-corporating AlN significantly improved the flexure strength,hardness,fracture toughness and thermal conductivity of TiB_(2)-h BN *** electrical conductivity of TB(3.06×10^(6)S/m)is larger than that of TBA(2.35×10^(6)S/m)at room temperature,but the value(6×10^(5)S/m)was lower than that of TBA(6.9×10^(5)S/m)at 1173 *** on the measurement of electrical and thermal conductivity,electron and phonon contributions to thermal conductivities of TB and TBA were calculated and their temperature dependences were illustrated.

关键词： Borides Microstructure Spark plasma sintering Mechanical property Thermo-physics property

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Constructing the discrete gradient structure for enhancing interfacial bond strength of Ti6Al4V/NiTi heterostructured materials

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材料科学技术（英文版） 2025年第11期214卷 266-271页

作者： Xingran Li Qiang Li Minghao Nie Pengfei Jiang Shenghong Yan Yue Jiang Zhihui Zhang Key Laboratory of Bionic Engineering(Ministry of Education) Jilin UniversityChangchun 130012China Institute of Structured and Architected Materials Liaoning Academy of MaterialsShenyang 110167China Key Laboratory of Bionic Engineering(Ministry of Education) Jilin UniversityChangchun 130012China State Key Laboratory of Advanced Welding and Joining Harbin Institute of TechnologyHarbin 150001China

*** The Ti6Al4V alloy is extensively utilized across various indus-trial sectors due to its favorable characteristics,such as lightweight design,high strength,and resistance to corrosion[1].In efforts to further reduce weight,functional elements like electric actuators can be substituted with intelligent materials like shape memory alloys(SMAs)[2,3].Among SMAs,NiTi alloy stands out for its sens-ing and actuation capabilities,significantly enhancing the safety and reliability of engineering structures[4,5].Integrating Ti6Al4V and NiTi alloys within a single component holds the potential to provide precise feedback on mechanical,thermal,or environmen-tal conditions[6,7].

关键词： structured niti bond constructing discrete enhancing gradient heterostructure interfacial materials

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Microstructure and yield phenomenon of an extruded Mg-Y-Cu alloy with LPSO phase

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Journal of Rare Earths 2023年第3期41卷 454-461,I0005页

作者： Guangli Bi Niuming Zhang Jing Jiang Yuandong Li Tijun Chen Wei Fu Xiaoru Zhang Daqing Fang Xiangdong Ding State Key Laboratory of Advanced Processing and Recycling of Nonferrous Metals Lanzhou University of TechnologyLanzhou 730050China School of Material Science and Engineering Lanzhou University of TechnologyLanzhou 730050China State Key Laboratory for Mechanical Behavior of Materials Xi'an Jiaotong UniversityXi'an 710049China

A yield phenomenon was firstly reported in an extruded Mg-6.8Y-2.5Cu alloy and the corresponding microstructure was also investigated in this work,The cast alloy is mainly composed ofα-Mg,18R long period stacking order(LPSO)phase,eutectic phase(Mg_(20)Cu_(4)Y_(1)),and Mg_(2)Cu *** 18R LPSO phase at the dendritic grain boundary transforms into the 14H LPSO phase in the grain interior during *** extrusion,the grain size of the homogenized alloy is remarkably refined to-3.69μm and the second phase is significantly broken and distributed in the extrusion *** testing curves of the extrude alloy at room temperature indicate that the yield strength and ultimate tensile strength increase while the elongation of the alloy decreases with increasing strain ***,a yield plateau fo rms and gradually decreases with increasing strain *** yield phenomenon is related to the dislocation multiplication and the interaction between the movable dislocations and solute atoms.

关键词： Extruded Mg-6.8Y-2.5Cu alloy Long period stacking order phase Microstructure Yield phenomenon Rare earths

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Water enhances photocatalytic activity for toluene selective oxidation in acetic acid solution

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Nano Research 2025年第3期18卷 223-233页

作者： Sheng Tian Jinxin Li Binghao Wang Xiong Wang Xingsheng Hu Huijuan Wang Lang Chen Shuang-Feng Yin Advanced Catalytic Engineering Research Center of the Ministry of Education State Key Laboratory of Chemo/Biosensing and ChemometricsCollege of Chemistry and Chemical EngineeringHunan UniversityChangsha 410082China College of Chemistry and Chemical Engineering Central South University of Forestry and TechnologyChangsha 410004China

Photocatalytic oxidation of hydrocarbons to value-added oxygen-containing compounds is a green and sustainable ***,the efficient activation of C(sp^(3))-H bonds under mild conditions remains a significant *** this study,we prepared BiOBr/Bi_(2)MoO_(6)Z-scheme heterostructure for photocatalytic selective oxidation of toluene to benzaldehyde utilizing acetic acid as solvent.A small amount of water as an additive established an acidic environment to facilitate the formation of highly reactive hydroxyl radicals(·OH)through the O_(2)→·O_(2)^(−)→H_(2)O_(2)→·OH ***·OH together with photogenerated holes acted as reactive species dissociate C(sp^(3))-H bonds,which is regarded as the rate-determining step for this reaction,boosting photocatalytic *** to the reaction system without water,the conversion of toluene increased from 23.6%to 39.0%,reaching a toluene conversion rate of 6110μmol·g^(-1)·h^(-1).Additionally,there is a slight improvement in the selectivity of benzaldehyde.

关键词： photocatalytic oxidation of toluene H_(2)O acidic chemical environment hydroxyl radicals BiOBr/Bi_(2)MoO_(6)

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Selenium-modified activated coke: a high-capacity and facile designed Hg0 adsorbent for coal-fired flue gas

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Environmental Science and Pollution Research 2024年第20期31卷 29656-29668页

作者： Zheng, Yang Zhang, Lin Wang, Xiaocong Guo, Fenghui Xing, Yi Li, Guoliang Yue, Tao School of Energy and Environmental Engineering University of Science and Technology Beijing Beijing100083 China State Key Laboratory of Advanced Metallurgy University of Science and Technology Beijing Beijing100083 China

The substantial amount of mercury emissions from coal-fired flue gas causes severe environmental contamination. With the Minamata Convention now officially in force, it is critical to strengthen mercury pollution control. Existing activated carbon injection technologies suffer from poor desulfurization performance and risk secondary-release risks. Therefore, considering the potential industrial application of adsorbents, we selected cost-effective and readily available activated coke (AC) as the carrier in this study. Four metal selenides—copper, iron, manganese, and tin—were loaded onto the AC to overcome the application problems of existing technologies. After 120 min of adsorption, the CuSe/AC exhibited the highest efficiency in removing Hg0, surpassing 80% according to the experimental findings. In addition, the optimal adsorption temperature window was 30–120 °C, the maximum adsorption rate was 2.9 × 10−2 mg·g−1·h−1, and the effectiveness of CuSe/AC in capturing Hg0 only dropped by 5.2% in the sulfur-containing atmosphere. The physicochemical characterization results indicated that the AC surface had a uniform loading of CuSe with a nanosheet structure resembling polygon and that the Cu-to-Se atomic ratio was close to 1:1. Finally, two possible Hg0 reaction pathways on CuSe/AC were proposed. Moreover, it was elucidated that the highly selective binding of Hg0 with ligand-unsaturated Se− was the key factor in achieving high adsorption efficiency and sulfur resistance in the selenium-functionalized AC adsorbent. This finding offers substantial theoretical support for the industrial application of this adsorbent. Graphical Abstract: (Figure presented.) © The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature 2024.

关键词： Mercury compounds

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Inertia Estimation Method of Single-stage Photovoltaic Systems 10

Inertia Estimation Method of Single-stage Photovoltaic Syste...

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10th IEEE International Power Electronics and Motion Control Conference, IPEMC 2024 ECCE Asia

作者： Deng, Tianhao Shi, Xiaojie Yan, Jianan Lin, Lei Huazhong University of Science and Technology State Key Laboratory of Advanced Electromagnetic Engineering and Technology Wuhan430074 China

ISBN: (纸本)9798350351330

Recently, photovoltaic (PV) systems have been leveraged to emulate inertia for the frequency support utilizing their DC capacitors. This approach, however, can deviate the single-stage PV arrays from the maximum power point (MPP), leading to a reduced and time-varying virtual inertia. To accurately estimate the inertia of single-stage PV systems, a method based on the frequency response model and equivalent synchronous generator (SG) is proposed in this paper. The results demonstrate that the inertia of a single-stage PV system, when relying exclusively on conventionally designed DC capacitors, tends to approach zero and demands for enhancement in scenarios requiring frequency support. Finally, all analyses are verified through simulation in MATLAB/Simulink. © 2024 IEEE.

关键词： Frequency response

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Fault locating for traveling-wave accelerators based on transmission line theory

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Nuclear Science and Techniques 2023年第8期34卷 24-34页

作者： Tong-Ning Hu Hai-Meng Wang Yi-Feng Zeng Hong-Jie Xu Li Chen Guang-Yao Feng Yuan-Ji Pei State Key Laboratory of Advanced Electromagnetic Engineering and Technology School of Electrical and Electronic EngineeringHuazhong University of Science and TechnologyWuhan 430074China State Grid Fujian Economic Research Institute Fuzhou 350012China National Synchrotron Radiation Laboratory University of Science and Technology of ChinaHefei 230029China

Radio-frequency(RF)breakdown analysis and location are critical for successful development of high-gradient traveling-wave(TW)accelerators,especially those expected to generate high-intensity,high-power *** with commonly used schemes involving dedicated devices or complicated techniques,a convenient approach for breakdown locating based on transmission line(TL)theory offers advantages in the typical constant-gradient TW-accelerating *** deliver such an approach,an equivalent TL model has been constructed to equate the TW-accelerating structure based on the fun-damental theory of the TL transient response in the time *** equivalence relationship between the TW-accelerating structure and the TL model has been established via analytical derivations associated with grid charts and verified by TL circuit ***,to validate the proposed fault-locating method in practical applications,an elaborate analysis via such a method has been conducted for the recoverable RF-breakdown phenomena observed at an existing prototype of a TW-accelerating-structure-based beam injector constructed at the Huazhong University of Science and *** addition,further considerations and discussion for extending the applications of the proposed method have been *** breakdown-locating approach involving the transient response in the framework of TL theory can be a conceivable supple-ment to existing methods,facilitating solution to construction problems at an affordable cost.

关键词： Traveling-wave structure RF breakdown Fault locating Transmission line

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Copper silicate nanoneedle arrays on reduced graphene oxide like“shelter forest”guiding Zn gradient deposition

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Green Energy & Environment 2025年第5期10卷 967-981页

作者： Na Gao Yang Wang Zhanming Gao Tianming Lv Mengyu Rong Xueying Dong Dongzhi Chen Changgong Meng Yifu Zhang State Key Laboratory of Fine Chemicals School of ChemistryDalian University of TechnologyDalian116024China State Key Laboratory of New Textile Materials&Advanced Processing Technology Wuhan Textile UniversityWuhan430073China Hubei Key Laboratory of Radiation Chemistry and Functional Materials School of Nuclear Technology and Chemistry&BiologyHubei University of Science and TechnologyXianning437100China College of Environmental and Chemical Engineering Dalian UniversityDalian116622China

With the sustainable and efficient development of aqueous zinc ion batteries(AZIBs),the research on addressing the issues of the adaptability and durability of zinc anodes has been hot-topic and is still of great *** this work,inspired by the sand treatment and afforestation of the Gobi Beach in Northwest China to ameliorate the problem of wind and sand encroachment,we propose a material with a morphology similar to that of a“shelter forest”,CuSiO_(3)nanoneedles arrays grown on both sides of reduced graphene oxide(rGO@CuSi),as a coating layer on the zinc metal surface to guide Zn gradient *** presence of rGO improves the electrical conductivity of CuSiO_(3),and the finite element simulation of the electric field and Zn^(2+)concentration proves that the electric field distribution can be effectively homogenized and the local current density can be reduced for the rGO@CuSi-Zn electrode with the surface presenting the shape of a protective *** is due to the abundant pores between the nano-needle array structures on the surface of the electrode,which provide high electron and ion transport paths,and are conducive to achieving uniform Zn deposition,like the principle of wind-sand stabilization by protective *** electrochemical experiments and density functional theory calculations show that the negatively charged surface of r GO@CuSi with good Zn affinity is more capable of guiding Zn^(2+)*** to its inherent material and structural characteristics,the r GO@CuSi-Zn anode has a high specific capacity and good cycling *** study provides insight for interface engineering like protective forest to accelerate the commercialization of high-performance Zn-based batteries.

关键词： Shelter forest CuSiO3nanoneedles arrays Coating Zn anode protection Aqueous Zn-ion batteries

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Interface engineering enabled sintering-resistant metal nanocatalysts via reverse Ostwald ripening

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Science China Chemistry 2024年第9期67卷 2789-2791页

作者： Ying Sun Wenhui Fang Jieshan Qiu Institute of Clean Energy Chemistry Key Laboratory for Green Synthesis and Preparative Chemistry of Advanced Materials of Liaoning ProvinceCollege of ChemistryLiaoning UniversityShenyang 110036China State Key Laboratory of Chemical Resource Engineering College of Chemical EngineeringBeijing University of Chemical TechnologyBeijing 100029China

The design and fabrication of advanced nanocatalysts with the high activity,selectivity,and superior durability remains a big challenge in industrial catalysis[1,2].The sintering of nanocatalysts under the thermally and/or chemically triggered conditions is a bottle-neck issue,which seriously decreases the amount of the exposed active sites and changes the original electronic structure of catalysts,resulting in the irreversible catalyst deactivation and high capital and time cost in industrial operation[3].

关键词： durability irreversible catalysis

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