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Effect of Heat Treatment on Microstructure and Properties of Fe(Al,Ta)/Fe_(2)Ta(Al)Eutectic Composite

Journal of Wuhan University of technology(materials Science) 2025年第2期40卷 374-381页

作者： LI Haolin CUI Chunjuan WANG Yan WANG Zhicong ZHAO Zhiqi WU Tongchao SU Haijun School of Metallurgical Engineering Xi’an University of Architecture&TechnologyXi’an 710055China Shaanxi Key Laboratory of Nano Materials and Technology Xi’an 710055China State Key Laboratory of Solidification Processing Northwestern Polytechnical UniversityXi’an 710072China

Fe(Al,Ta)/Fe_(2)Ta(Al)eutectic composites with solidification rates of 6,20,30,and 80μm/s were prepared by a modified Bridgman directional solidification *** coarse Fe_(2)Ta(Al)Laves phase was precipitated at the eutectic colony boundary during the solidification process,which can affect the stability of microstructure and properties of the *** coarse Laves phase was refined using different heat treatment processes in the present *** influences of different heat treatment parameters on the Laves phase content,lamella/rod spacing,and mechanical properties were investigated in *** addition,the corrosion behaviors of Fe(Al,Ta)/Fe_(2)Ta(Al)eutectic composites before and after being annealed heat treatment in a 3 g/L Na_(2)S_(2)O_(3)solution were also *** is shown that both the content of Laves phase and lamella/rod spacing are gradually decreased after heat ***-hardness is decreased,while the yield strength,compressive strength,and corrosion resistance are *** optimum heat treatment process is selected as well.

关键词： directional solidification heat treatment eutectic composite microstructure properties

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Effect of Structural Configu ations on Mechanical and Shape Recovery Properties of Ni Ti Triply Periodic Minimal Surface Porous Structures

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Chinese Journal of Mechanical Engineering 2024年第6期37卷 303-319页

作者： Shuaishuai Wei Bo Song Lei Zhang Xiaobo Wang Junxiang Fan Zhi Zhang Yusheng Shi State Key Laboratory of Materials Processing and Die and Mould Technology School of Materials Science and EngineeringHuazhong University of Science and TechnologyWuhan 430074China Institute of Materials China Academy of Engineering PhysicsMianyang 621907China Department of Mechanical Engineering City University of Hong KongKowloon 999077China

Based on the advantages of triply periodic minimal surface(TPMS)porous structures,extensive research on NiTi shape memory alloy TPMS scaffolds has been ***,the current reports about TPMS porous structures highly rely on the implicit equation,which limited the design *** this work,novel shell-based TPMS structures were designed and fabricated by laser powder bed *** comparisons of manufacturability,mechanical properties,and shape recovery responses between traditional solid-based and novel shell-based TPMS structures were *** indicated that the shell-based TPMS porous structures possessed larger Young's moduli and higher compressive ***,Diamond shell structure possessed the highest Young's moduli of 605.8±24.5MPa,while Gyroid shell structure possessed the highest compressive strength of 43.90±3.32 *** addition,because of the larger specific surface area,higher critical stress to induce martensite transformation,and lower austenite finish temperature,the Diamond shell porous structure exhibited much higher shape recovery performance(only 0.1%residual strain left at pre-strains of 6%)than other porous *** results substantially uncover the effects of structural topology on the mechanical properties and shape recovery responses of NiTi shape memory alloy scaffolds,and confirm the effectiveness of this novel structural design *** research can provide guidance for the structural design application of NiTi porous scaffolds in bone implants.

关键词： NiTi shape memory alloy Porous structure Laser powder bed fusion Mechanical property Shape recovery property

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Advancing the pressure sensing performance of conductive CNT/PDMS composite film by constructing a hierarchical-structured surface

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Nano materials Science 2023年第4期5卷 343-350页

作者： Ye Zhao Taoyu Shen Minyue Zhang Rui Yin Yanjun Zheng Hu Liu Hongling Sun Chuntai Liu Changyu Shen Key Laboratory of Materials Processing and Mold(Zhengzhou University) Ministry of EducationNational Engineering Research Center for Advanced Polymer Processing TechnologyZhengzhou UniversityZhengzhouHenan450002China China Astronaut Research and Training Center Beijing100094China

Flexible pressure sensors have attracted wide attention due to their applications to electronic skin,health monitoring,and human-machine ***,the tradeoff between their high sensitivity and wide response range remains a *** by human skin,we select commercial silicon carbide sandpaper as a template to fabricate carbon nanotube(CNT)/polydimethylsiloxane(PDMS)composite film with a hierarchical structured surface(h-CNT/PDMS)through solution blending and blade coating and then assemble the h-CNT/PDMS composite film with interdigitated electrodes and polyurethane(PU)scotch tape to obtain an h-CNT/PDMS-based flexible pressure *** on in-situ optical images and finite element analysis,the significant compressive contact effect between the hierarchical structured surface of h-CNT/PDMS and the interdigitated electrode leads to enhanced pressure sensitivity and a wider response range(0.1661 kPa^(-1),0.4574 kPa^(-1)and 0.0989 kPa^(-1)in the pressure range of 0–18 kPa,18–133 kPa and 133–300 kPa)compared with planar CNT/PDMS composite film(0.0066 kPa^(-1)in the pressure range of 0–240 kPa).The prepared pressure sensor displays rapid response/recovery time,excellent stability,durability,and stable response to different loading modes(bending and torsion).In addition,our pressure sensor can be utilized to accurately monitor and discriminate various stimuli ranging from human motions to pressure magnitude and spatial *** study supplies important guidance for the fabrication of flexible pressure sensors with superior sensing performance in next-generation wearable electronic devices.

关键词： Flexible pressure sensor Hierarchical structure Polydimethylsiloxane Carbon nanotubes Electronic skin

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S-scheme ZnO/WO3 heterojunction photocatalyst for efficient H2O2 production

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Journal of materials Science & technology 2022年第29期124卷 193-201页

作者： Zicong Jiang Bei Cheng Yong Zhang S.Wageh Ahmed A.Al-Ghamdi Jiaguo Yu Linxi Wang State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of TechnologyWuhan 430070China Laboratory of Solar Fuel Faculty of Materials Science and ChemistryChina University of GeosciencesWuhan 430074China Department of Physics Faculty of ScienceKing Abdulaziz UniversityJeddah 21589Saudi Arabia

Designing highly efficient photocatalyst for hydrogen peroxide(HO)production is an ideal strategy to avoid the shortcomings of traditional HOproduction and to realize the conversion of solar energy to chemical *** this work,a step-scheme(S-scheme)heterojunction photocatalyst composed of Zn O and WOis carefully prepared by hydrothermal and calcination method for efficient photocatalytic *** ZW30 composite photocatalysts exhibit enhanced activity with the highest HO-production rate of 6788μmol *** results show that the photocatalytic HOproduction process is dominated by a direct two-electron Oreduction *** enhanced photocatalytic HO-production activity is attributed to the formation of interfacial internal electric field(IEF)in the S-scheme heterojunction,which boosts the spatial separation of charge carriers and enables electrons with the strongest reduction power to participate in *** work provides an in-depth insight of the great advantages of S-scheme heterojunction in photocatalytic HOproduction.

关键词： Photocatalysis Hydrogen peroxide Step-scheme heterojunction O2 reduction Zinc oxide

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Microstructure and properties evolution of in-situ fiber-reinforced Ag-Cu-Ni-Ce alloy during deformation and heat treatment

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International Journal of Minerals,Metallurgy and materials 2022年第11期29卷 2000-2011页

作者： Xingqun He Huadong Fu Jianxin Xie Beijing Advanced Innovation Center for Materials Genome Engineering University of Science and Technology BeijingBeijing 100083China Beijing Laboratory of Metallic Materials and Processing for Modern Transportation University of Science and Technology BeijingBeijing 100083China Key Laboratory for Advanced Materials Processing(Ministry of Education) University of Science and Technology BeijingBeijing 100083China

Silver-based alloys are significant light-load electrical contact materials(ECMs).The trade-off between mechanical properties and electrical conductivity is always an important issue for the development of silver-based *** this paper,we proposed an idea for the regulation of the mechanical properties and the electrical conductivity of Ag-11.40Cu-0.66Ni-0.05Ce(wt%)alloy using in-situ composite *** alloy was processed using rolling,heat treatment,and heavy drawing,the strength and electrical conductivity were tested at different deformation stages,and the microstructures during deformation were observed using field emission scanning electron microscope(FESEM),transmission electron microscope(TEM)and electron backscatter diffraction(EBSD).The results show that the method proposed in this paper can achieve the preparation of in-situ composite fiber-reinforced Ag-Cu-Ni-Ce *** the heavy deformation drawing,the room temperature Vickers hardness of the as-cast alloy increased from HV 81.6 to HV 169.3,and the electrical conductivity improved from 74.3%IACS(IACS,i.e.,international annealed copper standard)to 78.6%*** the deformation increases,the alloy strength displays two different strengthening mechanisms,and the electrical conductivity has three stages of *** research provides a new idea for the comprehensive performance control of high-performance silver-based ECMs.

关键词： silver alloy electrical contact materials drawing in-situ fiber-reinforced

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Advances in the study of HOR reaction mechanisms under alkaline conditions

Advanced Sensor and Energy Materials

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advanced Sensor and Energy materials 2024年第1期3卷 23-38页

作者： Yuru Liao Shengchen Wang Yifan Zhang Yue Zhang Yun Gao Xueqin Mu Suli Liu Dingsheng Wang Zhihui Dai School of Chemistry and Molecular Engineering Nanjing Tech UniversityNanjing 211816China State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology InstitutionWuhan 430070China Engineering Research Center of Advanced Rare Earth Materials Department of ChemistryTsinghua UniversityBeijing100084China

Hydrogen energy is an important energy carrier,which is an ideal choice to meet energy demand and reduce harmful gas *** green recycling of hydrogen energy depends on water electrolysis and hydrogen fuel cells,which involves hydrogen oxidation reaction(HOR)and hydrogen evolution reaction(HER).The activity of HER/HOR in alkaline electrolyte,however,exhibits a significantly lower magnitude(2–3 orders)compared to that observed in an acidic medium,which hinders the development of alkaline water electrolysis and alkaline membrane fuel ***,comprehending the characteristics of HOR/HER activity in alkaline electrolytes and elucidating its underlyingmechanismis a prerequisite for the designof advanced *** on this background,this reviewwill briefly summarize the explanations and controversies about the basic HOR mechanism,including bifunctional mechanismand hydrogen binding energy ***,the crucial affecting factors of theHOR kinetics,such as dband center theory,interfacial water recombination,alkali metal cations and electronic effects,are ***,based on the above theories,the design principle,catalytic performance,and latest progress ofHOR electrocatalysts are *** outlook and future research perspectives of advanced catalysts for hydrogen energy recycling are *** reviewis helpful to understand the latest development ofHORmechanismand design cost-effective and high-performance HOR electrocatalysts towards the production of clean renewable energies.

关键词： Hydrogen oxidation reaction(HOR) Electrocatalytic mechanism Hydrogen binding energy theory(HBE) Bifunctional theory

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Low-coordination water Prussian white as cathode for high-performance potassium-ion batteries

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Chinese Chemical Letters 2021年第8期32卷 2433-2437页

作者： Yang Xia Wei Jin Yanyuan Qi Hang Li Zelang Jian Wen Chen State Key Laboratory of Advanced Technology for Materials Synthesis and Processing School of Materials Science and EngineeringWuhan University of TechnologyWuhan 430070China

Prussian whites(PWs) with a three-dimensional framework can accommodate the insertion and extraction of ions with large radius,which have been widely used in potassium ion ***,PWs show the poor cycling performance and inferior rate ability because of high coordinated *** this work,PWs with different water content were synthesized via a coprecipitation method by controlling the reaction *** sample with low-coordination water prohibits the best electrochemical *** shows a high capacity of 120.5 mAh/g at 100 mA/g for potassium-ion batteries(KIBs).It also exhibits a good rate performance,displaying a capacity of 73.2 mAh/g at 500 mA/g.

关键词： Prussian white Potassium ion batteries Low-coordinated water Cathode Reaction temperature

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Molecular dynamics simulation of the tribological performance of amorphous/amorphous nano-laminates

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Journal of materials Science & technology 2022年第10期105卷 226-236页

作者： Dongpeng Hua Wan Wang Dawei Luo Qing Zhou Shuo Li Junqin Shi Maosen Fu Haifeng Wang State Key Laboratory of Solidification Processing Center of Advanced Lubrication and Seal MaterialsNorthwestern Polytechnical UniversityXi’anShaanxi 710072PR China

Because the amorphous/amorphous nano-laminates could enhance signifcantly the mechanical properties of the amorphous materials,they have been widely studied as a new group of structural *** this study,the nano-scratch performance of the Cu_(80)Zr_(20)/Cu_(20)Zr_(80)(A/B-type)and the Cu_(20)Zr_(80)/Cu_(80)Zr_(20)(B/A-type)amorphous/amorphous nano-laminates was evaluated by molecular dynamics *** dependences on the type of indenter,layer thickness,stacking mode and scratch depth were systematically *** is a signifcant size effect for the tribological properties of amorphous/amorphous nanolaminates that the friction force of the A/B-type increases with the increase of layer thickness,but the friction force of the B/A-type decreases as the layer thickness *** interface has an obvious obstruction effect on the shear deformation and reduces the plastic affected region below the scratched ***,the contact environment of the indenter bottom has an important influence on the normal force,so it’s not that the deeper the depth,the greater the normal *** it should not be ignored when evaluating the tribological properties of the amorphous/amorphous *** work can deepen the understanding of hetero-interface on the deformation mechanism during nano-scratch,and help to design amorphous nano-laminates with tailored tribological performance for practical applications.

关键词： Amorphous/amorphous nano-laminates Nano-scratch Molecular dynamics simulation Tribology

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Unveiling the crystallization mechanism of cadmium selenide via molecular dynamics simulation with machine-learning-based deep potential

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Journal of materials Science & technology 2024年第18期185卷 23-31页

作者： Linshuang Zhang Manyi Yang Shiwei Zhang Haiyang Niu State Key Laboratory of Solidification Processing International Center for Materials DiscoverySchool of Materials Science and EngineeringNorthwestern Polytechnical UniversityXi’an 710072China Atomistic Simulations Italian Institute of TechnologyVia E.Melen 83Genoa 16152Italy

Cadmium selenide(CdSe)is an inorganic semiconductor with unique optical and electronic properties that make it useful in various applications,including solar cells,light-emitting diodes,and biofluorescent *** order to synthesize high-quality crystals and subsequently integrate them into devices,it is crucial to understand the atomic scale crystallization mechanism of ***,such studies are still absent in the *** overcome this limitation,we employed an enhanced sampling-accelerated active learning approach to construct a deep neural potential with ab initio accuracy for studying the crystallization of *** brute-force molecular dynamics simulations revealed that a spherical-like nu-cleus formed spontaneously and stochastically,resulting in a stacking disordered structure where the competition between hexagonal wurtzite and cubic zinc blende polymorphs is *** found that pure hexagonal crystal can only be obtained approximately above 1430 K,which is 35 K below its melting ***,we observed that the solidification dynamics of Cd and Se atoms were distinct due to their different diffusion *** solidification process was initiated by lower mobile Se atoms forming tetrahedral frameworks,followed by Cd atoms occupying these tetra-hedral centers and settling down until the third-shell neighbor of Se atoms sited on their lattice ***,the medium-range ordering of Se atoms governs the crystallization process of *** findings indicate that understanding the complex dynamical process is the key to comprehending the crystallization mechanism of compounds like CdSe,and can shed lights in the synthesis of high-quality crystals.

关键词： Crystallization mechanism Cadmium selenide Neural network potential Molecular dynamics simulation Enhanced sampling

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Sequential reactant water management by complementary multisite catalysts for surpassing platinum hydrogen evolution activity

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Nano Research 2024年第3期17卷 1232-1241页

作者： Yu Lin Defang Ding Shicheng Zhu Qunlei Wen Huangjingwei Li Zhen Li Youwen Liu Yi Shen China Engineering Research Center of Nano-Geomaterials of Ministry of Education Faculty of Materials Science and ChemistryChina University of GeosciencesWuhan 430078China State Key Laboratory of Materials Processing and Die&Mould Technology and School of Materials Science and EngineeringHuazhong University of Science and TechnologyWuhan 430074China

Alkaline hydrogen evolution reaction(HER)offers a near-zero-emission approach to advance hydrogen ***,the activity limited by the multiple reaction steps involving H_(2)O molecules transfer,absorption,and activation still unqualified the thresholds of economic ***,we proposed a multisite complementary strategy that incorporates hydrophilic Mo and electrophilic V into Ni-based catalysts to divide the distinct steps on atomically dispersive sites and thus realize sequential regulation of the HER *** Isotopic labeled in situ Raman spectroscopy describes 4-coordinated hydrogen bonded H_(2)O to be free H_(2)O passing the inner Helmholtz plane in the vicinity of the catalysts under the action of hydrophilic Mo ***,potential-dependent electrochemical impedance spectroscopy(EIS)reveals that electrophilic V sites with abundant 3d empty orbitals could activate the lone-pair electrons in the free H_(2)O molecules to produce more protic hydrogen,and dimerize into H_(2) at the Ni *** the sequential management of reactive H_(2)O molecules,NiMoV oxides multisite catalysts surpass Pt/C hydrogen evolution activity(49 mV@10 mA∙cm^(-2) over 140 h).Profoundly,this study provides a tangible model to deepen the comprehension of the catalyst–electrolyte interface and create efficient catalysts for diverse reactions.

关键词： hydrogen evolution activity complementary multisite catalysts sequential reactive water management interfacial water molecules

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