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Segregation behaviors in{101^(-)1}compressive twin boundaries of Mg-RE alloy under deformation at room temperature

Journal of Magnesium and Alloys 2025年第1期13卷 330-337页

作者： Yujie Cui Lili Guo Yunwei Gui Kenta Aoyagi Haotian Tong Qinqin Wei Fangzhou Liu Yuichiro Hayasaka Akihiko Chiba Beijing Advanced Innovation Center for Materials Genome Engineering University of Science and Technology BeijingBeijing 100083China Key Laboratory for Advanced Materials Processing(MOE) University of Science and Technology BeijingBeijing 100083China Beijing Laboratory of Metallic Materials and Processing for Modern Transportation Institute for Advanced Materials and TechnologyUniversity of Science and Technology BeijingBeijing 100083China School of Materials Science and Engineering University of Science and Technology BeijingBeijing 100083China Institute for Materials Research Tohoku University2-1-1 KatahiraAoba-kuSendaiMiyagi 980-8577Japan Department of Materials Science and Engineering Jilin University5988 Renmin StreetChangchunJilin 130025China School of Materials Science and Engineering Wuhan University of TechnologyWuhan 430070China The Electron Microscopy Center Tohoku UniversitySendai 980-8577Japan

Solute atoms and precipitates significantly influence the mechanical properties of Mg *** studies have mainly focused on the segregation behaviors of Mg alloys after *** this study,we investigated the segregation behaviors of an Mg-RE alloy under *** found that the enrichment of solute atoms occurred in{101^(-)1}compressive twin boundaries under compression at 298 K without any annealing in an Mg-RE alloy by scanning transmission electron microscopy and energy-dispersive X-ray *** segregated solutes and precipitates impeded the twin growth,partially contributing to the formation of small-sized{101^(-)1}compressive *** research indicates the twin boundaries can be strengthened by segregated solutes and precipitates formed under deformation at room temperature.

关键词： Magnesium alloys Compression test Scanning/transmission electron microscopy(STEM) Segregation Twin boundaries

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Bi nanoparticles encapsulated in nitrogen-doped carbon as a long-life anode material for magnesium batteries

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Journal of Magnesium and Alloys 2023年第11期11卷 4181-4188页

作者： Junjun Wang Ruohan Yu Jianxiang Wang Juncai Long Fan Qiao Lei Zhang Guanjie He Qinyou An Liqiang Mai State Key Laboratory of Advanced Technology for Materials Synthesis and Processing School of Materials Science and EngineeringWuhan University of TechnologyWuhan 430070China Christopher Ingold Laboratory Department of ChemistryUniversity College London20 Gordon StreetLondon WC1H 0AJUnited Kingdom of Great Britain and Northern IrelandUnited Kingdom Hubei Longzhong Laboratory Wuhan University of Technology(Xiangyang Demonstration Zone)Xiangyang 441000China

Bismuth has garnered significant interest as an anode material for magnesium batteries(MBs) because of its high volumetric specific capacity and low working potential. Nonetheless, the limited cycling performance(≤100 cycles) limits the practical application of Bi as anode for MBs. Therefore, the improvement of Bi cycling performance is of great significance to the development of MBs and is also full of challenges. Here, Bi nanoparticles encapsulated in nitrogen-doped carbon with single-atom Bi embedded(Bi@NC) are prepared and reported as an anode material for MBs. Bi@NC demonstrates impressive performance, with a high discharge capacity of 347.5 mAh g^(-1) and good rate capability(206.4 mAh g^(-1)@500 mA g^(-1)) in a fluoride alkyl magnesium salt electrolyte. In addition, Bi@NC exhibits exceptional long-term stability, enduring 400 cycles at 500 mA g^(-1). To the best of our knowledge, among reported Bi and Bi-based compounds for MBs, Bi@NC exhibits the longest cycle life in this work. The magnesium storage mechanism of Bi@NC is deeply studied through X-ray diffraction, transmission electron microscopy and X-ray photoelectron spectroscopy. This work provides some guidance for further improving the cycling performance of other alloy anodes in MBs.

关键词： Magnesium batteries Bismuth 3D tomography reconstruction Magnesium alloy Single-atom

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Programmable and reconfigurable humidity-driven actuators made with MXene(Ti_(3)C_(2)T_(x))-cellulose nanofiber composites for biomimetic applications

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Nano Research 2024年第7期17卷 6619-6629页

作者： Shaofeng Zeng Yuanji Ye Peidi Zhou Shimin Yi Qiaohang Guo Huamin Chen Guozhen Shen Mingcen Weng School of Mechanical and Automotive Engineering Fujian University of TechnologyFuzhou 350118China School of Materials Science and Engineering Fujian Provincial Key Laboratory of Advanced Materials Processing and ApplicationKey Laboratory of Polymer Materials and Products of Universities in FujianFujian University of TechnologyFuzhou 350118China Institute of Smart Marine and Engineering Fujian University of TechnologyFuzhou 350118China Fujian Key Laboratory of Functional Marine Sensing Materials College of Materials and Chemical EngineeringMinjiang UniversityFuzhou 350108China School of Integrated Circuits and Electronics Beijing Institute of TechnologyBeijing 100081China

Smart actuators have a wide range of applications in bionics and energy *** ability to reconfigure shape is essential for soft actuators to achieve various shapes and deformations,which is a crucial feature for next-generation ***,it is still an enormous challenge to establish a straightforward approach to creating programmable and reconfigurable ***-cellulose nanofiber composite film(MCCF)with a brick-and-mortar hierarchical structure was produced through a vacuum filtration *** demonstrates impressive mechanical properties such as a tensile stress of 68 MPa and a Young’s modulus of 4.65 ***,the MCCF highlights its potential for water-assisted shaping/welding due to the abundance of hydrogen bonds between MXene and cellulose *** also showcases capabilities as a humiditydriven actuator with a rapid response rate of 550°·s^(−1).Using the methods of water-assisted shaping/welding,several bionic actuators(such as flower,butterfly,and muscle)based on MCCF were designed,highlighting their versatility in applications of smart *** research showcases the impressive capabilities of MXene-based actuators and offers beneficial insights for the advancement of future intelligent materials.

关键词： MXene cellulose nanofibers programmable actuators humidity-driven

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Enhanced dynamic deformability and strengthening effect via twinning and microbanding in high density NiCoFeCrMoW high-entropy alloys

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Journal of materials Science & technology 2022年第32期127卷 164-176页

作者： Xuli Liu Yidong Wu Yansong Wang Jinbin Chen Rui Bai Lei Gao Zhe Xu William Yi Wang Chengwen Tan Xidong Hui State Key Laboratory for Advanced Metals and Materials University of Science and Technology BeijingBeijing 100083China School of Materials Science and Engineering Beijing Institute of TechnologyBeijing 100081China State Key Laboratory of Solidification Processing Northwestern Polytechnical UniversityXi’an 710072China

High density alloys with enhanced deformability and strength are urgently required in energy,military and nuclear industries,*** this work,we present a new kind of NiCoFeCrMoW high entropy alloys(HEAs)which possess higher densities and sound velocities than *** systematically investigate the phase structure,quasi-static tensile,dynamic compression and related deformation mechanism of these *** is shown that single FCC or FCC+μdual phases were formed in the HEAs depending on Mo and W content and annealing *** quasi-static tensile and dynamic compression properties have been achieved for these HEAs,***_(30)Co_(30)Fe_(21)Cr_(10)W_(9)HEA annealed at 1573 K exhibited a yield and ultimate tensile strength and elongation of~364 MPa,~866 MPa and~32%,respectively,in quasi-static test;a yield strength of~710 MPa and no fracture under the dynamic strain rate of 4100 s^(-1).Superior strain rate sensitivity(SRS)of yield strength than that of previously reported FCC HEAs have been *** dynamic stress-strain constitutive relation can be described by the modified Johnson-Cook *** for the dynamic deformation mechanism,it is envisaged that the regulation of stacking fault energy and Peierls barrier in current HEAs resulted in occurrences of abundant nanoscale deformation twins and microbands during high strain rate *** synergistic microbanding and twinning effectively contributes to the enhanced dynamic deformability and strengthening ***,the interactions of dislocations with precipitates,stacking faults(SFs)with twins,and between SFs also contribute to extraordinary work-hardening capacity.

关键词： High-entropy alloys Mechanical property Impact behavior Constitutive modeling Dynamic plastic deformation

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Modeling of the process-induced stress, damage, microstructure, and deformation evolution during the pyrolysis process manufacturing CMCs

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Journal of advanced Ceramics 2023年第12期12卷 2345-2359页

作者： Qiang Liu Suwan Ma Zeshuai Yuan Yuan Li Xiaodong Gong Junping Li Man Zhu Tianjian Lu State Key Laboratory of Mechanics and Control for Aerospace Structures Nanjing University of Aeronautics and AstronauticsNanjing 210016China Key Laboratory of Advanced Functional Composites Technology Aerospace Research Institute of Materials&Processing TechnologyBeijing 100076China College of Civil Engineering Nanjing Tech UniversityNanjing 211800China

An insightful understanding of the formation mechanism of process-inherent defects anddeformation is increasingly important for the property evaluation and structural design of ceramicmatrix composites (CMCs). For this purpose, a coupled thermal–diffusive–mechanical modelingapproach was proposed by considering three important phenomena that occur during the pyrolysisprocess for manufacturing CMCs: variations of the physical and mechanical properties of theconstituents, generation and diffusive of pyrolysis gas, and multiple thermal deformations. Thesynergistic effects of these three phenomena on the stress, damage development, microstructuralmorphology, and process deformation of SiC matrix composites were investigated using finiteelement simulations. This new approach was validated by comparing the simulation and experimentalresults. Significant volume shrinkage of the matrix during the polymer-to-ceramic transformationresulted in large tensile stresses and subsequent highly fragmented microstructure in CMCs. Thepyrolysis-gas-induced expansion on the matrix under a damage state may yield a positive processdeformation of CMCs at the macroscale, overcoming the effects of the volume shrinkage of the bulkmatrix at the microscale. The modeling approach is expected to guide high-quality manufacturing ofCMCs and comprehensive studies of structure–processing–property relationships.

关键词： SiC pyrolysis gas process simulation damage process deformation

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Grain refinement and phase precipitation simultaneously improve the strength and ductility of ultra-high strength titanium alloy sheets

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Progress in Natural Science:materials International 2024年第5期34卷 1066-1075页

作者： Xudong Kang Zhaoxin Du Shaojun Wang Jun Cheng Zhiyong Yue Tianhao Gong Jingshun Liu Shuzhi Zhang School of Materials Science and Engineering Inner Mongolia University of Technology Collaborative Innovation Center of Non-ferrous Metal Materials and Processing Technology Co-constructed by the Provience and Ministry Inner Mongolia Autonomous Region Inner Mongolia University of Technology Northwest Institute for Non-Ferrous Metal Research Shanxi Key Laboratory of Biomedical Metal Materials College of Mechanical Engineering Inner Mongolia University of Technology State Key Laboratory of Metastable Materials Science and Technology Yanshan University

The simultaneous high strength and high plasticity of metastable-β titanium alloy sheets remains a difficult challenge. In this work, a 1.2 mm thick sheet of Ti–15Mo–3Al-2.7Nb-0.25Si titanium alloy was obtained after rolling and annealing, and then subjected to a duplex-ageing treatment. The pre-ageing temperatures fell in the range of 300–390°C for 0.5–2h. The re-ageing temperatures were in the range of 500–600°C. After characterization, it was found that the alloy precipitates ω-phases during the pre-ageing process, and the distribution of such ω-phases evolves unevenly and increases in number with the increase of the pre-ageing ***, the strengthening mechanism of the alloy sheet is mainly α-phase nucleation assisted by ω-***, grain refinement appears as a mechanism to ensure the plasticity of the alloy. Finally the ω-phase evolution law is discussed in detail and the strengthening mechanism of the alloy sheet is also analyzed. At this work, a metastable-β titanium alloy sheet with strength of 1445.75 MPa and elongation of 6.55 % was *** study provides a new idea for the microstructure design and process improvement of the metastable-β titanium alloy sheet.

关键词： Metastable-β titanium Duplex-ageing treatment ω-phase Strengthening mechanism

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Swarming Responsive Photonic Nanorobots for Motile-Targeting Microenvironmental Mapping and Mapping-Guided Photothermal Treatment

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Nano-Micro Letters 2023年第9期15卷 205-223页

作者： Luolin Li Zheng Yu Jianfeng Liu Manyi Yang Gongpu Shi Ziqi Feng Wei Luo Huiru Ma Jianguo Guan Fangzhi Mou State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of TechnologyWuhan 430070People’s Republic of China School of Materials and Microelectronics Wuhan University of TechnologyWuhan 430070People’s Republic of China School of Materials Science and Engineering Wuhan University of TechnologyWuhan 430070People’s Republic of China School of Chemistry Chemical Engineering and Life ScienceWuhan University of TechnologyWuhan 430070People’s Republic of China

Micro/nanorobots can propel and navigate in many hard-to-reach biological environments,and thus may bring revolutionary changes to biomedical research and ***,current MNRs lack the capability to collectively perceive and report physicochemical changes in unknown *** we propose to develop swarming responsive photonic nanorobots that can map local physicochemical conditions on the fly and further guide localized photothermal *** RPNRs consist of a photonic nanochain of periodically-assembled magnetic Fe_(3)O_(4)nanoparticles encapsulated in a responsive hydrogel shell,and show multiple integrated functions,including energetic magnetically-driven swarming motions,bright stimuli-responsive structural colors,and photothermal ***,they can actively navigate in complex environments utilizing their controllable swarming motions,then visualize unknown targets(e.g.,tumor lesion)by collectively mapping out local abnormal physicochemical conditions(e.g.,pH,temperature,or glucose concentra-tion)via their responsive structural colors,and further guide external light irradiation to initiate localized photothermal *** work facilitates the development of intelligent motile nanosensors and versatile multifunctional nanotheranostics for cancer and inflam-matory diseases.

关键词： Micro/nanorobots Collective behaviors Responsive photonic crystals On-the-fly sensing Photothermal therapy

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Inclusion Defect Prediction and Multi-process Process Control of Outlet Pipe Casting 75

Inclusion Defect Prediction and Multi-process Process Contro...

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75th World Foundry Congress, WFC 2024

作者： Li, Tianyou Wang, Yu Yu, Peng Mao, Le Pan, Xuzheng Ji, Xiaoyuan Yin, Yajun Zhou, Jianxin State Key Laboratory of Materials Processing and Die & Mould Technology Huazhong University of Science and Technology Wuhan430074 China

Inclusion defects have a great influence on the performance of investment casting. When optimizing the process for inclusion defects, due to the production fluctuation in the casting site, the actual value of the process parameters will deviate from the set value. Therefore, this paper proposes a defect prediction and multi-process process control strategy combining BP neural network and improved particle swarm optimization algorithm. Firstly, data mining is carried out based on Huazhu ERP, and data cleaning is carried out on the collected process parameters. Secondly, an inclusion defect prediction model based on particle swarm optimization and BP neural network (PSO-BP) is established. Compared with the ordinary BP neural network, the accuracy is improved from 92.1% to 94.7%. Thirdly, a multi-process process control strategy combining K-nearest neighbor interpolation method and improved particle swarm optimization algorithm (KNN-IPSO) is proposed to control the process parameters of the subsequent process according to the deviation of the process parameters of the previous process, so as to ensure the stability of the casting quality. Finally, the simulation experiment was carried out. Compared with the ordinary pre-production process optimization method, the defect rate was reduced by 23%. © 2024 75th World Foundry Congress, WFC 2024. All rights reserved.

关键词： Interpolation

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Compressible thermoplastic polyurethane/silver nanorod foams for absorption dominant electromagnetic interference shielding

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Journal of materials Science & technology 2024年第30期197卷 9-16页

作者： Zhaoyang Li Yong Shen Yang Zhou Bing Zhou Chuntai Liu Yuezhan Feng State Key Laboratory of Structural Analysis Optimization and CAE Software for Industrial EquipmentNational Engineering Research Center for Advanced Polymer Processing TechnologyZhengzhou UniversityZhengzhou 450002China Shangqiu Normal University Shangqiu 476000China

Conductive polymer composites(CPCs)have attracted significant interest in the field of flexible electro-magnetic protection,but the challenge of balancing high electromagnetic interference shielding effec-tiveness(EMI SE)and low reflection losses still ***,thermoplastic polyurethane/silver nanorod(TPU/AgNR)composite foams have been successfully prepared using both the salt template and vacuum-assisted thermal compression *** varying the AgNRs content and employing a layer-by-layer bonding approach,a gradient structure with optimized impedance matching is ***“absorb-reflect-reabsorb”EM attenuation mechanismofthe asymmetricgradientEMI shieldingin theinternal structure is exploited,resulting in TPU/AgNR foam(TAF)with high EMI SE and significantly reduced EM ***,the three-layer foams exhibit an average shielding efficacy of 35.5 dB and a reflected power coefficient(R)of 0.085 in the X-band,thereby substantially mitigating secondary EM wave ***,these foams demonstrate exemplary compressive resilience,with the sample main-taining excellent EMI shielding stability even after undergoing 100 compression cycles at 50%***,a straightforward approach is employed to fabricate materials with high EMI SE and low reflectivity,offering the potential for use in EM shielding applications of next-generation flexible elec-tronic devices.

关键词： Thermoplastic polyurethane foam Asymmetric gradient structure EMI shielding EM wave absorption Mechanical properties

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分子间相互作用调控丝素蛋白/聚丙烯酰胺水凝胶的网络形貌和β片结晶,赋予水凝胶优异的黏附、应变和传感性能

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Science China materials 2024年第5期67卷 1533-1542页

作者：杨德桢孙传强韩哲袁宝刚潘栋陈金传许华杰刘春太申长雨 State Key Laboratory of Structural Analysis Optimization and CAE Software for Industrial EquipmentNational Engineering Research Center for Advanced Polymer Processing Technologythe Key Laboratory of Advanced Materials Processing&Mold of Ministry of EducationZhengzhou UniversityZhengzhou450002China

丝素蛋白(SF)作为一种特殊的天然聚合物,具有优异的生物相容性、生物降解性和双亲性,是制备柔性传感器的良好候选者.然而,丝素蛋白的高结晶度和结晶不可控性使获得这种出色的仿生水凝胶传感器具有挑战性.纯SF水凝胶是脆性的,没有黏性.在... 详细信息

丝素蛋白(SF)作为一种特殊的天然聚合物,具有优异的生物相容性、生物降解性和双亲性,是制备柔性传感器的良好候选者.然而,丝素蛋白的高结晶度和结晶不可控性使获得这种出色的仿生水凝胶传感器具有挑战性.纯SF水凝胶是脆性的,没有黏性.在此,我们通过引入聚丙烯酰胺(PAM)到SF水凝胶中来解决这一问题.由于SF/PAM水凝胶具有较强的分子间相互作用,其网络形貌由欧几里得孔改变为非欧几里得孔.同时,其β片结晶很容易被抑制到纳米尺度.这些演变不仅使SF/PAM水凝胶具有优异的机械性能,而且具有出色的黏附性能.与纯PAM水凝胶相比,SF8/PAM水凝胶的拉伸强度、拉伸破坏应变、抗压强度(80%应变下)和黏附性能(在猪皮上)分别提高了133.1%、120.9%、610.8%和104.8%.此外,SF的双亲性可以使碳纳米管(CNTs)在水凝胶中分散良好.制备的CNT0.3/SF8/PAM水凝胶继承并进一步改善了上述性能.除此之外,它还表现出优异的自黏附传感性能,最大灵敏度因子高达10.13,工作应变范围超过1000%,大应变下稳定循环拉伸达500次以上.同时,六种人类活动的精确检测也得到了验证.本工作为实现高性能SF基水凝胶提供了新策略,并证实SF/PAM水凝胶在柔性可穿戴应变传感器中具有广阔的应用前景.

关键词： silk fibroin intermolecular interaction network morphology β-crystallization adhesion hydrogel strain sensor

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