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Bioprocess-inspired preparation of silica with varied morphologies and potential in lithium storage

Journal of materials Science & technology 2021年第13期72卷 61-68页

作者： Fuqiang Wan Wenxuan Wang Zhaoyong Zou Hao Xie Hang Ping Zhengyi Fu State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of TechnologyWuhan430070China School of Chemistry Chemical Engineeringand Life ScienceWuhan University of TechnologyWuhan430070China

As one of the most delicate bioprocesses in nature,biosilicification is closely related to biosilica with various morphologies,and has provided abundant inspiration to materials *** the present study,to explore the biosilica formation process and fabricate silica with an exquisite microstructure for lithiumion battery(LIB)electrodes,a bacterial phage(M13)is used as a biotemplate to synthesize silica with diverse morphologies:cylinders,hexagonal prisms,assemblies of smaller cylinders and nanowires.A facile ethanol bath method is conducted to coat the nanowires with nitrogen-containing carbon and carbon-coated SiO_(2) nanowires with mesochannels(C@msSiO_(2) NWs)are first used as anode materials for *** to the uniform carbon coating and parallel mesochannel structure,the electronic conductivity and capacity to accommodate volume variations were significantly *** the electrochemical perfo rmance test,the composites calcined at 750℃(C@msSiO_(2) NWs-750)show an impressive capacity of 653 mA h g^(-1) at a current density of 500 mA g^(-1) and stability(1000 cycles).In view of the electrochemical test outcomes,the prepa ration of a sophisticated structure with an outstanding potential is easily achieved via a biomimetic strategy.

关键词： Biomimetic preparation Biosilicification M13 phage Silica nanowires Mesochannel

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Double flipping behavior of domains under unidirectional electric field and giant electrostrain by defect regulation

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材料科学技术（英文版） 2025年第12期215卷 15-21页

作者： Yuxin Jia Yongbo Fan Lin Lei Gang Li Yao Su Yuanbiao Gong Guangzhi Dong Weijia Wang Qiang Li Huiqing Fan School of Electronics and Information Northwestern Polytechnical UniversityXi'an710072China Department of Applied Physics Hong Kong Polytechnic University11 Yucai RoadKowloonHong KongChina State Key Laboratory of Solidification Processing School of Materials Science and EngineeringNorthwestern Polytechnical UniversityXi'an710072China Institute of Flexible Electronics School of Materials Science and EngineeringNorthwestern Polytechnical UniversityXi'an710072China School of Advanced Materials and Nanotechnology Xidian UniversityXi'an710071China School of Electronics and Information Northwestern Polytechnical UniversityXi'an710072China State Key Laboratory of Solidification Processing School of Materials Science and EngineeringNorthwestern Polytechnical UniversityXi'an710072China

Ferroelectric materials find extensive applications in brake systems due to their capability to convert elec-trical energy into mechanical *** research has focused on lead-free materials for their envi-ronmentally friendly ***,they exhibit several challenges such as significant negative strain,limited strain values,and large driving *** this work,novel preparation techniques(electro-spinning)were utilized for BaTiO3 to introduce oxygen vacancies and barium defects,facilitating the cre-ation of oriented defect dipoles coupled with an intrinsic electric field(Ei)after poling and *** to the existence of Ei,two minimum points in the strain hysteresis loop were shifted to the same quadrant in the Strain-Electric field ***,when applying an electric field along the Ei direction,negative strain is ***,the actual electric field is the sum of the applied electric field and Ei,thereby reducing the required driving field of the *** stretching of defect dipoles under the electric field further amplified the total *** the proposed mechanisms,this work achieved a substantial unipolar electrostrain of 1.04％under a relatively low electric field(30 kV/cm)in *** work successfully addressed the challenges of high-driving electric fields,limited strain values,and nega-tive strain,providing a comprehensive approach for improving field-induced strain performance through point defect engineering in ferroelectric materials.

关键词： BaTiO3 Electrostrain Defect dipole Intrinsic electric field Electrospinning

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Prediction of intrusive gas pores caused by resin burning in sand core for iron castings

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China Foundry 2025年第1期22卷 23-32页

作者： Ji-wu Wang Xiao-long Wang Yu-cheng Sun Yu-hang Huang Xiu-ming Chen Xiong-zhi Wu Na Li Jin-wu Kang Tao Jing Tian-you Huang Hai-liang Yu School of Mechanical Electronic and Control EngineeringBeijing Jiaotong UniversityBeijing 100044China Weichai Power Co. Ltd.Weifang 261061ShandongChina School of Mechanical Engineering Central South UniversityChangsha 41000China School of Materials Science and Engineering Key Laboratory for Advanced Materials Processing TechnologyTsinghua UniversityBeijing 100084China

In the production of castings,intrusive gas pore represents a kind of common defects which can lead to leakage in high gas-tightness requirement castings,such as cylinder blocks and cylinder heads for *** occurs due to the intrusion of gases generated during the resin burning of the sand core into castings during the casting ***,a gas generation and flow constitution model was established,in which the gas generation rate is a function of temperature and time,and the flow of gas is controlled by the gas release,conservation,and Darcy's *** heat transfer and gas flow during casting process was numerically *** dangerous point of cores is firstly identified by a virtual heat transfer method based on the similarity between heat transfer and gas flow in the sand *** gas pores in castings are predicted by the gas pressure,the viscosity and state of the melt for these dangerous *** distinct sand core structures were designed and used for the production of iron castings,and the simulated gas pore results were validated by the obtained castings.

关键词： gas pore numerical simulation iron casting sand core resin

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Properties and Characteristics of Regolith-Based materials for Extraterrestrial Construction

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Engineering 2024年第6期37卷 159-181页

作者： Cheng Zhou Yuyue Gao Yan Zhou Wei She Yusheng Shi Lieyun Ding Changwen Miao National Center of Technology Innovation for Digital Construction Huazhong University of Science and TechnologyWuhan 430074China School of Civil and Hydraulic Engineering Huazhong University of Science and TechnologyWuhan 430074China School of Materials Science and Engineering Southeast UniversityNanjing 214135China State Key Laboratory of Materials Processing and Die&Mould Technology School of Materials Science and EngineeringHuazhong University of Science and TechnologyWuhan 430074China

The construction of extraterrestrial bases has become a new goal in the active exploration of deep *** the construction techniques,in situ resource-based construction is one of the most promising because of its good sustainability and acceptable economic cost,triggering the development of various types of extraterrestrial construction materials.A comprehensive survey and comparison of materials from the perspective of performance was conducted to provide suggestions for material selection and *** types of typical construction materials are discussed in terms of their reliability and applicability in extreme extraterrestrial ***,thermal and optical,and radiation-shielding properties are *** influencing factors and optimization methods for these properties are *** the perspective of material properties,the existing challenges lie in the comprehensive,long-term,and real characterization of regolith-based construction ***,the suggested future directions include the application of high-throughput characterization methods,accelerated durability tests,and conducting extraterrestrial experiments.

关键词： Extraterrestrial construction Characterization Mechanical property Thermal property Optical property Radiation-shielding

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1800℃下具有优异高强度且含氧化物杂质的高熵二硼化物陶瓷

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Science China materials 2023年第5期66卷 2061-2070页

作者：柳洁杨青青邹冀王为民王新刚傅正义 State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of TechnologyWuhan 430070China Hubei Longzhong Laboratory Xiangyang 441000China Shanghai Institute of Ceramics Chinese Academy of SciencesShanghai 201899China

以硼热/碳热还原合成高熵二硼化物粉体为原料,在2000℃/单轴加压50 MPa条件下,经10分钟放电等离子烧结,成功制备了含有~2 vol%的氧化物和~1 vol%气孔的高熵(Ti_(0.2)Zr_(0.2)Nb_(0.2)Hf_(0.2)Ta_(0.2))B_(2)陶瓷(HEBs).经研究确认,其中... 详细信息

以硼热/碳热还原合成高熵二硼化物粉体为原料,在2000℃/单轴加压50 MPa条件下,经10分钟放电等离子烧结,成功制备了含有~2 vol%的氧化物和~1 vol%气孔的高熵(Ti_(0.2)Zr_(0.2)Nb_(0.2)Hf_(0.2)Ta_(0.2))B_(2)陶瓷(HEBs).经研究确认,其中残留氧化物是固溶少量硼和碳的m-(Hf,Zr)O_(2).室温下HEBs的弹性模量、维氏硬度和断裂韧性分别为508.5 GPa、17.7±0.4 GPa和4.2±0.2 MPa m^(1/2).烧结得到的HEBs具有优良的抗弯强度,特别是其高温强度.HEBs在室温、1600和1800℃下的四点抗折强度分别为400.4±47.0 MPa、695.9±55.9 MPa和751.6±23.2 MPa.对1800℃下断裂的HEBs样品进行了失效分析,在其拉伸和断裂面附近区域,仅在裂纹尖端和孔隙边缘发现了数量有限的位错线的存在,没有观察到位错运动的痕迹.本研究首次报道了高熵二硼化物陶瓷的高温强度,发现其强度直至1800℃并无衰减,并对其高温下的强韧化机制进行了有益的探讨.

关键词： borides high-entropy ceramics high-temperature strength mechanical properties microstructure

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Cobalt-Free BaFe_(0.6)Zr_(0.1)Y_(0.3)O_(3−δ)Oxygen Electrode for Reversible Protonic Ceramic Electrochemical Cells

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Transactions of Tianjin University 2023年第6期29卷 444-452页

作者： Chenghao Yang Jin Li Ao Hu Jian Pu Bo Chi State Key Laboratory of Materials Processing and Die and Mould Technology School of Materials Science and EngineeringHuazhong University of Science and TechnologyWuhan 430074China Hubei Collaborative Innovation Center for Advanced Organic Chemical Materials MOE Key Laboratory for the Green Preparation and Application of Functional MaterialsFaculty of Materials Science and EngineeringHubei UniversityWuhan 430062China MOE Key Laboratory of Material Chemistry for Energy Conversion and Storage Huazhong University of Science and TechnologyWuhan 430074China

Reversible protonic ceramic electrochemical cells(R-PCECs)are ideal,high-effi ciency devices that are environmentally friendly and have a modular *** paper studies BaFe_(0.6)Zr_(0.1)Y_(0.3)O_(3−δ)(BFZY3)as a cobalt-free perovskite oxygen electrode for high-performance R-PCECs where Y ions doping can increase the concentration of oxygen vacancies with a remarkable increase in catalytic *** cell with confi guration of Ni-BZCYYb/BZCYYb/BFZY3 demonstrated promising performance in dual modes of fuel cells(FCs)and electrolysis cells(ECs)at 650℃with low polarization resistance of 0.13Ωcm^(2),peak power density of 546.59 mW/cm^(2)in FC mode,and current density of−1.03 A/cm^(2)at 1.3 V in EC *** alternative operation between FC and EC modes for up to eight cycles with a total of 80 h suggests that the cell with BFZY3 is exceptionally stable and reversible over the long *** results indicated that BFZY3 has considerable potential as an air electrode material for R-PCECs,permitting effi cient oxygen reduction and water splitting.

关键词： Protonic ceramic cells Oxygen electrode Perovskite oxides Cobalt-free Oxygen vacancies

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Synergistic effect between Er-doped MoS_(2)nanosheets and interfacial Mo-N coupling phases for enhanced electrocatalytic hydrogen evolution

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Rare Metals 2024年第3期43卷 1301-1308页

作者： Nian-Peng Li Lei Zhang Hua Zhang Fan-Fei Min Lei Wang Sam Toan Xi-Jun Liu Guang-Zhi Hu State Key Laboratory of Mining Response and Disaster Prevention and Control in Deep Coal Mines School of Materials Science and EngineeringAnhui University of Science and TechnologyHuainan232001China Donghai Laboratory Zhoushan316021China Department of Chemical Engineering University of Minnesota-DuluthDuluthMN55812USA School of Ecology and Environmental Science Institute for Ecological Research and Pollution Control of Plateau LakesYunnan UniversityKunming650504China MOE Key Laboratory of New Processing Technology for Non-Ferrous Metals and Materials Guangxi Key Laboratory of Processing for Non-Ferrous Metals and Featured MaterialsGuangxi UniversityNanning530004China

Hydrogen production via electrochemical water splitting is a promising and green *** one of the most representative transition metal sulfides layered materials,Molybdenum disulfide(MoS_(2))has immense potential for the hydrogen evolution reaction(HER).We successfully prepared a nitrogen-doped carbon(NC)in situ-grown erbium-doped MoS_(2)polyhedral structure(Er-MoS_(2)/NC)that incorporates an interfacial Mo-N coupling phase.

关键词： hydrogen interfacial coupling

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Hierarchical microstructure enables high strength and good ductility in as-cast Fe_(27)Ni_(35)Cr_(18.25)Al_(13.75)Co_(2)Ti_(2)Mo_(2) high-entropy alloy

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Journal of materials Science & technology 2024年第12期179卷 9-21页

作者： Jiacheng Niu Zhiqiang Fu Weiping Chen Tiwen Lu Liangyan Hao Wei Xiong Haiming Wen Guangdong Key Laboratory for Advanced Metallic Materials Processing South China University of TechnologyGuangzhou 510640China National Engineering Research Center of Near-net-shape Forming for Metallic Materials South China University of TechnologyGuangzhou 510640China Key Laboratory of Pressure Systems and Safety Ministry of EducationEast China University of Science and TechnologyShanghai 200237China Physical Metallurgy and Materials Design Laboratory Department of Mechanical Engineering and Materials ScienceUniversity of PittsburghPittsburghPA15261United States of America Department of Materials Science and Engineering Missouri University of Science and TechnologyRollaMissouri 65409United States of America

As-cast alloys often require complex thermomechanical processing to obtain a hierarchical structure to achieve a good combination of strength and *** in this work,a novel hierarchical Fe_(27)Ni_(35)Cr_(18.25)Al_(13.75)Co_(2)Ti_(2)Mo_(2) high-entropy alloy(HEA)with ultra-high tensile strength and excellent ductility was fabricated by direct *** as-cast alloy exhibits hierarchical structure with an ul-trafine lamellar microstructure(ULM),ultrafine rhombus microstructure(URM),ultrafine vermicular mi-crostructure(UVM),nanosized precipitates and spinodal decomposition(SP)that develops during casting and *** incompatibility of face-centered cubic(FCC)and body-centered cubic(BCC)phases in the deformation process leads to heterogeneous deformation-induced(HDI)hardening,which brings the alloy a tensile yield strength(YS)of~1056 MPa,an ultimate tensile strength(UTS)of~1526 MPa and a total elongation(El)of~15.6%.Additionally,the numerous interfaces generated by the hierarchical structure absorb the energy during deformation,effectively retarding the dislocation motion and causing strong work-hardening.

关键词： Direct casting High-entropy alloy Hierarchical microstructure Mechanical properties

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Air sensitivity of electrode materials in Li/Na ion batteries:Issues and strategies

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InfoMat 2022年第6期4卷 83-108页

作者： Ruiwang Zhang Sijie Yang Haobo Li Tianyou Zhai Huiqiao Li State Key Laboratory of Materials Processing and Die&Mould Technology School of Materials Science and EngineeringHuazhong University of Science and TechnologyWuhanChina

With the development of electrode materials in lithium ion batteries-upgrading from LiCoO_(2)and LiFePO_(4)to Ni-rich layered oxides,and the shifting of battery systems from high cost lithium ion to low cost sodium ion technology,the air sensitivity of the electrode materials has become an increasingly important issue in both production and ***,the air sensitivity of electrode materials must be carefully considered throughout nearly all stages of their life,including material design,synthesis,production,storage,packaging,transportation,and battery ***,a fundamental understanding of the air degradation mechanism of electrode materials and the exploration of new methods to enhance their air stability are of great significance for the development of batteries with better ***,we provide a review of the issues related to air exposure of electrode materials in Li/Na ion batteries,including factors related to air sensitivity,degradation mechanisms,and recent progress in improving their air *** merits and existing challenges of different strategies are presented,and a rational design perspective as well as general principles for evaluating air stability are proposed.

关键词： air sensitivity air stability electrode materials lithium ion batteries sodium ion batteries

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Effect of Fe_(2)O_(3)nanoparticle on the interface microstructure and properties of Al/Cu plasma arc fusion-brazing joints

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China Welding 2023年第3期32卷 10-20页

作者：李岩杨楠樊丁黄健康张欢 Materials Science and Engineering College Lanzhou University of TechnologyLanzhou 730050China State Key Laboratory of Advanced Processing and Recycling of Non-Ferrous Metals Lanzhou 730050China

The lap joint of T2 copper plate and 1060 pure aluminum plate was made by using the plasma arc welding method with adding Fe_(2)O_(3)nanoparticles in different *** research analysis found that the thickness of the IMC(intermetallic compound)and eutect-ic region decreased after the addition of nanoparticles due to its inhibitory *** the proportion of Fe_(2)O_(3)nanoparticles is 3%,the in-terface intermetallic compound layer is the ***,after this ratio is continuously increased,the inhibition effect is weakened by the agglomeration of nanoparticles,and the thickness begins to increase *** mechanical and electrical properties of the joint are mainly affected by the thickness of the IMC *** nanoparticles are agglomerated into large particles with high ***,the tensile strength and relative electrical conductivity of the joint are first increasing and then decreasing with the increase of nanoparticle *** the proportion of nanoparticles is 3%,the tensile strength and electrical conductivity are maximum.

关键词： Aluminum-copper dissimilar metals Fe_(2)O_(3)nanoparticles intermetallic compound mechanical properties conductive properties

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