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Hierarchy in materials for maximized efficiency

国家科学评论（英文版） 2020年第11期7卷 1626-1630页

作者： Li-Hua Chen Yu Li Bao-Lian Su State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology China Laboratory of Inorganic Materials Chemistry University of Namur Belgium

HIERARCHY Hierarchy, originated from an ancient Greek word'εραρχα', is a property characterized by the arrangement of a set of individual items [1] that are placed 'above','below'or'a...

HIERARCHY Hierarchy, originated from an ancient Greek word'εραρχα', is a property characterized by the arrangement of a set of individual items [1] that are placed 'above','below'or'at the same level as' one another in different *** items can be physical matter such as atoms, molecules, particles, objects, etc., or can be abstract and intangible entities such as names, values, categories, ***, although we are not consciously aware of its existence, is an essential concept in a wide variety of fields, such as life science, materials science, computer science, philosophy, mathematics, physics,chemistry, biology, geography, topography, organizational theory, systems theory, architecture, urban construction, industrial processes and the social sciences.

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ON THE GRAIN-BOUNDARIES OF ZRO2-BASED SOLID-ELECTROLYTE

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SOLID state IONICS 1995年第1-2期80卷 159-166页

作者： GUO, X YUAN, RZ State Key Laboratory for Synthesis and Processing of Advanced Materials Wuhan University of Technology Wuhan Hubei 430070 P.R. China

On the basis of experiments, the ZrO2 grain boundaries are classified into three types: the ''clean'' grain boundaries, the grain boundaries with amorphous phases and the grain boundaries with crystal phases. The structure and property of the three types of grain boundaries were analyzed from the aspects of microstructure and lattice defects, and the conductivity of the crystal grain boundary phases was calculated with the effective-medium theory to be as three times higher as that of the matrix, an idea of further enhancing the ionic conduction of ZrO2 by modifying grain boundaries was thus proposed. The effect of the ZrO2 grain boundaries on the EMF of the oxygen sensor was discussed with simplified models.

关键词： SOLID ELECTROLYTE GRAIN BOUNDARY OXYGEN SENSOR ZIRCONIUM OXIDE

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synthesis of Ti_3SiC_2/TiB_2 Composite by In-situ Hot Pressing (HP) Method

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Journal of Wuhan University of technology(materials Science) 2008年第6期23卷 863-865页

作者：周卫兵 School of Materials Science and Engineering Wuhan University of Technology State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology

Ti3SiC2/TiB2 composite was successfully obtained by hot pressing Ti/TiC/Si/B4C power *** fraction of TiB2 in Ti3SiC2/TiB2 composite can not exceed 10%.Incorporation of excessive TiB2 will affect the reactions *** and Ti5Si3 were two important intermediate phases during the whole *** microstructure characteristics of the Ti3SiC2/TiB2 composites were analyzed using scanning electron microscopy （SEM） and transmission electron microscopy （TEM）.The experimental results show that the grains of Ti3SiC2/TiB2 composite are structured in a layered form,and the formation of TiB2 particles as reinforcements with elongated or equiaxed shape distributes in Ti3SiC2 matrix.

关键词： titanium silicon carbide in-situ synthesis TiB2

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Fabrication and Characterization of Nano Silver Powder Prepared by Spray Pyrolysis

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Journal of Wuhan University of technology(materials Science) 2009年第6期24卷 871-874页

作者：章桥新 School of Mechanical and Electronic Engineering Wuhan University of Technology State Key Laboratory of Advanced Technology for Materials Synthesis & Processing Wuhan University of Technology

Silver powder was fabricated by spray pyrolysis, using 2%-20% AgNO3 solution, 336-500 mL/h flux of AgNO3 solution, 0.28-0.32 MPa flux of carrier gas and in the 620-820 ℃ temperature range. The effects of furnace set temperature, concentration of AgNO3 aqueous solution, flux of AgNO3 aqueous solution as well as carrier gas on the morphology and particle size distribution of silver powder, were investigated. The experimental results showed that with the high concentration of AgNO3 aqueous solution, the average grain size of silver decreased with the increasing of furnace set temperature. But the gain size distribution was not homogenous, the discontinuous grain growth occurred. With the low concentration of AgNO3 aqueous solution, the higher furnace set temperature made the nano sliver grains sintered together to grow. Nano silver powder about 100 nm was fabricated by spray pyrolysis, using 2wt% AgNO3 solutions, 336 mL/h flux of AgNO3 aqueous solution, 0.32 MPa flux of carrier gas at 720 ℃ furnace set temperature.

关键词： nano silver powder fabrication characterization spray pyrolysis

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S-scheme photocatalyst Bi2O3/TiO2 nanofiber with improved photocatalytic performance

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Journal of materials Science & technology 2020年第17期52卷 145-151页

作者： Rongan He Haijuan Liu Huimin Liu Difa Xu Liuyang Zhang Hunan Province Key Laboratory of Applied Environmental Photocatalysis Changsha UniversityChangsha 410022China State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of TechnologyWuhan 430070China

In this study,a hierarchical Bi2O3/TiO2 fibrous composite was in-situ fabricated on an electrospun TiO2 nanofiber at ambient *** the Bi2O3/TiO2 composite,S-scheme electron migration occurred between Bi2O3 and *** the photocatalytic degradation of phenol under simulated sunlight,the asprepared Bi2O3/TiO2 nanofibers considerably outperformed Bi2O3 nanoparticles and TiO2 *** improvement is contributed by maintaining and effectively utilizing the useful carriers and consuming the useless holes and electrons,realized by the S-scheme heterojunction and hierarchical *** study also provides an alternative design fashion for photocatalysts.

关键词： Electrospinning Bismuth Fiber In-situ synthesis

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synthesis and Characterization of Soluble Aromatic Azopolyamides Containing Sulfone and Ether Units

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Journal of Wuhan University of technology(materials Science) 2009年第4期24卷 594-598页

作者：董丽杰熊传溪 School of Materials Science and Engineering Wuhan University of Technology State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology

A series of new polyamides 3a-d containing aryl-azo, ether and sulfone groups in the main chain were synthesized from bis[4-（4-aminophenoxy）phenyl sulfone] 1 and several azo aromatic diacyl chlorides 2a-d by the low temperature solution polycondensation technique. FTIR spectroscopy, nuclear magnetic resonance （NMR） and elemental analyses confirmed the structure of these polymers. Owing to the aryl and amide groups in the main chain, these polymers exhibit photochromic properties as well as excellent thermal stabilities. The transition temperatures （Tg） are between 242 and 265℃, and the char yields at 800 ℃ in nitrogen atmosphere were above 39%. Based on incorporation of flexible ether linkages and polar sulfone groups, the polyamides show desirable solubility in organic solvents such as DMAc, N,N-dimethylformamide （DMF）, N-methyl-2-pyrroidinone （NMP） and dimethylsulfoxide （DMSO）. And it is exemplified that polyamide containing 2 and 2＇ substitutes performed better solubility.

关键词： aromatic azopolyamide photochromic behavior thermal properties soluble properties

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Preparation,Structure and Dielectric Properties of Tungsten Bronze Ferroelectrics in SrO-Eu_2O_3-TiO_2-Nb_2O_5 System

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Journal of Wuhan University of technology(materials Science) 2011年第2期26卷 312-315页

作者：胡长征 State Laboratory Breeding Base of Nonferrous Metals and Specific Materials Processing Guilin University of Technology Key Laboratory of Nonferrous Materials and New Processing Technology Ministry of EducationGuilin University of Technology State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology

Compounds Sr4Eu2Ti4Nb6O30 and Sr5EuTi3Nb7O30 with filled tetragonal tungsten bronze structure were prepared,and the dielectric characteristics and ferroelectric transition were *** ceramics displayed weak frequency dependence in room temperature dielectric constant,which decreased from 125 to 118 for Sr4Eu2Ti4Nb6O30,from 206 to 195 for Sr5EuTi3Nb7O30 in the frequency range of 10 kHz to 1 *** present ceramics showed a diffuse ferroelectric phase *** frequency independent transition temperature （Tm） indicated the above compounds had no relaxor *** diffuseness （γ） was 1.45 and 1.64 for Sr4Eu2Ti4Nb6O30 and Sr5EuTi3Nb7O30 *** weak ferroelectric of the present materials are indicated from the P-E hysteresis loops,and a small 2Pr of 0.596 μC/cm2 and 0.068 μC/cm2 were observed for Sr4Eu2Ti4Nb6O30 and Sr5EuTi3Nb7O30 respectively.

关键词： tungsten bronze dielectric properties X-ray diffraction phase transition

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Photoexcitation-induced passivation of SnO2 thin film for efficient perovskite solar cells

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National Science Review 2023年第11期10卷 183-191页

作者： Nianyao Chai Xiangyu Chen Zhongle Zeng Ruohan Yu Yunfan Yue Bo Mai Jinsong Wu Liqiang Mai Yi-Bing Cheng Xuewen Wang State Key Laboratory of Advanced Technology for Materials Synthesis and Processing International School of Materials Science and EngineeringWuhan University of Technology National Energy Key Laboratory for New Hydrogen-Ammonia Energy Technologies Foshan Xianhu Laboratory

A high-quality tin oxide electron transport layer(ETL) is a key common factor to achieve high-performance perovskite solar cells(PSCs). However, the conventional annealing technique to prepare high-quality ETLs by continuous heating under near-equilibrium conditions requires high temperatures and a long fabrication time. Alternatively, we present a non-equilibrium, photoexcitation-induced passivation technique that uses multiple ultrashort laser pulses. The ultrafast photoexcitation and following electron–electron and electron–phonon scattering processes induce ultrafast annealing to efficiently passivate surface and bulk defects, and improve the crystallinity of Sn O2, resulting in suppressing the carrier recombination and facilitating the charge transport between the ETL and perovskite interface. By rapidly scanning the laser beam, the annealing time is reduced to several minutes, which is much more efficient compared with conventional thermal annealing. To demonstrate the university and scalability of this technique, typical antisolvent and antisolvent-free processed hybrid organic–inorganic metal halide PSCs have been fabricated and achieved the power conversion efficiency(PCE) of 24.14% and 22.75% respectively, and a12-square-centimeter module antisolvent-free processed perovskite solar module achieves a PCE of 20.26%,with significantly enhanced performance both in PCE and stability. This study establishes a new approach towards the commercialization of efficient low-temperature manufacturing of PSCs.

关键词： photoexcitation-induced passivation ultrafast laser carrier management electron transport layer perovskite solar cells

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Diffusion Kinetics of Carbonate Hydroxyapatite (CHAP) for Adsorbing F^- Dissolved in Water

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Acta Geologica Sinica(English Edition) 2006年第2期80卷 243-248页

作者： HUANG Zhiliang ZHANG Lianmeng LIU Yu WANG Qilin HE Qianjun CHEN Wei State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology Wuhan Hubei 430070 Research Institute of Mineral Material Wuhan Institute of Technology Wuhan Hubei 430073

A systematic research was performed about diffusion kinetics of adsorbing F^- dissolved in water for carbonate hydroxyapatite （CHAP） from the natural hydroxyapatite which was modified by adulterating with CO3^2-. The result shows that the speed of F^- adsorption is controlled by membrane diffusion when F^- concentration is relatively low, which is expressed by the kinetic equation of diffusion Q=0.0005（Ci-C）（t-ti）＋0.3967, or by vacancy diffusion when F^- concentration is relatively high, which is expressed by the kinetic equation of diffusion In[C（o, t）]=8.4718-0.5048Int. Based on the feature of CHAP for adsorbing F^- dissolved in water and its special channel of the structure of CO3^3- modified hydroxyapatite, models of vacancy diffusion and membrane diffusion were established.

关键词： carbonate hydroxyapatite （CHAP） F^- ion diffusion kinetics

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synthesis Approach and Adsorption Properties of SiOC Nanocomposite by Chitin Templating

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Journal of Wuhan University of technology(materials Science) 2022年第6期37卷 1041-1047页

作者： HUANG Yaoxuan PING Hang WANG Kun FU Zhengyi State Key Laboratory of Silicate Materials for Architectures Wuhan University of TechnologyWuhan 430070China State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of TechnologyWuhan 430070China

Using chitin as the templating material,we obtained layered nanocomposites like shrimp or crab shells via a sol-gel self-assembly *** images show a layered structure and XRD patterns present a typical peak of chitin,which indicates the templating role of chitin in the as-received hybrid ***,the layer spacing of chitin/silica hybrid materials is reduced with increasing content of *** the heat treatment for carbonization,layered SiOC nanocomposites with mesoporous structures were obtained and showed good dye adsorption *** present study demonstrates a reliable and self-assembly synthesis technique for the development of advanced high-performance nanocomposites with biomimetic nanostructures.

关键词： chitin sol-gel method self-assembly biomimetic structure SiOC nanocomposite

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