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Damage induced bending strength variation and crack initiation mechanism during thermal cycling shock of laser deposited Stellite alloy coating for engine valve

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Journal of materials Research and technology 2025年 36卷 6062-6074页

作者： Wei Li Rui Cao Feng Zhu Yingjie Yan Jinyuan Ma Yanli Zhu State Key Laboratory of Advanced Processing and Recycling of Non-ferrous Metal Lanzhou University of Technology Lanzhou 730050 China Department of Materials Science and Engineering Lanzhou University of Technology Lanzhou 730050 China Department of Engineering University of Leicester LE1 7RH UK National Key Laboratory of Marine Engine Science and Technology Shanghai 201108 China

Stellite alloy coatings can significantly enhance the wear resistance of valves; however, cyclic thermal loading can induce thermal cycling shock, thereby reducing their service life and overall performance. This study systematically investigates the mechanisms of damage evolution, variations in bending properties, and crack initiation under thermal shocks in laser-deposited Stellite alloy coatings through quenching experiments coupled with multiscale characterization and numerical simulations. The results indicate that the critical temperature of macroscopic cracking is in the range from 350 °C to 400 °C. The damage, such as slip bands, micropores, and microcracks, is primarily induced by thermal stress concentrations driven by rapid cooling. The bending strength of the coatings deteriorates with an increasing damage fraction, which is attributed to the increase of the stress concentration factor in the damage area. Higher peak temperatures produce higher thermal stress, accelerating crack initiation and rapid propagation along the interfaces between the eutectic carbides and the matrix above the critical temperature. Conversely, at lower peak thermal shocking temperatures, the high density of geometrically necessary dislocations (from 74.786 × 10 12 to 178.269 × 10 12 /m 2 ) leads to significant localized stress concentrations, which synergistically with the interfacial damage degradation promote crack initiation.

关键词： Stellite alloy coating Thermal cycling shock Damage Bending strength Crack initiation

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An interpretable uncertainty quantification framework for proton exchange membrane fuel cell degradation prediction

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Renewable Energy 2025年 249卷

作者： Guo, Bingxin Zhu, Wenchao Yang, Wenlong Yang, Yang Wei, Peng You, Li Xiong, Liangli Xie, Changjun School of Automation Wuhan University of Technology Wuhan430070 China State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology Wuhan430070 China Hubei Key Laboratory of Advanced Technology for Automotive Components Wuhan University of Technology Wuhan430070 China State Grid Hubei Electric Power Research Institute Wuhan430077 China National Graduate College for Engineers Wuhan University of Technology Wuhan430119 China

Accurate prediction of fuel cell degradation characteristics is crucial for its control and health diagnosis. However, existing mainstream data-driven methods often fail to adequately account for uncertainty factors during model training and the transient changes in fuel cell characteristics, resulting in predictions that typically provide only point estimates, lacking both credibility and interpretability. To address this, this paper proposes a framework that integrates multi-head attention mechanisms and Bayesian 1D convolution (Bayes-1DCNN-MSH), aimed at quantifying uncertainty in the predictions of various deep learning models while offering interpretable prediction information. This method uses multi-head attention to capture critical multi-dimensional features impacting fuel cell output voltage and applies Bayesian 1D convolution to quantify uncertainty, offering predictions with probability density distributions and confidence intervals for degradation forecasting. The Bayes-1DCNN-MSH structure, validated across six deep learning models, shows a 100 % improvement rate under diverse conditions, significantly enhancing noise resistance and reliability. Experimental results confirm that the framework effectively captures transient feature changes and explains prediction uncertainty through feature probability distributions. This approach improves the reliability and interpretability of fuel cell prediction models, supporting safer integration into sectors like transportation. © 2025 Elsevier Ltd

关键词： Prediction models

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synthesis and structure of NaNbO_3 ceramic powders in ultrahigh pressure field

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Science China(Technological Sciences) 2007年第5期50卷 658-663页

作者： CAO MingHe TIAN Wei LI MingFa SUN WenHua HU MingJi LIU HanXing State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology Wuhan 430070 China State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology Wuhan 430070 China State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology Wuhan 430070 China State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology Wuhan 430070 China State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology Wuhan 430070 China State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology Wuhan 430070 China

The NaNbO3 powders were synthesized and their crystal structure changes were analyzed by ultrahigh pressure up to 6 *** results indicate that the pure NaNbO3 powders can be synthesized at 300℃ under a pressure of 4 GPa, to sig- nificantly restrain the Na element volatilization compared with the traditional syn- thesis method. It is found that the crystal structure of synthesized NaNbO3 changes from low symmetry to high symmetry with the increase of the pressure.

关键词： pressure synthesis, NaNbO3 powder, crystal structure

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Propagation properties and spatial-mode UWOC performance of quasi-perfect optical vortex beam in an improved oceanic channel

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Optics and Laser technology 2025年 188卷

作者： Xiao, Zhiwei Zhou, Jian Wang, Lin Liu, Guizhen Ding, Zhongjun State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology Wuhan430070 China School of Information Engineering Wuhan University of Technology Wuhan430070 China Hubei Key Laboratory of Broadband Wireless Communication and Sensor Networks Wuhan University of Technology Wuhan430070 China National Deep Sea Center Qingdao266237 China

In this study, the Quasi-perfect optical vortex (Quasi-POV) beam with topological charge-independence radial distribution is investigated to enhance the performance of underwater wireless optical communication (UWOC) system based on spatial modes. Additionally, the oceanic channel model is modified to obtain more reliable simulation results. The propagation and communication performance of perfect optical vortex (POV) beam and Quasi-POV beam are compared and analyzed through the modified model. With the optimization of beam's parameters, Quasi-POV beam achieves lower bit-error rate (BER) and higher average capacity in multiple phase shift keying (M−PSK) modulated UWOC system. The results indicate that Quasi-POV beam receives higher normalized intensity and lower crosstalk probability than the POV beam, the average simulation results for the three topologic charge cases show that the BER of Quasi-POV beam at 100 m reduced by approximately 52%, the average capacity of Quasi-POV beam increased by approximately 13.3%. The Quasi-POV beam has better performance than the POV beam in Spatial-Mode UWOC system according to the simulation results, which is more suitable for UWOC system based on spatial modes with smaller values of topologic charge. © 2025 Elsevier Ltd

关键词： Vortex flow

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Nonclassical crystallization of zinc carbonate hydroxide hydrate nanofilm mediated by calcium ions

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Progress in Natural Science:materials International 2022年第5期32卷 579-585页

作者： Qihang Wang Bicheng Yuan Wenduo Gao Huifeng Hu Meng Cai Zhaoyong Zou Zhengyi Fu State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology Hubei Longzhong Laboratory

To satisfy the demand of zinc oxide（ZnO） with advanced muti-functional properties, significant efforts have been made in synthesizing ZnO with various structure and morphology. In particular, hydrothermal method has attracted considerable attentions, in which Zn4CO3（OH）6·H2O（ZCHH） is commonly found as a metastable precursor. However, the formation and crystallization mechanisms of ZCHH are still lacking and urgently needed. In the present study, the crystallization pathway of ZCHH was systematically investigated, and the results demonstrate that the amorphous zinc carbonate（AZC） was an even more unstable precursor. AZC nanoparticles typically aggregated to form one-dimensional（1D） ZCHH nanorods, however, two-dimensional（2D） ZCHH nanofilms were obtained in the presence of a certain concentration of calcium ion. The results suggest that calcium ions could promote the partial dissolution of AZC and facilitate the aggregation of AZC nanoparticles to form crystalline nanofilm. Moreover, 2D ZnO nanofilms could be obtained by heat treatment of the ZCHH nanofilms. The calcium ion mediated nonclassical crystallization pathway provides inspiration for fabrication of ZnO with controlled morphology and offers new opportunities for inorganic regulated material synthesis.

关键词： Zn4CO3(OH)6·H2O Calcium ion Crystallization ZnO nanofilm

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β-relaxation anomaly with low modulus and enhanced recoverable strain in strain glasses crossover

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Acta Materialia 2025年 286卷

作者： Liang, Chuanxin Wang, Dong Ji, Yuanchao Zhang, Jian Ren, Xiaobing Wang, Yunzhi Center of Microstructure Science Frontier Institute of Science and Technology State Key Laboratory for Mechanical Behavior of Materials Xi'an Jiaotong University Xi'an710049 China Frontier Institute of Science and Technology MOE Key Laboratory for Nonequilibrium Synthesis and Modulation of Condensed Matter State Key Laboratory for Mechanical Behavior of Materials Xi'an Jiaotong University Xi'an710049 China Jiangsu Key Laboratory of Advanced Food Manufacturing Equipment and Technology School of Mechanical Engineering Jiangnan University Wuxi214122 China Ferroic Physics Group National Institute for Materials Science Ibaraki Tsukuba305-0047 Japan Department of Materials Science and Engineering The Ohio State University 2041 College Road ColumbusOH43210 United States

The β-relaxation phenomenon in glasses has shown important effects on toughness, ductility, and creep. However, such a β-relaxation has not been reported yet in an important class of glassy materials, ferroic glasses. Here, we report the existence of a β-relaxation anomaly and its physical origin in strain glass systems by combining molecular statics calculation and phase field simulation. The resolved β-relaxation is observed below the strain glass transition temperature at a critical composition accompanied with spontaneous strain glass to normal martensitic phase transformation, and the internal friction for this β-relaxation anomaly fits well with the Arrhenius equation. The superelasticity with β-relaxation has shown low modulus with high recoverable strain over a wide temperature range. Calculated microstructural evolution and the local stress field caused by point defects suggest that the formed percolation-like metastable suppression field under cooling could be the physical origin of the β-relaxation in strain glass systems and is correlated with crystallization. © 2024 Acta Materialia Inc.

关键词： Point defects

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Bioprocess inspired formation of calcite mesocrystals by cation-mediated particle attachment mechanism

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National Science Review 2023年第4期10卷 159-168页

作者： Qihang Wang Bicheng Yuan Wenyang Huang Hang Ping Jingjing Xie Kun Wang Weimin Wang Zhaoyong Zou Zhengyi Fu State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology Hubei Longzhong Laboratory

Calcite mesocrystals were proposed, and have been widely reported, to form in the presence of polymer additives via oriented assembly of nanoparticles. However, the formation mechanism and the role of polymer additives remain elusive. Here, inspired by the biomineralization process of sea urchin spine comprising magnesium calcite mesocrystals, we show that calcite mesocrystals could also be obtained via atachment of amorphous calcium carbonate(ACC) nanoparticles in the presence of inorganic zinc ***, we demonstrate that zinc ions can induce the formation of temporarily stabilized amorphous nanoparticles of less than 20 nm at a significantly lower calcium carbonate concentration as compared to pure solution, which is energetically beneficial for the atachment and occlusion during calcite growth. The cation-mediated particle atachment crystallization significantly improves our understanding of mesocrystal formation mechanisms in biomineralization and offers new opportunities to bioprocess inspired inorganic ions regulated materials fabrication.

关键词： nonclassical crystallization mesocrystal calcium carbonate zinc ion particle attachment

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External field-assisted catalysis

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eScience 2025年

作者： Linbo Jiang Lintao Jiang Xu Luo Ruidong Li Qingqu Zhou Weihao Zeng Jun Yu Lei Chen Shichun Mu State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of TechnologyWuhan 430070 China

In recent years, substantial effort has been dedicated to improving the intrinsic catalytic activity of catalysts through structural modification, component regulation, and chemical state optimization. However, complexity in the design and construction of catalysts, and the possibility of encountering performance ceilings, may constrain their widespread use. Currently, the introduction of in situ external fields, such as force, electric, magnetic, acoustic, light, and thermal fields, is an attractive approach to enhance the catalytic efficiency of catalysts. Such in situ physical fields feature continuity, reversibility, and controllability, and can exert external force or energy on catalysts, thereby affecting their microscopic structures and electron arrangements, accelerating their mass transfer and reaction kinetics. Mutual coupling and conversion among different external fields are also worth exploring. Various in situ external field effects work in multifaceted ways to promote catalysis in energy-environment systems by optimizing mass/energy transfer processes, modifying structures, and accelerating catalytic reaction kinetics, thereby significantly improving the catalytic properties of materials. This review summarizes and analyzes the latest developments in external field-assisted methods for boosting catalyst performance. The external field effect, related catalysis mechanism, and external field-enhanced catalysis are highlighted, and we discuss future challenges, countermeasures, and opportunities for external field-assisted catalysis and beyond.

关键词： Catalysis External field Field-assisted effects Reaction mechanism

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Dynamic response of B4C, TiB2 and TiB2-B4C under shock wave compression

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Ceramics International 2025年

作者： Shu, Zaiqin Jing, Qiang Wan, Mingming Zhang, Jinyong School of Physics and Mechanics Wuhan University of Technology Wuhan430070 China School of Material Science and Engineering Wuhan University of Technology Wuhan430070 China State Key laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology Wuhan430070 China Inner Mongolian Metal Materials Research Institute Yantai264003 China

TiB2-B4C (TBC) has been widely utilized in lightweight armor due to its exceptional mechanical properties. The Hugoniot elastic limit (HEL) has been considered as an important dynamic property of ceramics. This paper presents the shock responses of pure B4C, pure TiB2, and TiB2-B4C composite. By microstructure analysis, the amorphization in B4C and dislocations in TiB2 at shock pressures around 37 GPa in the recycled debris were observed. The dislocations in TiB2 are believed to be the reason for ‘two HELs’ in TiB2. The addition of TiB2 has little effect on the shock properties of B4C, while the shock pressure exceeds HEL. Additionally, a failure wave was detected in the ceramics at shock pressures lower than HEL. A damage parameter was defined to quantify the extent of damage in the failure zone. The incorporation of TiB2 into B4C can significantly slow down failure propagation in TBC at pressure lower than HEL. Furthermore, the analysis of the damage parameter suggests that TBC exhibits superior impact resistance compared to pure B4C and TiB2. © 2025 Elsevier Ltd and Techna Group S.r.l.

关键词： Amorphization

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Hot Deformation Behavior and Microstructure Evolution of Electrolytic Copper

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Xiyou Jinshu Cailiao Yu Gongcheng/Rare Metal materials and Engineering 2025年第4期54卷 920-929页

作者： Zhang, Han Sang, Chen Zhang, Yan Xu, Yangtao Qiao, Jisen Xia, Tiandong School of Materials Science and Engineering Lanzhou University of Technology Lanzhou730050 China State Key Laboratory of Advanced Processing and Recycling of Nonferrous Metals Lanzhou University of Technology Lanzhou730050 China Jinchuan Group Copper Co. Ltd Jinchang737100 China

The hot deformation behavior of electrolytic copper was investigated using a Gleeble-3500 thermal simulation testing machine at temperatures ranging from 500 °C to 800 °C and strain rates ranging from 0.01 s-1 to 10 s-1, under 70% deformation conditions. The true stress-true strain curves were analyzed and a constitutive equation was established at a strain of 0.5. Based on the dynamic material model proposed by Prasad, processing maps were developed under different strain conditions. Microstructure of compressed sample was observed by electron backscatter diffraction. The results reveal that the electrolytic copper demonstrates high sensitivity to deformation temperature and strain rate during high-temperature plastic deformation. The flow stress decreases gradually with raising the temperature and reducing the strain rate. According to the established processing map, the optimal processing conditions are determined as follows: deformation temperatures of 600–650 °C and strain rates of 5–10 s-1. Discontinuous dynamic recrystallization of electrolytic copper occurs during high-temperature plastic deformation, and the grains are significantly refined at low temperature and high strain rate conditions. Copyright © 2025, Northwest Institute for Nonferrous Metal Research. Published by Science Press. All rights reserved.

关键词： Constitutive equations

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