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Ductile and high strength Cu fabricated by solid-state cold spray additive manufacturing

Journal of materials Science & technology 2023年第3期134卷 234-243页

作者： Chaoyue Chen Yingchun Xie Shuo Yin Wenya Li Xiaotao Luo Xinliang Xie Ruixin Zhao Chunming Deng Jiang Wang Hanlin Liao Min Liu Zhongming Ren State Key Laboratory of Advanced Special Steels School of Materials Science and EngineeringShanghai UniversityShanghai 200444China Institute of New Materials Guangdong Academy of SciencesNational Engineering Laboratory of Modern Materials Surface Engineering TechnologyGuangdong Provincial Key Laboratory of Modern Surface Engineering TechnologyGuangzhou 510651China Trinity College Dublin The University of DublinDepartment of Mechanical and Manufacturing EngineeringParsons BuildingDublin 2Ireland State Key Laboratory of Solidification Processing Shaanxi Key Laboratory of Friction Welding TechnologiesSchool of Materials Science and EngineeringNorthwestern Polytechnical UniversityXi’an 710072China State Key Laboratory for Mechanical Behavior of Materials School of Materials Science and EngineeringXi’an Jiaotong UniversityXi’an 710049China Key laboratory for Light-weight Materials Nanjing Techchnology UniversityNanjing 211816China ICB UMR 6303 CNRSUniv.Bourgogne Franche-ComtéUTBMF-90010 BelfortFrance

In this work,pure Cu with excellent strength and ductility(UTS of 271 MPa,elongation to fracture of 43.5%,uniform elongation of 30%)was prepared using cold spray additive manufacturing(CSAM),realizing a breakthrough in the *** in-depth investigation was conducted to reveal the microstructure evolution,strengthening and ductilization mechanisms of the CSAM Cu,as well as the single *** results show that the CSAM Cu possesses a unique heterogeneous microstructure with a bimodal grain structure and extensive infinitely circulating ring-mounted distribution of *** on the single splat observation,the entire copper particle forms a gradient nano-grained(GNG)structure after high-speed impact *** GNG-structured single splat serves as a unit to build the heterogeneous microstructure with bimodal grain distribution during the successive deposition in *** results also show that CSAM can achieve synergistic strengthening and ductilization by controlling the grain refinement and dislocation *** work provides potential for CSAM technique in manufacturing various metallic parts with the desired combination of high strength and good ductility without additional post-treatments.

关键词： Cold spray additive manufacturing Copper Heterogeneous microstructure Strength Ductility

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synthesis of hierarchical SAPO-11-based catalysts with Al-based metal-organic framework derivative as mesoporogen to improve n-decane branched isomerization

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Petroleum Science 2022年第6期19卷 3171-3181页

作者： Xue-Man Wang Cheng-Long Wen Yu Fan State Key Laboratory of Heavy Oil Processing China University of PetroleumBeijing102249China Jiangsu Key Laboratory of Advanced Catalytic Materials and Technology Advanced Catalysis and Green Manufacturing Collaborative Innovation Centerand School of Petrochemical EngineeringChangzhou UniversityChangzhouJiangsu213164China

Hierarchical SAPO-11 molecular sieve(ACS-11) was successfully synthesized employing the Al2O3/carbon(Al_(2)O_(3)/C) composite obtained through the pyrolysis of Al-based metal-organic framework(Al-MOF-96)as *** other carbon-based mesoporogens with strong hydrophobicity,the Al_(2)O_(3)/C interacts with phosphoric acid and generates the AlPO_(4)/C structure,which promotes the Al2O3/C dispersion in the synthesis gel of SAPO-11 and avoids the phase separation between *** Al_(2)O_(3)/C as mesoporogen decreases the crystallite size of SAPO-11 via preventing the aggregation of ***,the addition of Al_(2)O_(3)/C improves the Si distribution in the ACS-11 ***,ACS-11 has smaller crystallites,more mesopores,and a greater amount of medium Bronsted acid centers than the conventional microporous SAPO-11 and the SAPO-11 synthesized using activated carbon as *** corresponding Pt/ACS-11 catalyst exhibits the maximal selectivity to multi-branched C10isomers(23.28%) and the minimal cracking selectivity(15.83%) in n-decane hydroisomerization among these *** research provides a new approach for preparing hierarchical silicoaluminophosphate molecular sieve-based catalysts to produce high-quality fuels.

关键词： Hierarchical SAPO-11 Al_(2)O_(3)/C composite Hydroisomerization Branched isomers

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Deformation Evolution and Perceptual Prediction for Additive Manufacturing of Lightweight Composite Driven by Hybrid Digital Twins

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Chinese Journal of Mechanical Engineering 2024年第5期37卷 94-112页

作者： Jinghua Xu Linxuan Wang Mingyu Gao Chen Jia Qianyong Chen Kang Wang Shuyou Zhang Jianrong Tan Shaomei Fei State Key Lab of Fluid Power and Mechatronic Systems Zhejiang UniversityHangzhou 310058China Zhejiang Key Lab of Advanced Manufacturing Technology School of Mechanical EngineeringZhejiang UniversityHangzhou 310058China State Key Laboratory of Materials Processing and Die and Mould Technology Huazhong University of Science and TechnologyWuhan 430074China Institute of Design Engineering Zhejiang UniversityHangzhou 310058China School of Mechanical and Aerospace Engineering Nanyang Technological UniversitySingapore City 639798Singapore

This paper proposes a deformation evolution and perceptual prediction methodology for additive manufacturing of lightweight composite driven by hybrid digital twins(HDT).In order to improve manufacturing quality of irregular lightweight composite through boosting conceptual design in aeronautic and aerospace engineering,the HDT meaning hybridization of physical and digital domains,including deformation and energy efficiency can be built,where the essential parameters can be perceptually predicted in advance,by virtue of the fusion of physical sensors and digital *** long short term memory(LSTM)can be employed to void vanishing gradient problem and improve predicting precision via Recurrent Neural Networks,thereby laying a foundation for the *** diverse manufacturing requirements of different regions are integrated into the parameters designing phase by attaching region weights confirmed via empiricism and in-service *** effects of slicing strategy and external support structures on manufacturing quality are considered from the perspective of improving dimensional *** manufacturing efficiency and comprehensive costs are accounted as consideration factors,which are perceptually predicted via *** designed manufacturing parameters through HDT were virtually examined by evaluating the deformation and equivalent stress distributions of fabricated lightweight component with composite material through AM process *** physical experiments were conducted to verify the HDT-based pre-designing and optimization method of manufacturing parameters via fused deposition modeling(FDM).The energy consumption of actual manufacturing process was measured via digital power meter and applied to evaluate accuracy of perceptual prediction *** dimensional accuracy and distortion distribution of the manufactured lightweight prototype made with composite material were measured through the coordinate measuring machine(CMM)and 3D optica

关键词： Deformation evolution Perceptual prediction Lightweight composite Hybrid digital twins(HDT) Long short term memory(LSTM)

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Persistence of charge density wave against variation of band structures in V_(x)Ti_(1−x)Se_(2)(x=0–0.1)

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Nano Research 2024年第3期17卷 2129-2135页

作者： Zhanfeng Liu Tongrui Li Wen Zhu Hongwei Shou Mukhtar Lawan Adam Qilong Cui Yuliang Li Sheng Wang Yunbo Wu Hongen Zhu Yi Liu Shuangming Chen Xiaojun Wu Shengtao Cui Li Song Zhe Sun National Synchrotron Radiation Laboratory CAS Center for Excellence in NanoscienceUniversity of Science and Technology of ChinaHefei 230029China CAS Key Laboratory of Strongly-coupled Quantum Matter Physics University of Science and Technology of ChinaHefei 230026China Collaborative Innovation Center of Advanced Microstructures Nanjing 210093China State Key Laboratory of Inorganic Synthesis and Preparative Chemistry College of ChemistryJilin UniversityChangchun 130012China School of Chemistry and Materials Sciences CAS Key Laboratory of Materials for Energy Conversionand CAS Center for Excellence in NanoscienceUniversity of Science and Technology of ChinaHefei 230026China School Zhejiang Institute of Photonelectronics Jinhua 321004China

Charge density wave(CDW)is a phenomenon that occurs in materials,accompanied by changes in their intrinsic electronic *** study of CDW and its modulation in materials holds tremendous significance in materials research,as it provides a unique approach to controlling the electronic properties of ***_(2) is a typical layered material with a CDW phase at low *** V substitution for Ti in TiSe_(2),we tuned the carrier concentration in V_(x)Ti_(1-x)Se_(2) to study how its electronic structures ***-resolved photoemission spectroscopy(ARPES)shows that the band-folding effect is sustained with the doping level up to 10%,indicating the persistence of the CDW phase,even though the band structure is strikingly different from that of the parent compound TiSe_(2).Though CDW can induce the band fold effect with a driving force from the perspective of electronic systems,our studies suggest that this behavior could be maintained by lattice distortion of the CDW phase,even if band structures deviate from the electron-driven CDW *** work provides a constraint for understanding the CDW mechanism in TiSe_(2),and highlights the role of lattice distortion in the band-folding effect.

关键词： charge density wave band structure lattice distortion

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Metal halide perovskite nanocrystals with enhanced photoluminescence and stability toward anti-counterfeiting highperformance flexible fibers

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Nano Research 2023年第2期16卷 3542-3551页

作者： Ranran Zhou Chi-An Cheng Xuyi Wang Kun Nie Jing Wu Mengyun Wu Xiuqiang Duan Ziyao Hu Injamam Ul Huq Hua Wang Luoxin Wang Lefu Mei Haikun Liu Xiaoxue Ma School of Materials Science and Engineering Hubei Key Laboratory for New Textile Materials and ApplicationsKey Laboratory of Polyphenylene Sulfide Fiber and Application in Textile Industryand State Key Laboratory of New Textile Materials&Advanced Processing TechnologyWuhan Textile UniversityWuhan 430200China Beijing Key Laboratory of Materials Utilization of Nonmetallic Minerals and Solid Wastes National Laboratory of Mineral MaterialsSchool of Materials Science and TechnologyChina University of Geosciences(Beijing)Beijing 100083China Department of Bioengineering University of California Los AngelesLos Angeles 90095USA China Bluestar Chengrand Co. LtdHigh Tech Organic Fiber Key Laboratory of Sichuan ProvinceChengdu 610042China Department of Energy and Chemical Engineering Dongguan University of TechnologyDongguan 523808China

As a new type of light-collecting and luminescent material,all-inorganic cesium lead halide CsPbX_(3)(X=Cl,Br,I)perovskite nanocrystals(NCs)are expected to have a wide range of applications in the fields of photovoltaics,optoelectronics,and fluorescence anti-counterfeiting,***,improving the fluorescence performance and stability of CsPbX_(3)perovskite NCs to prompt their applications would promise both fundamental and practical significance for in-depth research in the field of halide *** this paper,we developed a modification strategy to introduce a halogen source,zinc bromide(ZnBr_(2))in hexane,to CsPbX_(3)perovskite that can be conducted under atmospheric conditions with reduced reaction cost and easier *** first work in this paper was to apply the modification strategy to CsPbI_(3)nanowires(NWs).Compared with the untreated NWs,the ZnBr_(2)/hexane modified CsPbI_(3)NWs exhibited better fluorescence ***,based on the study of perovskite NWs,we investigated perovskite nanocrystal-CsPbI_(3)nanorods(NRs)with different morphologies and *** was found that the luminescence properties of nanorods(NRs)were ***,we infiltrated the modified NRs into the aramid/polyphenylene sulfide(ACFs/PPS)composite paper yielded from our previous work to study its fluorescence performance for *** luminescence properties under ultraviolet light irradiation enable better performance in fluorescence *** ZnBr_(2)/hexane modification strategy and the applications studied in this work will expand the scope of perovskite research,laying the foundation for the applications of fluorescent anti-counterfeiting,nano-photoelectric devices,and fluorescent composite materials.

关键词： perovskite nanocomposites photoluminescence fluorescent anti-counterfeiting aramid/polyphenylene sulfide compound paper

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Strength-ductility balance of AZ31 magnesium alloy via accumulated extrusion bonding combined with two-stage artificial cooling Author links open overlay panel

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Journal of Magnesium and Alloys 2023年第5期11卷 1549-1555页

作者： Tingzhuang Han Guangsheng Huang Heng Li Lifei Wang Hua Zhang Fusheng Pan State Key Laboratory of Solidification Processing School of Materials Science&EngineeringNorthwestern Polytechnical UniversityXi'an 710072PR China Shaanxi Key Lab oratory of High-Performance Precision Forming Technology and Equipment Northwestern Polytechnical UniversityXi'an 710072PR China State Key Laboratory of Mechanical Transmission College of Materials Science and EngineeringChongqing UniversityChongqing 400044PR China College of Materials Science and Engineering Taiyuan University of TechnologyTaiyuan 030024PR China Institute for Advanced Studies in Precision Materials Yantai UniversityYantai 264005PR China

AZ31 Mg alloy with heterogeneous bimodal grain structure(smaller grain size of 5-20µm and coarser grain size of 100-200µm)was subjected to accumulated extrusion bonding(AEB)at 250℃combined with two-stage artificial cooling in this work,*** water cooling and artificial *** microstructure developed consecutively as a result of discontinuous dynamic recrystallization(DDRX)for the AEBed samples.{10-12}tensile twinning also played an important role for the AEB with local water cooling at the initial extrusion stage in the *** water cooling could further reduce the DRXed grain size to~2.1µm comparing that without water *** the grain growth rate was reduced by artificial cooling out of extrusion *** the combination of two-stage cooling,the fine DRXed grains at sizing band were almost retained with average grain size of~2.3µm after the sheet out of extrusion die,and the unDRXed grains with high residual dislocation density accumulation were also *** tensile tests results indicated that a good strength-ductility balance with a high ultimate tensile strength(319 MPa vs.412 MPa)and fracture elongation(19.9%vs.30.3%)were *** strength enhancement was mainly owing to the grain refinement and local residual plastic strain reserved by the artificial *** excellent ductility originated from fine DRXed microstructure and ED-tilt double peak texture.

关键词： Magnesium alloy Accumulated extrusion bonding Local water cooling Artificial cooling Microstructure Mechanical properties

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Playdough-like carbon electrode: A promising strategy for high efficiency perovskite solar cells and modules

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eScience 2024年第2期4卷 101-107页

作者： Aodong Zhu Lin Chen Ao Zhang Chenpu Zhu Xinxin Zhang Jie Zhong Fuzhi Huang Yi-Bing Cheng Junyan Xiao School of Materials Science and Engineering Wuhan University of Technology122 Luoshi RoadWuhanHubeiChina State Key Laboratory of Advanced Technologies for Materials Synthesis and Processing Wuhan University of Technology122 Luoshi RoadWuhanHubeiChina School of Chemistry and Chemical Engineering Huazhong University of Science and Technology1037 Luoyu RoadWuhanHubeiChina Research Centre for Advanced Thin Film Photovoltaics Wuhan University of Technology122 Luoshi RoadWuhanHubeiChina Jinan Municipal Bureau of Industry and Information Technology JinanShandongChina

Carbon-based perovskite solar cells(C-PSCs)are promising candidates for large-scale photovoltaic applications due to their theoretical low cost and high ***,the fabrication of high-performance C-PSCs with large-area electrodes remains *** this work,we propose a novel playdough-like graphite putty as top electrode in the perovskite *** electrode with soft nature can form good contact with the holetransporting layer and the conductive substrate at room temperature by a simple pressing technique,which facilitates the fabrication of both small-area devices and perovskite solar *** this preliminary research,the corresponding small devices and modules can achieve efficiencies of 20.29%(~0.15 cm^(2))and 16.01%(~10 cm^(2)),***,we analyze the limitations of the optical and electrical properties of this playdough-like graphite electrode on the device performance,suggesting a direction for further improvement of C-PSCs in the future.

关键词： Perovskite solar cells Large-area module Carbon electrode Conductive playdough

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Quasi-Phase Equilibrium Prediction of Multi-Element Alloys Based on Machine Learning and Deep Learning

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Computers, materials & Continua 2023年第7期76卷 49-64页

作者： Changsheng Zhu Borui Zhao Naranjo Villota Jose Luis Zihao Gao Li Feng College of Computer and Communication Lanzhou University of TechnologyLanzhou730050China State Key Laboratory of Gansu Advanced Processing and Recycling of Non-Ferrous Metal Lanzhou University of TechnologyLanzhou730050China College of Materials Science and Engineering Lanzhou University of TechnologyLanzhou730050China

In this study,a phase field model is established to simulate the microstructure formation during the solidification of dendrites by taking the Al-Cu-Mg ternary alloy as an example,and machine learning and deep learning methods are combined with the Kim-Kim-Suzuki(KKS)phase field model to predict the quasi-phase *** paper first uses the least squares method to obtain the required data and then applies eight machine learning methods and five deep learning methods to train the quasi-phase equilibrium prediction *** obtaining different models,this paper compares the reliability of the established models by using the test data and uses two evaluation criteria to analyze the performance of these *** work find that the performance of the established deep learning models is generally better than that of the machine learning models,and the Multilayer Perceptron(MLP)based quasi-phase equilibrium prediction model achieves the best *** the Convolutional Neural Network(CNN)based model also achieves competitive *** experimental results show that the model proposed in this paper can predict the quasi-phase equilibrium of the KKS phase-field model accurately,which proves that it is feasible to combine machine learning and deep learning methods with phase-field model simulation.

关键词： Deep learning machine learning quasi-phase equilibrium material simulation

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Significantly enhanced energy storage performance of BaTiO3-based amorphous thin films through the synergistic function of variable valence ions

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Ceramics International 2025年

作者： Yao, Yiming Tao, Cheng Huang, Rui Zhang, Jian Zhang, Tianyu Hao, Hua Yao, Zhonghua Liu, Hanxing Cao, Minghe State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology Wuhan430070 China International School of Materials Science and Engineering Wuhan University of Technology Wuhan430070 China

Amorphous thin films have been widely studied due to the excellent breakdown strength in recent years. However, their practical application faces significant challenges primarily caused by low polarization and energy density. Herein, we propose a multi-variable valence ions doping strategy to enhance the energy storage performance of BaTiO3-based amorphous thin films. The Ba0.92Bi0.08Ti1-x(Ni0.5Mn0.5)xO3(BBTNM) amorphous thin films were fabricated by chemical solution deposition method. In addition, the synergistic effects of variable valence ions (Ni, Mn) on the microstructure, dielectric and energy storage properties of the films were systematically studied. Compared with the undoped Ba0.92Bi0.08TiO3(BBT) film, the polarization and energy storage performance of the BBTNM film have been significantly improved owing to the defect dipoles generated by the incorporation of variable valence ions. Notably, a high discharge energy density of 93.3 J/cm3 together with an energy efficiency of 83 % could be achieved in the x = 0.08 film at 7.05 MV/cm. Simultaneously, the film exhibits excellent thermal stability within the range of 20 °C–160 °C, and still maintains favorable performance after 105 cycles. Overall, this work introduces a new approach for designing BaTiO3-based thin film materials. © 2025

关键词： Amorphous films

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Machine learning in energy storage materials

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Interdisciplinary materials 2022年第2期1卷 175-195页

作者： Zhong-Hui Shen Han-Xing Liu Yang Shen Jia-Mian Hu Long-Qing Chen Ce-Wen Nan State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Center of Smart Materials and DevicesWuhan University of TechnologyWuhanChina International School of Materials Science and Engineering Wuhan University of TechnologyWuhanChina State Key Lab of New Ceramics and Fine Processing School of Materials Science and EngineeringTsinghua UniversityBeijingChina Department of Materials Science and Engineering University of Wisconsin-MadisonMadisonWisconsinUSA Department of Materials Science and Engineering The Pennsylvania State UniversityUniversity ParkPennsylvaniaUSA

With its extremely strong capability of data analysis,machine learning has shown versatile potential in the revolution of the materials research ***,taking dielectric capacitors and lithium‐ion batteries as two representa-tive examples,we review substantial advances of machine learning in the research and development of energy storage ***,a thorough discussion of the machine learning framework in materials science is ***,we summarize the applications of machine learning from three aspects,including discovering and designing novel materials,enriching theoretical simulations,and assisting experimentation and ***,a brief outlook is highlighted to spark more insights on the innovative implementation of machine learning in materials science.

关键词： dielectric capacitor energy storage lithiumion battery machine learning

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