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Electropolymerization of Ni(salen) on carbon nanotube carrier as a capacitive material by pulse potentiostatic method

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Science China Chemistry 2012年第7期55卷 1338-1344页

作者： LI JianLing GAO Fei ZHANG YaKun KANG FeiYu WANG XinDong YE Feng YANG Jun State Key Laboratory of Advanced Metallurgy University of Science and Technology BeijingBeijing 100083China China Electric Power Research Institute Beijing 100192China Department of Material Science and Engineering Tsinghua UniversityBeijing 100084China State Key Laboratory of Multiphase Complex Systems Institute of Process Engineering Chinese Academy of SciencesBeijing 100080China

The composites of poly[Ni（salen）] and multi-walled carbon nanotube （MWCNT） were synthesized by pulse potentiostatic method. The composites were characterized by field emission scanning electron microscopy, Fourier transform infrared spectra, and electrochemical impedance spectroscopy. The wrapping of carbon nanotubes with poly[Ni（salen）] varied significantly with anodic pulse duration. Variance of structure of poly[Ni（salen）] caused by anodic pulse duration affected the ability of absorption to solvent molecules or solvated ions, which was indicated by v （C≡N） intensity. The ability to store/release charge of poly[Ni（salen）] caused by redox switching was evaluated in the form of low-frequency capacitance. Correlations of chargetransfer resistance/ionic diffusion resistance with potential and anodic pulse duration were investigated.

关键词： poly[Ni（salen）] carbon nanotubes potential pulse electrochemical impedance spectroscopy

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Investigation on Heat Transfer Characteristics of the H-type Finned Tube in Flue Gas with High Content of Ash

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Energy Procedia 2017年 105卷 4680-4684页

作者： Tao Han Chang’an Wang Qi Cao Wufeng Chen Defu Che State Key Laboratory of Multiphase Flow in Power Engineering School of Energy and Power Engineering Xi’an Jiaotong University Xi’an 710049 China

H-type finned tube is rarely used in waste heat recovery power generation stations, though it has an efficient heat transfer performance in large thermal power stations (WHRPGs, hereafter). To date, understanding of heat performance of H-type finned tube in WHRPGs is still lacked. The heat transfer characteristics of H-type finned tube in gas with high content of ash in WHRPGs was investigated in practical cement plant in present work. The actual ash deposition pattern was observed meanwhile. The characteristics of heat transfer process including heat transfer coefficient, heat effective coefficient, and flue resistance at gas velocity between 4.5 - 6.5 m·s –1 are obtained. Experimental results show that the heat transfer coefficient increases with gas velocity linearly, the heat effective coefficient nearly keep stable on the other hand, and serious ash-block problem occurs in flow area in the heat exchanger at the gas velocity of 4.5 - 6.5 m·s –1 . The max heat transfer coefficient remain below 10 w·m –2 ·k –1 , implying heat performance of H-type finned tube in WHRPGs is possibly inefficient.

关键词： H-type finned tube heat performance heat transfer

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Slagging characteristics on the superheaters of a 12 MW biomass-fired boiler

Slagging characteristics on the superheaters of a 12 MW biom...

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作者： Niu, Yanqing Tan, Hongzhang Ma, Lin Pourkashanian, Mohamed Liu, Zhengning Liu, Yang Wang, Xuebin Liu, Haiyu Xu, Tongmo State Key Laboratory of Multiphase Flow in Power Engineering School of Energy and Power Engineering Xian Jiaotong University Xian 710049 China School of Process Environmental and Materials Engineering University of Leeds Leeds LS2 9JT United Kingdom

In an attempt to understand the problem of severe slagging in biomass-fired boilers, slags formed on the fourth-, second-, and first-stage superheaters in a 12 MW biomass-fired grate furnace have been collected, sampled, and analyzed using X-ray fluorescence (XRF) and X-ray diffraction (XRD) techniques. The slag collected on each superheater has a unique morphology and structure. The slag on the fourth-stage superheater is loose and porous, while on the secondary and the primary superheaters, the slag shows a clear layered structure of different colors and levels of hardness. Aluminosilicate is the major component in the slag on the fourth-stage superheater, which is formed by Si, Al, and alkali species. On both the secondary and primary superheaters, the sticky sylvine, potassium calcium sulfate, and aphthitalite in the bottom layer trap coarse, large particles, resulting in further slagging. In the alternating layers, the particles containing high concentrations of K, Na, and Cl form the initial deposit layer, the yellow layer in the secondary superheater. Then, it traps the coarse, large particles containing high Si, Al, Ca, Mg, and Fe to form the brown layer. Similarly, the particles in the pale-yellow layer of the primary superheater containing high concentrations of K, Na, and Cl form the initial deposit layer, and then, it traps the coarse, large particles containing high Si, Al, Ca, Mg, and Fe to form the black layer. Accompanied by the periodic blowing, the alternating layer is formed and the slag gradually becomes thicker. © 2010 American Chemical Society.

关键词： Iron

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THE VELOCITY FIELD OF multiphase flow AND EFFICIENCY OF BIOLOGICAL AERATION FILTER

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Journal of Hydrodynamics 2010年第2期22卷 260-264页

作者： CHENG Wen HU Bao-wei YANG Chun-di CHENG Wen-juan Environment Research Institute Xian University of Technology Xi＇an 710048 China State Key Laboratory of Multiphase Flow in Power Engineering Xi＇ an Jiaotong University Xi＇an 710049 China Key Laboratory of Northwest Water Resources and Environmental Ecology of Education Ministry Xi＇anUniversity of Technology Xi＇an 710048 China Yuanpei College Shaoxing University Shaoxing 312000 China Environment Research Institute Xi＇an University of Technology Xi＇an 710048 China

Aeration is an important factor affecting the biological aeration *** a set of experiment device specially designed for the purpose,and the particle image velocimetry technique,the velocity field of the gas-liquid two-phase flow is studied under different *** various simulated aeration states were actually applied to the experimental device of sewage treatment,and the results of the numerical simulation were *** final experimental results indicate that the most efficient state occurs when the ratio of water in aeration tank h / w =1,the diameter of capillary tubes d=0.6mm and the velocity of bubbles v=0.3m/s.

关键词： ratio of water diameter of capillary tube bubbles velocity sewage disposal efficiency

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Numerical Simulation Study on Wet Gas flowmetering Overreading Characteristics of Venturi Tube under Low Pressure Conditions 3

Numerical Simulation Study on Wet Gas Flowmetering Overreadi...

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3rd International Conference on Testing Technology and Automation engineering, TTAE 2023

作者： Xing, Zhaokai Wu, Fang Hu, Rongyuan Xu, Guobin Xie, Hongjun Fan, Shaohua Wang, Shanshan Yang, Jinfeng Meng, Lin Liu, Qihang State Nuclear Electric Power Planning Design & Research Institute Co Ltd Beijing100095 China Shandong Nuclear Power Company Ltd Yantai265116 China Xi'an Jiaotong University State Key Laboratory of Multiphase Flow in Power Engineering Xi'an710049 China

ISBN: (纸本)9781510674769

A numerical simulation study of Venturi overreading characteristics is carried out with Mixture model and Realizable k-e model, and a prediction model of Venturi overreading under low pressure conditions is proposed. Compared with the existing experimental data, it demonstrates that the numerical simulation results have high accuracy, the results indicate that the quality is the main factor affecting the Venturi overreading Meanwhile, the model in this paper is compared with with ten classical overreading prediction models such as homogeneous model. It shows that the average prediction deviation of the model in this paper is 3.2%, ranking second, and the maximum prediction deviation is 7.3%. This study can provide reference for the study of Venturi wet gas flowmetering overreading model, and also provide a theoretical basis and options for flowmetering technology. © 2024 SPIE.

关键词： Forecasting

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Three-dimensional positioning method for moving particles based on defocused imaging using single-lens dual-camera system

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Chinese Optics Letters 2016年第3期14卷 42-46页

作者：周骛金娜贾敏华杨荟楠蔡小舒 Institute of Particle and Two-Phase Flow Measurement/Shanghai Key Laboratory of Multiphase Flow and Heat Transfer in Power Engineering University of Shanghai for Science and Technology Key Laboratory of Energy Thermal Conversion and Control of Ministry of Education Southeast University

A method to three-dimensional position moving particles with one lens and two cameras is proposed. Two par- ticle images with different degrees of defocusing are adopted to solve the ambiguous problem of particle positions. A single-lens dual-camera system is developed to simultaneously capture these two images for the moving par- ticles. The measurement principles and theoretical analysis are introduced first, and then simulated investiga- tions and experimental research are discussed. The measurement errors in the simulations and experiments are less than 1% and 4%, respectively, in 20 times the depth of field of the system, which validates the feasibility of this method.

关键词： Optics Physics

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Design of High-Order Difference Scheme and Analysis of Solution Characteristics - Part II: A Kind of Third-Order Difference Scheme and New Scheme Design Theory

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Numerical Heat Transfer: Part B -- Fundamentals 2007年第3期52卷 271-295页

作者： Jin, W. W. Tao, W. Q. wqtao@*** State Key Laboratory of Multiphase Flow in Power Engineering School of Energy &Power Engineering Xi''an Jiaotong University Xi''an People''s Republic of China

In this Part II, on the basis of the general style design of second-order difference scheme and the analysis of the absolutely stable scheme proposed in Part I, the companion article, the general design method of any high-order difference scheme is proposed. Based on this method, a new kind of third-order difference scheme including 17 different variants is constructed, which uses the same grid points as existing second-order difference schemes but is different from them in that the grids are chosen symmetrically from two sides of the interface. Because they have the same matrix style created by the same grid plots of the discretization equation, these third-order schemes require the same CPU time and memory as the second-order schemes; however, this kind of symmetrical third-order difference scheme will keep the consistency between the false diffusion and the stability, and the stability of the scheme is better than that of the existing biased second-order scheme. Further research shows that under the conditions of matrix style and computer memory, the scheme constituted by symmetrically numbered grids from two sides of the interface with odd order of accuracy can maintain consistency between numerical accuracy and stability better than any kind of scheme designed according to the 'upwind' idea. Based on this understanding, a new scheme design theory called symmetric and odd-order accuracy scheme design theory is proposed. [ABSTRACT FROM AUTHOR]

关键词： power (Mechanics) NUMERICAL analysis HEAT transfer multiphase flow NUMERICAL calculations

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Influence of(Mg_(1/3)Nb_(2/3))complex substitutions on crystal structures and microwave dielectric properties of Li2TiO3 ceramics with extreme low loss

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Journal of Materiomics 2018年第4期4卷 368-382页

作者： Huan-Huan Guo Di Zhou Li-Xia Pang Jin-Zhan Su Electronic Materials Research Laboratory Key Laboratory of the Ministry of Education&International Center for Dielectric ResearchSchool of Electronic and Information EngineeringXi'an Jiaotong UniversityXi'an710049China Micro-optoelectronic Systems Laboratories Xi'an Technological UniversityXi'an710032ShaanxiChina International Research Centre for Renewable Energy State Key Laboratory of Multiphase Flow in Power EngineeringXi'an Jiaotong UniversityXi'anShaanxi710049China

A systematic investigation of the Li2Ti1-x(Mg_(1/3)Nb_(2/3))xO_(3)(0.1≤x≤0.35)solid solutions synthesized by traditional solid-state reaction method is reported in this *** the composition range of 0.1≤x≤0.25,a monoclinic rock salt structured solid solution was *** x increased to 0.3,a phase transition from monoclinic to cubic phase,along with an order-disorder phase transition,was *** x increased from 0.1 to 0.35,the microwave permittivity(εr)and temperature coefficient of resonant frequency(TCF)of the Li2Ti1-x(Mg_(1/3)Nb_(2/3))xO_(3)ceramics decreased linearly from 21.0 to 18.6,+27.1 to-19.4 ppm/℃,*** Li_(2)Ti_(0.75)(Mg_(1/3)Nb_(2/3))0.25O_(3)ceramic sintered at 1170℃shows high performance of microwave dielectric properties with aεr~19.6,a Qf(Q=quality factor=1/dielectric loss;f=resonant frequency)~109,770 GHz(at 7.7 GHz)and a near zero TCF~t 1.2 ppm/℃.Moreover,the burying sintering process can reduce the volatilization of lithium so that the porosity of Li_(2)Ti_(0.75)(Mg_(1/3)Nb_(2/3))0.25O_(3)ceramic was reduced effectively,which made Li_(2)Ti_(0.75)(Mg_(1/3)Nb_(2/3))0.25O_(3)ceramic promising for future *** area electron diffraction patterns,high-resolution transmission electron microscopy,Raman and far-infrared spectra were employed to study the relation between crystal structure and microwave dielectric properties in detail.

关键词： Microwave dielectric properties Phase evolution Crystal structure High quality

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Surfactant’s Effect on the Photoactivity of Fe-doped TiO2

Surfactant’s Effect on the Photoactivity of Fe-doped TiO2

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中国材料大会2012

作者： Qingyun Chen Chao Xue Xianglin Li Yunhai Wang State Key Laboratory of Multiphase Flow in Power Engineering Xi'an Jiao tong University

ISBN: (纸本)9783037856062

Ti(OC4H9)4 was used as the Ti precursor and titanium dioxide (TiO2 ) was prepared by sol-gel method. During the preparation process, Fe3+ was doped and different surfactants, such as SDS, PEG, CTAB, were added to improve the photocatalytic activity of TiO2 . The effect of the different type of surfactants on the structure of Fe-doped TiO2 was discussed. The photocatalysts were characterized by thermogravimetric thermal analysis, X-ray diffraction, scanning electron microscopy and UV-Vis spectrophotometer. The red shift of the absorption edge of the Fe-doped TiO2 prepared by using different surfactants was observed. Methyl orange (MO) solution was degraded under sunlight irradiation to evaluate the photocatalytic performance. The results indicated that the photocatalyst prepared with PEG addition had the highest activity and MO degradation ratio could reach 90% after 4 hours irradiation with the best photocatalyst.

关键词： Sol-gel, Iron-doped titania, Photocatalytic activity, Surfactant.

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Experimental study on optical properties of the collector

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International Solar Energy Society Solar World Congress 2007, ISES 2007

作者： Wang, Juan Zhao, Liang Li, Huashan School of Science Xi'an Jiaotong University P.O. Box 2264 Xi'an 710049 China State Key Laboratory of Multiphase Flow in Power Engineering Xi'an Jiaotong University Xi'an 710049 China

ISBN: (纸本)9781622765447

Solar collector is one of the most important parts of solar chimney power plant. It plays an important role in improving the efficiency and saving the cost of the whole system. In this paper, several transparent materials which could be used as the collector were chosen to study the optical properties. The materials include polymethyl methacrylate (PMMA), polycarbonate (PC), perspex (PS) and ordinary glass. Firstly, an experiment device was designed with the collector angles varying from 15° to 60°. Secondly, different thickness of glass and different slope angles of the collector of these materials mentioned above on transmittance was compared. The effect of pollutions caused by the natural environment such as dust, rain and aging on these materials was considered in the experiment. Based on the experimental results, a conclusion was made that PMMA has the highest transmittance among the four materials without considering other factors.

关键词： Optical properties

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