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Steel-refractory reactions in lanthanum-,cerium-,and ytrium-added steels

Journal of Iron and Steel Research International 2024年第6期31卷 1473-1485页

作者： Jian Kang Hong-po Wang Yu Wang College of Materials Science and Engineering Chongqing UniversityChongqing 400044China The State Key Laboratory of Mechanical Transmissions Chongqing UniversityChongqing 400044China

A systematic experimental study was conducted on the similarities and differences in the reactions between commonly used rare earth elements(REEs)and frequently used refractories in the steelmaking *** results indicate that the reaction behaviors of La,Ce,and Y with MgO,Al_(2)O_(3),and MgO·Al_(2)O_(3) crucibles differed *** consumption rates of La,Ce,and Y in the molten steel were in descending order of La>Ce>Y for smelting with all three kinds of *** the REEs reacted with the crucible,the contents of Mg and Al showed a trend of first increasing and then *** laboratory-scale smelting conditions,the reactions related to REEs were dominated by steel-crucible reactions,and the contact area between the unit mass of molten steel and refractory materials mainly determined the consumption rates of ***-and Ce-crucible reactions generated loose and porous reaction interfaces;however,Y-crucible reactions generated a dense Y_(2)O_(3) layer,dramatically suppressing the consumption rate of *** calculation indicated that the reactions between rare earth and different refractory materials were first-order *** crucible materials significantly affected the product type and morphology of the steel-crucible reaction interfaces,thereby influencing the consumption rate of *** reactions between REEs and refractories must be seriously considered,especially for small-scale smelting.

关键词： Rare earth Inclusion Refractory Thermodynamics Dynamics

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AR assistance for efficient dynamic target search

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Computational Visual Media 2023年第1期9卷 177-194页

作者： Zixiang Zhao Jian Wu Lili Wang State Key Laboratory of Virtual Reality Technology and Systems School of Computer Science and EngineeringBeihang UniversityBeijingChina

When searching for a dynamic target in an unknown real world scene,search efficiency is greatly reduced if users lack information about the spatial structure of the *** target search studies,especially in robotics,focus on determining either the shortest path when the target’s position is known,or a strategy to find the target as quickly as possible when the target’s position is ***,the target’s position is often known intermittently in the real world,e.g.,in the case of using surveillance *** goal is to help user find a dynamic target efficiently in the real world when the target’s position is intermittently *** order to achieve this purpose,we have designed an AR guidance assistance system to provide optimal current directional guidance to users,based on searching a prediction *** assume that a certain number of depth cameras are fixed in a real scene to obtain dynamic target’s *** system automatically analyzes all possible meetings between the user and the target,and generates optimal directional guidance to help the user catch up with the target.A user study was used to evaluate our method,and its results showed that compared to free search and a top-view method,our method significantly improves target search efficiency.

关键词： augmented reality(AR) search guidance

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A survey on federated learning:a perspective from multi-party computation

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Frontiers of Computer science 2024年第1期18卷 93-103页

作者： Fengxia LIU Zhiming ZHENG Yexuan SHI Yongxin TONG Yi ZHANG Institute of Artificial Intelligence and Key Laboratory of Mathematics Informatics Behavioral Semantics Beihang UniversityBeijing 100191China State Key Laboratory of Software Development Environment and Advanced Innovation Center for Future Blockchain and Privacy Computing Beihang UniversityBeijing 100191China Pengcheng Laboratory Shenzhen 518055China Zhongguancun Laboratory Beijing 100190China Institute for Mathematical Sciences and Engineering Research Center of Financial Computing and Digital Engineering Renmin University of ChinaBeijing 100872China

Federated learning is a promising learning paradigm that allows collaborative training of models across multiple data owners without sharing their raw *** enhance privacy in federated learning,multi-party computation can be leveraged for secure communication and computation during model *** survey provides a comprehensive review on how to integrate mainstream multi-party computation techniques into diverse federated learning setups for guaranteed privacy,as well as the corresponding optimization techniques to improve model accuracy and training *** also pinpoint future directions to deploy federated learning to a wider range of applications.

关键词： sfederated learning multi-party ycomputation privacy-preserving data mining distributed learning

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Structural Optimization of Polyimide Foam via Composition with Hyperbranched Polymer Modified Fluorinated Carbon Nanotubes

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Chinese Journal of Polymer science 2023年第1期41卷 117-128页

作者： Jian Liu Zhuang Nie Rui Qin An-Ping Ou Tao Zhang Xu Wang Xiang-Yang Liu College of Polymer Science and Engineering State Key Laboratory of Polymer Material and EngineeringSichuan UniversityChengdu610065China Zhejiang Key Laboratory of Marine Materials and Protective Technologies Key Laboratory of Marine Materials and Related TechnologiesCASNingbo315000China

The key to improve the foam’s performance is to optimize the cellular structure and its bulk-material ***,the hyperbranched polymer modified fluorinated multi-walled carbon nanotube(HPMCNT-F)based on the nucleophilic reactions of MCNT-F was successfully prepared and used to composite with PI *** pristine MCNT shows a poor dispersity and weak interfacial interaction with PI *** HPMCNT-F exhibits an excellent dispersity and effectively forms covalent/non-covalent interaction with PI matrix due to the surface-structure engineering,resulting in the enhancement of the PI ***,HPMCNT-F works as a heterogeneous nucleation agent in PI foam to optimize the cellular *** enhancement of PI bulk and the optimizing of cellular structure result in the increase of compressive special strength of composite foam by 58.9%with a low loading of 1.6 wt%***,the hyperbranched polymers effectively prevent the thermal conduction among HPMCNT-F,and the isolated MCNTs effectively block thermal radiation through absorption and reflection the infrared ***,the thermal conductivity was reduced by 8.0%simultaneously.

关键词： Foams Nanocomposites Mechanical properties Thermal properties

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Enhanced preparation of dendritic metallic vanadium in recyclable NaCl-KCl-VCl_(2) molten salt by V_(2)CO electrolysis

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Rare Metals 2024年第8期43卷 3961-3973页

作者： Jia-Liang An Ming-Yong Wang Yong-Zheng Jia Jin-Tao Zhang Bao-Yan Feng Shu-Qiang Jiao State Key Laboratory of Advanced Metallurgy University of Science and Technology BeijingBeijing 100083China College of Material Science and Engineering Hebei Province Laboratory of Inorganic Nonmetallic MaterialsNorth China University of Science and TechnologyTangshan 063210China

A promising method for the preparation of pure metallic vanadium via V_(2)CO anode electrolysis was proposed and *** simple and controllable synthesis of a molten chloride salt containing VCl_(2) by an insitu reaction between VCl_(3) and metallic vanadium was verified through thermodynamic analysis and ***-KCl-VCl_(2) molten salt exhibited excellent recycling performance and could be repetitively used to prepare metallic vanadium by V_(2)CO *** V^(2+) ions remained in the molten salt after *** electrolysis conditions,such as the cathode diameter,current density,V^(2+) ion concentration,and temperature,were optimised to maximise the current *** was also simulated to reveal the regulatory *** highest current efficiency was 85%.The purity of metallic vanadium was up to 99.8%.In this study,an easy and efficient preparation of pure metallic vanadium was achieved.

关键词： V_(2)CO Metallic vanadium Current efficiency Molten salt electrolysis

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Bottlebrush Random Copolymers at Oil-Oil Interfaces

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Chinese Journal of Chemistry 2025年第2期43卷 139-145页

作者： Yaxin Wang Yunhui Wen Yuzheng Luo Shuailong Li Jiaqiu Luo Shaowei Shi State Key Laboratory of Chemical Resource Engineering Beijing Advanced Innovation Center for Soft Matter Science and EngineeringBeijing University of Chemical TechnologyBeijing100029 China

Oil-in-oil nonaqueous emulsions are of great interest for developing emulsion-templated polymers and encapsulation systems that are incompatible with water-sensitive ***-made amphiphilic block copolymers are by far the most efficient stabilizers for oil-in-oil emulsions while less attention is given to copolymers with more complex ***,we report the stabilization of DMSO-silicone oil interface by bottlebrush random copolymers(BRCPs)containing norbornene backbones with densely grafted poly(methyl methacrylate)(PMMA)and polystyrene(PS)side *** assembly kinetics of BRCPs at the DMSO-silicone oil interface can be divided into three processes,including diffusion,reconfiguration and reorganization,and can be varied by tuning the degree of polymerization of the backbone(NB).Due to the high efficiency of BRCPs in reducing the interfacial tension,when using BRCPs as stabilizers,stable silicone oil-in-DMSO traditional emulsions and high internal phase emulsions(HIPEs)can be successfully obtained,while no stable emulsions can be achieved with linear PMMA-b-PS serving as the *** study,for the first time,underscores the great potential of amphiphilic bottlebrush copolymers in preparing oil-in-oil *** the advances in polymerization strategy,a broad variety of amphiphilic bottlebrush copolymers are expected to be synthesized and applied in the stabilization of nonaqueous biphasic systems.

关键词： Bottlebrush copolymers Oil-oil interfaces|Emulsions Surfactants Assembly dynamics

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Plasma induced grain boundaries to boost electrochemical reduction of CO_(2)to formate

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Journal of Energy Chemistry 2024年第8期95卷 636-643,I0014页

作者： Guan Wang Shengtao Zhong Xiaoqian Xiong Jing Li Fangyuan Wang Li Huo Daoxiong Wu Xingqi Han Zhitong Wang Qi Chen Xinlong Tian Peilin Deng School of Marine Science and Engineering State Key Laboratory of Marine Resource Utilization in South China SeaHainan UniversityHaikou 570228HainanChina

Bismuth-based catalysts are highly promising for the electrochemical carbon dioxide reduction reaction(eCO_(2)RR)to formate ***,achieving high activity and selectivity towards formate and ensuring long-term stability remains *** work reports the oxygen plasma inducing strategy to construct the abundant grain boundaries of Bi/BiO_x on ultrathin two-dimensional Bi *** oxygen plasma-treated Bi nanosheet(OP-Bi)exhibits over 90%Faradaic efficiency(FE)for formate at a wide potential range from-0.5 to-1.1 V,and maintains a great stability catalytic performance without significant decay over 30 h in flow ***,membrane electrode assembly(MEA)device with OPBi as catalyst sustains the robust current density of 100 mA cm^(-2)over 50 h,maintaining a formate FE above 90%.In addition,rechargeable Zn-CO_(2)battery presents the peak power density of1.22 mW cm^(-2)with OP-Bi as bifunctional *** mechanism experiments demonstrate that the high-density grain boundaries of OP-Bi provide more exposed active sites,faster electron transfer capacity,and the stronger intrinsic activity of Bi *** situ spectroscopy and theo retical calculations further elucidate that the unsaturated Bi coordination atoms between the grain boundaries can effectively activate CO_(2)molecules through elongating the C-O bond,and reducing the formation energy barrier of the key intermediate(^(*)OCOH),thereby enhancing the catalytic performance of eCO_(2)RR to formate product.

关键词： CO_(2)electroreduction Bi nanosheet Grain boundary Unsaturation Bi atoms MEA device

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A blast furnace fault monitoring algorithm with low false alarm rate:Ensemble of greedy dynamic principal component analysis-Gaussian mixture model

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Chinese Journal of Chemical engineering 2023年第5期57卷 151-161页

作者： Xiongzhuo Zhu Dali Gao Chong Yang Chunjie Yang State Key Laboratory of Industrial Control Technology College of Control Science and EngineeringZhejiang UniversityHangzhou 310027China

The large blast furnace is essential equipment in the process of iron and steel manufacturing. Due to the complex operation process and frequent fluctuations of variables, conventional monitoring methods often bring false alarms. To address the above problem, an ensemble of greedy dynamic principal component analysis-Gaussian mixture model(EGDPCA-GMM) is proposed in this paper. First, PCA-GMM is introduced to deal with the collinearity and the non-Gaussian distribution of blast furnace ***, in order to explain the dynamics of data, the greedy algorithm is used to determine the extended variables and their corresponding time lags, so as to avoid introducing unnecessary noise. Then the bagging ensemble is adopted to cooperate with greedy extension to eliminate the randomness brought by the greedy algorithm and further reduce the false alarm rate(FAR) of monitoring results. Finally, the algorithm is applied to the blast furnace of a large iron and steel group in South China to verify *** with the basic algorithms, the proposed method achieves lowest FAR, while keeping missed alarm rate(MAR) remain stable.

关键词： Chemical processes Principal component analysis Gaussian mixture model Process monitoring Ensemble Process control

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A novel high-Cr CoNi-based superalloy with superior high-temperature microstructural stability, oxidation resistance and mechanical properties

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International Journal of Minerals,Metallurgy and Materials 2024年第6期31卷 1373-1381页

作者： Xiaorui Zhang Min Zou Song Lu Longfei Li Xiaoli Zhuang Qiang Feng Beijing Advanced Innovation Center for Materials Genome Engineering State Key Laboratory for Advanced MetalsUniversity of Science and Technology BeijingBeijing 100083China

A novel multicomponent high-Cr CoNi-based superalloy with superior comprehensive performance was prepared,and the evaluation of its high-temperature microstructural stability,oxidation resistance,and mechanical properties was conducted mainly using its cast polycrystalline *** results disclosed that the morphology of theγ′phase remained stable,and the coarsening rate was slow during the long-term aging at 900–1000℃.The activation energy forγ′precipitate coarsening of alloy 9CoNi-Cr was(402±51)kJ/mol,which is higher compared with those of CMSX-4 and some other Ni-based and Co-based ***,there was no indica-tion of the formation of topologically close-packed phases during this *** these factors demonstrated the superior microstructural stability of the *** mass gain of alloy 9CoNi-Cr was 0.6 mg/cm^(2) after oxidation at 1000℃ for 100 h,and the oxidation resistance was comparable to advanced Ni-based superalloys CMSX-4,which can be attributed to the formation of a continuous Al_(2)O_(3) protective ***,the compressive yield strength of this cast polycrystalline alloy at high temperatures is clearly higher than that of the conventional Ni-based cast superalloy and the compressive minimum creep rate at 950℃ is comparable to that of the conventional Ni-based cast superalloy,demonstrating the alloy’s good mechanical properties at high *** is partially because high Cr is bene-ficial in improving theγandγ′phase strengths of alloy 9CoNi-Cr.

关键词： CoNi-based superalloys microstructure coarsening oxidation mechanical properties

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Photocatalytic dicarboxylation of strained C-C bonds with CO_(2) via consecutive visible-light-induced electron transfer

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Chinese Chemical Letters 2024年第6期35卷 268-273页

作者： Yi Liu Zhe-Hao Wang Guan-Hua Xue Lin Chen Li-Hua Yuan Yi-Wen Li Da-Gang Yu Jian-Heng Ye Key Laboratory of Green Chemistry&Technology of Ministry of Education College of ChemistrySichuan UniversityChengdu 610064China College of Polymer Science and Engineering State Key Laboratory of Polymer Materials EngineeringSichuan UniversityChengdu 610065China State Key Laboratory of Elemento-Organic Chemistry Nankai UniversityTianjin 300071China

Dicarboxylic acids have a wide range of applications in the polymer industry to construct valuable *** has recently emerged as an efficient and sustainable strategy to generate dicarboxylic ***,photocatalytic dicarboxylation with CO_(2) is mainly limited to unsaturated bonds,and the dicarboxylation of C-C single bonds still remains a ***,we report a photocatalytic dicarboxylation of C-C single bonds in strained rings with CO_(2) units via consecutive photo-induced electron transfer(ConPET).It is also the first photocatalytic reductive ring-opening reaction of ***,this transition-metal-free protocol exhibits good functional group tolerance,broad substrate scope,facile scalability,and easy product ***,diacids can easily be derivatized to mainchain liquid crystalline polyesters.

关键词： Consecutive photo-induced electron transfer Visible-light catalysis Dicarboxylation Carbon dioxide Cyclopropanes

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