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Dense carbon nanofiber self-supporting electrode fabricated by orientation/compaction strategy for high volumetric lithium storage capacity

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Progress in Natural Science:Materials International 2025年第1期35卷 229-237页

作者： Haihui Liu Chaoqun Chen Qiang Xu Yan Song Xiangwu Zhang Chang Ma Tianjin Municipal Key Lab of Advanced Fiber and Energy Storage Technology Tiangong University CAS Key Laboratory of Carbon Materials Institute of Coal Chemistry Chinese Academy of Sciences Fiber and Polymer Science Program Department of Textile Engineering Chemistry and Science Wilson College of Textiles North Carolina State University

Low bulk density greatly restricts the large-scale application of electrospun carbon-based fiber membrane as electrode in energy storage devices. To solve the above challenges, herein an orientation-compaction densification strategy is proposed to enhance the bulk density and volumetric capacity of PAN-based carbon nanofiber membranes as self-supporting electrode used in lithium-ion batteries（LIBs）. Specifically, highly-oriented fibers are achieved by high-speed roller collecting during electrospinning, and compaction densification is conducted by hot-pressing treatment. The effects of collecting speed and hot-pressing pressure on the morphology, conductivity,bulk density, tensile strength, and flexibility of the obtained carbon nanofiber membrane are *** to conventional fiber membranes, of which fibers are disorderly stacked, the oriented fiber membrane is much easier to achieve dense stacking by compaction. The obtained dense carbon nanofiber membrane demonstrates a bulk density of 0.566 g cm-3, and shows a significantly-enhanced volumetric capacity(318.3 mA h cm-3), high-rate performance(86.6 mA h cm-3at 5 A g-1), and satisfactory cycling stability when used as selfsupporting electrode of LIBs.

关键词： Bulk density Densification Electrospinning Orientation-compaction Volumetric capacity

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Cellulose acetate nanofiber modified with polydopamine polymerized MOFs for efficient removal of noxious organic dyes

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Environmental Science and Pollution Research 2024年第20期31卷 29992-30008页

作者： Eze, Esther Omer, Ahmed M. Hassanin, Ahmed H. Eltaweil, Abdelazeem S. El-Khouly, Mohamed E. Nanoscience Program Institute of Basic and Applied Sciences Egypt-Japan University of Science and Technology New Borg El-Arab City Alexandria Egypt New Borg El-Arab City Alexandria Egypt Department of Textile Faculty of Engineering Alexandria University Alexandria Egypt Wilson College Textile North Carolina State University RaleighNC United States Department of Chemistry Faculty of Science Alexandria University Alexandria21934 Egypt Department of Engineering Faculty of Engineering and Technology University of Technology and Applied Sciences Muscat Oman

The need to effectively remove toxic organic dyes from aquatic systems has become an increasingly critical issue in the recent years. In pursuit of this objective, polydopamine (PDA)-binary ZIF-8/UiO-66 (MOFs) was synthesized and incorporated into cellulose acetate (CA), producing ZIF-8/UiO-66/PDA@CA composite nanofibers under meticulously optimized conditions. The potential of fabricated nanofibers to remove cationic methylene blue (MB) dye was investigated. Various analysis tools including FTIR, XRD, SEM, zeta potential, BET, tensile strength testing, and XPS were employed. Results revealed a substantial leap in tensile strength, with ZIF-8/UiO-66/PDA@CA registering an impressive 2.8 MPa, as a marked improvement over the neat CA nanofibers (1.1 MPa). ZIF-8/UiO-66/PDA@CA nanofibers exhibit an outstanding adsorption capacity of 82 mg/g, notably outperforming the 22.4 mg/g capacity of neat CA nanofibers. In binary dye systems, these nanofibers exhibit a striking maximum adsorption capacity of 108 mg/g, establishing their eminence in addressing the complexities of wastewater treatment. Furthermore, the adsorption data fitted to the Langmuir isotherm, and the pseudo-second-order kinetic model. The fabricated nanofiber demonstrates good reproducibility and durability, consistently upholding its performance over five cycles. This suite of remarkable attributes collectively underscores its potential as a robust, durable, and highly promising solution for the effective and efficient removal of pernicious MB dye, in the context of both water quality improvement and environmental preservation. Graphical Abstract: (Figure presented.) © The Author(s), under exclusive licence to Springer-Verlag GmbH Germany, part of Springer Nature 2024.

关键词： Adsorption

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Coprecipitation Strategy for Halide-Based Solid-State Electrolytes and Atmospheric-Dependent In Situ Analysis

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ACS Applied Materials and Interfaces 2024年第21期16卷 27394-27399页

作者： Bilo, Josanelle Angela V. Chang, Chung-Kai Chuang, Yu-Chun Fang, Mu-Huai Research Center for Applied Sciences Academia Sinica Taipei11529 Taiwan Department of Engineering and System Science National Tsing Hua University Hsinchu30013 Taiwan Nano Science and Technology Program Taiwan International Graduate Program Academia Sinica and National Tsinghua University Hsinchu30013 Taiwan Department of Science and Technology Philippine Textile Research Institute Taguig City1631 Philippines National Synchrotron Radiation Research Center Hsinchu300 Taiwan

In the continuous pursuit of an energy-efficient alternative to the energy-intensive mechanochemical process, we developed a coprecipitation strategy for synthesizing halide-based solid-state electrolytes that warrant both structural control and commercial scalability. In this study, we propose a new coprecipitation approach to synthesized Li3InCl6, exhibiting both structural and electrochemical performance stability, with a high ionic conductivity of 1.42 × 10-3 S cm-1, comparable to that of traditionally prepared counterparts. Through the in situ synchrotron X-ray diffraction technique, we unveil the stability mechanisms and rapid chemical reactions of Li3InCl6 under dry Ar, dry O2, and high-humidity atmosphere, which were not previously reported. Furthermore, the fast reversibility capability of moisture-exposed Li3InCl6 was tracked under vacuum, revealing the optimal recovery conditions at low temperatures (150-200 °C). This work addresses the critical challenges in structural engineering and sustainable mass production and provides insights into chemical reactions under real-world conditions. © 2024 The Authors. Published by American Chemical Society.

关键词： Coprecipitation

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Evaluating mechanism of banana pseudo-stem retting using seawater:A cost-effective surface pre-treatment approach

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Journal of Bioresources and Bioproducts 2024年第3期9卷 322-335页

作者： Prince Hotor Ahmed H.Hassanin Osbert Akatwijuka Mohamed A.H.Gepreel Mitsuo Yamamoto Yukie Saito Ahmed Abdel-Mawgood Egypt-Japan University of Science and Technology Biotechnology ProgramAlexandria GovernorateNew Borg Al Arab 21934Egypt Alexandria University Department of Textile EngineeringAlexandria GovernorateBab Sharqi 5424041Egypt Egypt-Japan University of Science and Technology Material Science and EngineeringAlexandria GovernorateNew Borg Al Arab 21934Egypt Graduate School of Agricultural and Life Sciences The University of TokyoBunkyo-KuTokyo 113-8657Japan

Retting has been employed to extract natural fibers from agricultural wastes as a biological and cost-effective approach for *** its global abundance,banana pseudo-stem is a promising agro-waste for lignocellulosic fiber *** this study,fibers were extracted from the pseudo-stems after being pre-treated under four conditions using seawater at room temperature for up to 35 d Bacterial isolation from the fresh seawater sample and screening for ligninolytic ability were *** load as well as laccase and manganese peroxidase enzyme activity profile assay during the retting duration were *** transform infrared(FT-IR)and X-day diffraction(XRD)analyses were also examined for both pre-treated and untreated extracted *** results shows that six out of the eight bacterial isolates had the ability to degrade *** treatments(Raw stem+Raw seawater)and(Autoclaved stem+Raw seawater)recorded the highest viable bacterial load of 9.24×102 and 4.46×102 CFU,respectively,on the 14th day of the retting ***,the highest laccase and manganese peroxidase enzymes activity was recorded for(Raw stem+Raw seawater)and(Autoclaved stem+Raw seawater)treatments in the second to the third *** FT-IR spectra of the pre-treated fibers revealed relative reductions in peaks attributed to polysaccharides and other amorphous substances for all retting *** XRD diffractogram revealed that the crystallinity index(CI)of pre-treated fibers increased in all seawater retting treatment ***,the CI for fibers pre-treated under enzymatic conditions were enhanced even after five *** analysis for selected bacterial isolates showed homology to sequences of Bacillus velezensis,Shewanella sp.L8–5,and Citrobacter amalonaticus and Bacillus subtilis j8 *** these findings,it was suggested that physical,biological,and chemical actions were collectively involved in the seawater retting process of banana ps

关键词： Seawater retting Banana pseudo-stem Natural fiber Enzyme activity Colony forming unit

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A Review on Digital Simulation Strategies and Its Applications for Advanced Compression Garments 16

A Review on Digital Simulation Strategies and Its Applicatio...

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16th textile Bioengineering and Informatics Symposium, TBIS 2023

作者： Youn, Seonyoung Darden, Ryan Mathur, Kavita Fiber and Polymer Science Ph.D. Program North Carolina State University RaleighNC27606 United States Department of Textile Engineering Chemistry and Sciences M.S. Textile Engineering Program North Carolina State University RaleighNC27606 United States Department of Textile and Apparel Technology and Management North Carolina State University RaleighNC27606 United States

ISBN: (纸本)9781713879473

This paper presents a comprehensive review on the current state of digital simulation technology and its strategic application usages with a key focus on advanced compression garments. Although three-dimensional (3D) digital garment simulators have significantly impacted the apparel and textile industry, their use has been limited to visual prototyping, quality checking, or marketing. The physical properties of garment simulators have been overlooked in advanced functional manufacturing. This literature review investigates the possibility of strategically utilizing virtual physical properties to enhance garment functions, specifically in wearables and medical-grade compression fields. The first phase of this paper gives an overview of the current state of 3D garment simulation tools and their measurement features. This is followed by a gap analysis between simulated and physical property evaluations, focusing on minimizing the gaps. The literature is thoroughly examined to identify appropriate studies that uses digital tools for compressional garments and add value to wearables and healthcare applications. This paper provides valuable insights for apparel and textile engineers, enabling them to better understand the limitations and capabilities of garment simulators in improving advanced features for specific end users. © TBIS 2023. All rights reserved.

关键词： Physical properties

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Nanofiber Materials for Lithium‑Ion Batteries

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Advanced Fiber Materials 2023年第4期5卷 1141-1197页

作者： Xinwang Cao Chang Ma Lei Luo Lei Chen Hui Cheng Raphael Simha Orenstein Xiangwu Zhang National Engineering Laboratory for Advanced Yarn and Fabric Formation and Clean Production College of Textiles Science and EngineeringWuhan Textile UniversityWuhan 430200China Tianjin Municipal Key Lab of Advanced Fiber and Energy Storage Technology Tiangong UniversityTianjin 300387China Fiber and Polymer Science Program Department of Textile EngineeringChemistry and ScienceWilson College of TextilesNorth Carolina State UniversityRaleighNC 27695USA

The lithium-ion(Li-ion)battery has received considerable attention in the field of energy conversion and storage due to its high energy density and *** academic and commercial progress has been made in Li-ion battery *** area of advancement has been the addition of nanofiber materials to Li-ion batteries due to their unique and desirable structural features including large aspect ratios,high surface areas,controllable chemical compositions,and abundant composite *** the past few decades,considerable research efforts have been devoted to constructing advanced nanofiber materials possessing conductive networks to facilitate efficient electron transport and large specific surface areas to support catalytically active sites,both for the purpose of boosting electrochemical ***,we focus on recent advancements of nanofiber materials with carefully designed structures and enhanced electrochemical properties for use in Li-ion *** synthesis,structure,and properties of nanofiber cathodes,anodes,separators,and electrolytes,and their applications in Li-ion batteries are *** research challenges and prospects of nanofiber materials in Li-ion battery applications are delineated.

关键词： Nanofiber Lithium-ion battery Cathode Anode Separator Electrolyte

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Two-dimensional MXenes:New frontier of wearable and flexible electronics

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InfoMat 2022年第4期4卷 1-28页

作者： Abbas Ahmed Sudeep Sharma Bapan Adak Md Milon Hossain Anna Marie LaChance Samrat Mukhopadhyay Luyi Sun Polymer Program Institute of Materials ScienceUniversity of ConnecticutStorrsConnecticutUSA Advanced Sensor and Energy Research(ASER)Lab Department of Electronic EngineeringKwangwoon UniversitySeoulSouth Korea Department of Textile and Fiber Engineering Indian Institute of TechnologyNew DelhiIndia Department of Textile Engineering Chemistry and ScienceNorth Carolina State UniversityRaleighNorth CarolinaUSA Department of Textile Engineering Khulna University of Engineering&TechnologyKhulnaBangladesh Department of Chemical and Biomolecular Engineering University of ConnecticutStorrsConnecticutUSA

Wearable electronics offer incredible benefits in mobile healthcare monitoring,sensing,portable energy harvesting and storage,human-machine interactions,etc.,due to the evolution of rigid electronics structure to flexible and stretchable ***,transition metal carbides and nitrides(MXenes)are highly regarded as a group of thriving two-dimensional nanomaterials and extraordinary building blocks for emerging flexible electronics platforms because of their excellent electrical conductivity,enriched surface functionalities,and large surface *** article reviews the most recent developments in MXene-enabled flexible electronics for wearable *** MXeneenabled electronic devices designed on a nanometric scale are highlighted by drawing attention to widely developed nonstructural attributes,including 3D configured devices,textile and planer substrates,bioinspired structures,and printed ***,the unique progress of these nanodevices is highlighted by representative applications in healthcare,energy,electromagnetic interference(EMI)shielding,and humanoid control of *** emerging prospects of MXene nanomaterials as a key frontier in nextgeneration wearable electronics are envisioned and the design challenges of these electronic systems are also discussed,followed by proposed solutions.

关键词： flexible electronics MXene nanostructures wearable electronics

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Edge atomic Fe sites decorated porous graphitic carbon as an efficient bifunctional oxygen catalyst for Zinc-air batteries

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Journal of Energy Chemistry 2023年第8期83卷 602-611,I0014页

作者： Ruihui Gan Yali Wang Xiangwu Zhang Yan Song Jingli Shi Chang Ma Tianjin Municipal Key Lab of Advanced Fiber and Energy Storage Technology Tiangong UniversityTianjin 300387China Fiber and Polymer Science Program Department of Textile EngineeringChemistry and ScienceWilson College of TextilesNorth Carolina State UniversityRaleighNC 27695-8301uNITED sTATES CAS Key Laboratory of Carbon Materials Institute of Coal ChemistryChinese Academy of SciencesTaiyuan 030001ShanxiChina

The development of advanced bifunctional oxygen electrocatalysts for oxygen reduction and evolution reactions(ORR and OER) is critical to the practical application of zinc-air batteries(ZABs). Herein, a silica-assisted method is reported to integrate numerous accessible edge Fe-Nx sites into porous graphitic carbon(named Fe-N-G) for achieving highly active and robust oxygen electrocatalysis. Silica facilitates the formation of edge Fe-Nx sites and dense graphitic domains in carbon by inhibiting iron *** purification process creates a well-developed mass transfer channel for Fe-N-G. Consequently,Fe-N-G delivers a half-wave potential of 0.859 V in ORR and an overpotential of 344 m V at10 m A cm^(-2)in OER. During long-term operation, the graphitic layers protect edge Fe-Nx sites from demetallation in ORR and synergize with Fe OOH species endowing Fe-N-G with enhanced OER *** functional theory calculations reveal that the edge Fe-Nx site is superior to the in-plane Fe-Nx site in terms of OH* dissociation in ORR and OOH* formation in OER. The constructed ZAB based on Fe-N-G cathode shows a higher peak power density of 133 m W cm^(-2)and more stable cycling performance than Pt/C + RuO2counterparts. This work provides a novel strategy to obtain high-efficiency bifunctional oxygen electrocatalysts through space mediation.

关键词： Bifunctionality EdgeFe-Nxsites Oxygen catalysis Graphitic domains Zinc-air batteries

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A Review on Digital Simulation Strategies and Its Applications for Advanced Compression Garments

A Review on Digital Simulation Strategies and Its Applicatio...

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作者： Seonyoung Youn Ryan Darden Kavita Mathur Fiber and Polymer Science Ph.D.program North Carolina State University Department of Textile Engineering Chemistry and Sciences M.S.Textile Engineering program North Carolina State University Department of Textile and Apparel Technology and Management North Carolina State University

This paper presents a comprehensive review on the current state of digital simulation technology and its strategic application usages with a key focus on advanced compression garments. Although three-dimensional(3D) digital garment simulators have significantly impacted the apparel and textile industry, their use has been limited to visual prototyping, quality checking, or marketing. The physical properties of garment simulators have been overlooked in advanced functional manufacturing. This literature review investigates the possibility of strategically utilizing virtual physical properties to enhance garment functions, specifically in wearables and medical-grade compression fields. The first phase of this paper gives an overview of the current state of 3D garment simulation tools and their measurement features. This is followed by a gap analysis between simulated and physical property evaluations, focusing on minimizing the gaps. The literature is thoroughly examined to identify appropriate studies that uses digital tools for compressional garments and add value to wearables and healthcare applications. This paper provides valuable insights for apparel and textile engineers, enabling them to better understand the limitations and capabilities of garment simulators in improving advanced features for specific end users.

关键词： 3D Digital Garment Simulator Advanced Compression Garment Digital Strategy Medical-grade Compression Simulated Physical Property Virtual Evaluation

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Highly Thermally Stable, Highly Electrolyte-Wettable Hydroxyapatite/Cellulose Nanofiber Hybrid Separators for Lithium-Ion Batteries

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ACS Applied Energy Materials 2023年第7期6卷 3862-3871页

作者： Liu, Yi Li, Chunxing Li, Chao Liang, Zhenye Hu, Xueshan Liu, Hao Zhang, Ze Cui, Meng Chen, Gang Wan, Jiayu Zhang, Xiangwu Tao, Jinsong State Key Lab of Pulp and Paper Engineering South China University of Technology Guangzhou510640 China SUSTech Energy Institute for Carbon Neutrality Southern University of Science and Technology Shenzhen518055 China Department of Mechanical and Energy Engineering Southern University of Science and Technology Shenzhen518055 China Fiber and Polymer Science Program Department of Textile Engineering Chemistry and Science Wilson College of Textiles North Carolina State University RaleighNC27695-8301 United States

Separators have an important influence on the safety and performance of lithium-ion batteries (LIBs). However, traditional polyolefin-based separators suffer from poor thermal stability and weak electrolyte wettability. Here, by using hydroxyapatite (HAP) and cellulose nanofibers (CNFs) as raw materials, we fabricated a unique HAP/CNF hybrid separator. The separators exhibit excellent thermal properties, with high thermal stability (up to 250 °C) and outstanding flame retardancy. The separators also demonstrate excellent electrolyte wettability. Compared to polypropylene (PP) separators, the HAP/CNF separators show a smaller contact angle with electrolytes, 17.2° for HAP/CNF and 45.5° for PP. Meanwhile, the HAP/CNF separators illustrate an excellent smoothness of 68.0 nm. In addition, the batteries assembled with the hybrid separators display a better performance compared with the batteries assembled with commercial PP separators. The raw materials are green, and the fabrication processes are free of organic solvents. We envision that the HAP/CNF hybrid separator could be a promising separator candidate for next-generation high-safety and high-performance LIBs. © 2023 American Chemical Society.

关键词： Thermodynamic stability

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