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Synthesis of novel high-entropy diborides with high-efficiency electromagnetic wave absorption and excellent thermal stability

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Journal of advanced Ceramics 2025年第2期14卷 185-197页

作者： Chencheng Liu Qingyun Chen Peng Sun Xingye Wang Shuyi Zeng Qijie Chen Tong Zhu Yi Zhu Wenlong Zhang Hui Song Yuezhong Wang Kazuhito Nishimura Huasong Liu Nan Jiang College of Physics and Electronic Information Engineering Guilin University of TechnologyGuilin 541004China State Key Laboratory of Advanced Marine Materials Ningbo Institute of Materials Technology and EngineeringChinese Academy of SciencesNingbo 315201China Tianjin Key Laboratory of Optical Thin Films Tianjin Jinhang Technical Physics InstituteTianjin 300308China

Ceramic materials have obvious advantages in thermal stability,but impedance mismatch limits their ability to attenuate electromagnetic(EM)***,a novel series of high-entropy(V_(0.2)Nb_(0.2)Zr_(0.2)Ta_(0.2)X_(0.2))B_(2)(X=Mo,Ti,and Hf)ceramics were successfully synthesized via ultrafast high-temperature sintering(UHS)apparatus based on joule *** results indicated that the effect of high-entropy component on the magnetic loss of the system was relatively small,but the effect on the dielectric loss was *** them,the(V_(0.2)Nb_(0.2)Zr_(0.2)Ta_(0.2)Ti_(0.2))B_(2)(HEB-Ti)sample demonstrated superior absorbing properties due to relatively moderate dielectric loss and optimal EM impedance ***,because of its relatively moderate attenuation constant,it could achieve the maximum penetration of the EM wave and the minimum reflection after absorbing *** a result,the minimum reflection loss(RL_(min))was as low as−40.7 dB,and the effective absorption band covered the entire low-frequency range from 2 to 8 *** excellent absorption performance was mainly due to the synergistic effect of various dielectric attenuation mechanisms,including defect polarization,dipole polarization,and conduction ***,thermogravimetric(TG)analysis showed that the sample exhibited excellent thermal stability and could withstand temperatures up to 550℃in air and 1000℃in an argon gas *** relevant work could provide meaningful references for the design of new high-performance ceramic wave-absorbing materials.

关键词： high-entropy diborides(HEBs) ultrafast high-temperature sintering(UHS) electromagnetic(EM)wave absorption impedance matching

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Improving aircraft nose wheel steering stability based on control continuation method

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Science China(Technological Sciences) 2025年第3期68卷 258-277页

作者： Qiaozhi YIN Dexu KONG Jiawei WANG Hong NIE Xiaohui WEI National Key Laboratory of Helicopter Aeromechanics Nanjing210016China State Key Laboratory of Mechanics and Control for Aerospace Structures Nanjing210016China Key Laboratory of Fundamental Science for National Defense-Advanced Design Technology of Flight Vehicle Nanjing210016China AVIC Nanjing Engineering Institute of Aircraft Systems Nanjing211106China

Aircraft steering instability during the taxiing process sometimes occurs resulting from the unstable bifurcation phenomena of the nonlinear steering dynamic system,which may lead to severe *** this study,the control parameter design of an aircraft nose wheel steering control system based on the control continuation method is proposed to reduce the number of unstable bifurcation points and enlarge the system stable region area in a certain parameter ***,the aircraft turning performance can be improved ***,a nonlinear aircraft rollout dynamic model is constructed,and the aircraft ground steering bifurcation characteristics are obtained under the open-loop steering control ***,the bifurcation performances under three closed-loop nose wheel steering controllers based on the feedback control method are compared,and the control parameter of the quadratic nonlinear controller with a better bifurcation control effect is selected as a second bifurcation parameter to analyze the directional system stability via two-parameter bifurcation ***,the influence of a crosswind on the aircraft ground steering bifurcation performance is studied for various control parameter ***,the control effects of a traditional proportional-integral-derivative(PID)nose wheel steering control law and the designed feedback controller are compared and ***,a semi-physical experiment of the aircraft nose wheel steering system is carried out,and different control parameter values are selected for test verification,which can further verify the control effect of the designed nonlinear feedback *** results indicate that the feedback control method is unable to vary the system bifurcation types,but appropriate control parameter design can effectively shrink the system instability region and even eliminate the unstable Hopf bifurcation points under some specific working conditions,improving the aircraft ground turning stability re

关键词： aircraft taxiing dynamics and stability nose wheel steering control system control continuation steering bifurcation characteristics quadratic feedback control

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The superior ballistic performance of highly stretchable and flexible double-face knitted fabrics(DFKF):An experimental investigation

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Defence technology(防务技术) 2025年第3期45卷 119-136页

作者： Yi Zhou Xiangpeng Xin Yang Li Yang Zhou Rui Zhang Lizhi Xu State Key Laboratory of New Textile Materials and Advanced Processing Technologies Wuhan Textile UniversityWuhan 430200China School of Mechanical Engineering Nanjing University of Science and TechnologyNanjing 210094China

When the protective and protected systems are detached,the former can be allowed to absorb the kinetic energy of the impacting projectile through large deformation without considering the back face signature of the *** paper presents a novel double-face knitted fabric(DFKF)designed for this very impacting *** tests equipped with high-speed camera were used to characterize the ballistic performance with the impact velocities ranging from 100 m/s to 450 m/*** results showed that the ballistic limits(V_(bl))of DFKF are approximately triple and double that of its counterpart UD and plain fabrics,*** mass-normalized metrics,the specific energy absorption(SEA)is 250%and 350%greater than the UD and plain fabrics at their corresponding V_(bl)*** quasi-static tests showed that the DFKF displayed greater resilience,crease recovery properties,and flexibility,which also made it an especially better candidate than UD and plain weaves for the design of umbrella surface *** was also found that DFKF is dependent on yarn count and the incorporation of spandex.A prototype anti-ballistic umbrella is manufactured using DFKF made of 200D multi-filament *** ballistic performance is also sensitive to the impact site when the umbrella is subjected to impact.

关键词： DFKF Ballistic performance SEA Resilience Energy absorption Anti-ballistic umbrella

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The impact of the coupling relationship between projectile size and yarn dimension on the ballistic performance of plain weave fabric

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Defence technology(防务技术) 2025年第1期43卷 288-303页

作者： Kaiying Wang Xuan Zhou Wenke Ren Yiding Wu Yilei Yu Yi Zhou Lizhi Xu Guangfa Gao School of Mechanical Engineering Nanjing University of Science and TechnologyNanjing210094China State Key Laboratory of New Textile Materials and Advanced Processing Technologies Wuhan Textile UniversityWuhan430079China

Aramid fibers,due to their relatively high inter-yarn friction,high strength,high modulus,and other characteristics,have become a typical representative of flexible anti-ballistic materials in modern *** research on the anti-penetration of aramid fabrics mostly focuses unilaterally on the structure and performance of aramid fabrics or the shape and size of projectiles,with fewer studies on the coupled effect of both on ballistic *** study analyzes how the coupling relationship(or size effect)between the projectile and fiber bundle dimensions affects the fabric ballistic performance from a mesoscopic scale *** plain weave aramid fabric as the research object,considering different diameter projectiles,through a large number of ballistic impact tests and numerical simulations,parameters such as ballistic limit velocity,average energy absorption of fabric,and specific energy absorption ratio(average energy absorption of fabric divided by projectile cross-sectional area)are obtained for ballistic performance *** influence law of projectile size on the ballistic performance of high-performance fabrics is as follows:The relative range of fitted ballistic limit velocity at different target positions gradually decreases and then stabilizes as the projectile diameter increases,indicating that the fabric structure effect gradually disappears at a projectile diameter of 12 mm;The average ballistic limit velocity at three impact positions,P1,P2,and P3,provides the corresponding ballistic limit velocity for 1000D aramid fabric,which increases with projectile diameter but the rate of increase slows down at an inflection point,which in this study occurs where the fabric structure effect nearly disappears at a projectile diameter of 12 mm;The energy absorption ratio increases and then decreases as the projectile diameter increases from 4 mm to 20 mm,reaching a peak at the diameter of 12 mm due to the gradual disappearance of the fabri

关键词： Plain weave fabric Ballistic performance Aramid fiber Projectile size Ballistic experiment

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Thermal strain engineering in cobalt-coordinated Mo2N for efficient ampere-level current density alkaline fresh/seawater hydrogen evolution electrocatalysis

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Journal of Energy Chemistry 2025年第4期103卷 282-293页

作者： Yuwen Hu Meilian Tu Tuzhi Xiong Yanxiang He Muhammad Mushtaq Hao Yang Zeba Khanam Yongchao Huang Jianqiu Deng M.-Sadeeq Balogun College of Materials Science and Engineering Hunan Joint International Laboratory of Advanced Materials and Technology for Clean Energy Hunan University School of Chemistry and Chemical Engineering University of South China School of Chemistry & Chemical Engineering Guangxi Key Laboratory of Electrochemical Energy Materials Guangxi Colleges and Universities Key Laboratory of Applied Chemistry Technology and Resource Development Guangxi University Institute of Environmental Research at Greater Bay Key Laboratory for Water Quality and Conservation of the Pearl River Delta Ministry of Education Guangzhou University Guangxi Key Laboratory of Information Materials Guilin University of Electronic Technology State Key Laboratory of Non-Food Biomass and Enzyme Technology Guangxi Academy of Sciences

Lattice-strain engineering has demonstrated its capability to influence the electronic structure and catalytic performance of ***,we present a facile method for inducing thermal strain in cobalt/molybdenum nitride rod-shaped structures（denoted Co/Mo2N） via ammonia-assisted reduction,which effectively modulating the HER *** optimized Co/Mo2N-500,characterized by 3% tensile lattice strain,demonstrates exceptional HER activity with lower overpotentials of140 mV and 184 mV at high current density of 1000 mA cm-2in alkaline freshwater and seawater electrolytes,***/Mo2N also exhibits excellent long-term durability even at a high current density of 300 mA cm-2,surpassing its counterparts and benchmark Pt/C *** functional theory calculations validate that the tensile strain optimizes the d-band states,water dissociation,and hydrogen adsorption kinetics of the strained Mo2N in Co/Mo2N,thereby improving its catalytic *** work provides valuable insights into controlling lattice strain to develop highly efficient electrocatalysts towards advanced electrocatalytic applications.

关键词： Ampere-level current density Co/Mo2N Hydrogen evolution reaction Seawater splitting Thermal strain engineering

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Fast deposition of Ni doped YSZ coatings by cathode plasma electrolysis for solid oxide fuel cell applications

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Ceramics International 2025年第13期51卷 17268-17277页

作者： Liu, Chenxu Du, Ke Song, Chen Song, Yang Zhou, Chenchen Zhang, Jin Liu, Min Tian, Yu Meng, Yonggang State Key Laboratory of Tribology in Advanced Equipment Tsinghua University Beijing100084 China Institute of New Materials Guangdong Academy of Sciences National Engineering Laboratory of Modern Materials Surface Engineering Technology Guangdong Provincial Key Laboratory of Modern Surface Engineering Technology Guangdong-Hong Kong Joint Laboratory of Modern Surface Engineering Technology Guangzhou510650 China School of Materials Science and Engineering Nanyang Technological University 639798 Singapore Beijing Key Laboratory for Corrosion Erosion and Surface Technology Institute of Advanced Materials and Technology University of Science and Technology Beijing Beijing100083 China

The fast fabrication of high-quality anode layers of solid oxide fuel cells (SOFCs) is a key factor for their efficient applications. In this work, a one-step method of cathode plasma electrolytic deposition (CPED) is developed to prepare Ni doped YSZ coatings with a thickness of 35–55 μm on porous stainless steel. Compared to the several hours required by traditional methods, a faster coating deposition that only takes 60 s is achieved owing to the effect of enormous energy of plasma arc at the solid-liquid interface in the CPED method. The preparation process is analyzed by recording the variation of current with voltage. The unique micro-structure of the coatings is observed, and the formation mechanism of the Ni doped YSZ coating during the CPED process is proposed. The deposited coatings show an excellent performance as the anode layers for SOFCs, with Sc2O3 stabilized ZrO2 coating prepared by atmospheric plasma spraying as electrolyte and La0.6Sr0.4Co0.2Fe0.8O3-δ as the cathode. The open circuit voltage of the cells reaches 1.000 V and the maximum power density reaches 817.4 mW cm−2 at 800 °C. The finding opens a novel pathway for the efficient preparation of anode materials for SOFCs. © 2025

关键词： Plasma spraying

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Decentralized Federated Learning Algorithm Under Adversary Eavesdropping

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IEEE/CAA Journal of Automatica Sinica 2025年第2期12卷 448-456页

作者： Lei Xu Danya Xu Xinlei Yi Chao Deng Tianyou Chai Tao Yang the State Key Laboratory of Synthetical Automation for Process Industries Northeastern University the Department of Mechanical Engineering University of Victoria Shanghai Institute of Intelligent Science and Technology Tongji University IEEE the Institute of Advanced Technology Nanjing University of Posts and Telecommunications

In this paper, we study the decentralized federated learning problem, which involves the collaborative training of a global model among multiple devices while ensuring data *** classical federated learning, the communication channel between the devices poses a potential risk of compromising private information. To reduce the risk of adversary eavesdropping in the communication channel, we propose TRADE(transmit difference weight) concept. This concept replaces the decentralized federated learning algorithm's transmitted weight parameters with differential weight parameters, enhancing the privacy data against eavesdropping. Subsequently, by integrating the TRADE concept with the primal-dual stochastic gradient descent(SGD)algorithm, we propose a decentralized TRADE primal-dual SGD algorithm. We demonstrate that our proposed algorithm's convergence properties are the same as those of the primal-dual SGD algorithm while providing enhanced privacy protection. We validate the algorithm's performance on fault diagnosis task using the Case Western Reserve University dataset, and image classification tasks using the CIFAR-10 and CIFAR-100 datasets,revealing model accuracy comparable to centralized federated learning. Additionally, the experiments confirm the algorithm's privacy protection capability.

关键词： Adversary eavesdropping decentralized federated learning privacy protection stochastic gradient descent

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Surrogate-Assisted Multiobjective Gene Selection for Cell Classification from Large-Scale Single-Cell RNA Sequencing Data

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IEEE Transactions on Evolutionary Computation 2025年第3期29卷 601-615页

作者： Lin, Jianqing He, Cheng Jiang, Hanjing Huang, Yabing Jin, Yaochu Huazhong University of Science and Technology Key Laboratory of Image Information Processing and Intelligent Control of Education Ministry of China School of Artificial Intelligence and Automation Wuhan430074 China Huazhong University of Science and Technology State Key Laboratory of Advanced Electromagnetic Technology School of Electrical and Electronic Engineering Wuhan430074 China Renmin Hospital Department of Pathology Wuhan University Wuhan430060 China Westlake University Trustworth and General Artificial Intelligence Laboratory School of Engineering Hangzhou310030 China

Accurate cell classification is crucial but expensive for large-scale single-cell RNA sequencing (scRNA-seq) analysis. Gene selection (GS) emerges as a pivotal technique in identifying gene subsets of scRNA-seq for classification accuracy improvement and gene scale reduction. Nevertheless, the rising scale of scRNA-seq data presents challenges to existing GS methods regarding performance and computational time. Thus, we propose a surrogate-assisted evolutionary algorithm for multiobjective GS to address these deficiencies. An innovative two-phase initialization method is proposed to select sparse solutions to provide preliminary insights into gene contributions. Then, a binary competitive swarm optimizer is proposed for effective global search, where a local search method is embedded to eliminate irrelevant genes for efficiency consideration. Additionally, a surrogate model is adopted to forecast classification accuracy efficiently and substitutes part of the computationally expensive classification process. Experiments are conducted on eight large-scale scRNA-seq datasets with more than 20,000 genes. The effectiveness of the proposed GS method for scRNA-seq cell classification compared with eight state-of-the-art methods is validated. Gene expression analysis results of selected genes further validated the significance of the genes selected by the proposed method in the classification of scRNA-seq data. © 1997-2012 IEEE.

关键词： Gene expression

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Niobium oxide/MXene heterostructure for simultaneous production of ammonia and energy via rechargeable Zn-N2 battery system

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Journal of Energy Chemistry 2025年第4期103卷 448-457页

作者： Xinyu Dai Wei Zhang Ying Sun Zhenyi Du Zhanliang Tao Jingang Wang Wenhui Fang Xuehan Xing Yang Chen Hui Li Hao Zheng Jieshan Qiu Tianyi Ma Institute of Clean Energy Chemistry Key Laboratory for Green Synthesis and Preparative Chemistry of Advanced Materials of Liaoning Province College of ChemistryLiaoning University State Key Laboratory of Clean and Efficient Coal Utilization Taiyuan University of Technology Key Laboratory of Advanced Energy Materials Chemistry (Ministry of Education) Renewable Energy Conversion and Storage Center College of Chemistry Nankai University College of Science Liaoning Petrochemical University College of Chemical Engineering State Key Laboratory of Chemical Resource Engineering Beijing University of Chemical Technology Centre for Atomaterials and Nanomanufacturing (CAN) School of Science RMIT University ARC Industrial Transformation Research Hub for Intelligent Energy Efficiency in Future Protected Cropping (E2Crop) College of Chemical State Key Laboratory of Chemical Resource Engineering Beijing University of Chemical Technology

Aqueous Zn-N2batteries with unique configuration are of potential for simultaneous N2electro reduction and electricity generation,in which the electrocatalysts are critical for improving the NH3yield and the energy ***,a heterostructure Nb2O5/Nb2CTXwith abundant exposed Nb active sites and tuned electron density has been synthesized by in situ formation and anchoring of Nb2O5nanoparticles on the surface of Nb2CTXMXene,which shows an enhanced N2adsorption/activation *** heterostructure Nb2O5/Nb2CTXwas used as the cathode of Zn-N2battery that can deliver a peak power density of 1.25 mW cm-2in 1.0 M KOH and can continuously produce NH3with a yield of3.62 μg *** NH3formed in the battery system can be easily collected as a net product without circulating the ***,the Nb2O5/Nb2CTXhas a long durability,evidenced by 70 h of operation at-0.4 V *** hydrogen electrode,which is the highest among the MXene-based electrocatalysts reported thus *** work may provide a new methodology based on Zn-N2battery for sustainable and large-scale NH3production with minimal energy consumption.

关键词： NH 3 production Zn-N 2 battery N 2 Electroreduction Nb 2 O 5 /Nb 2 CT X heterostructure

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Nonflammable electrolyte with weak-solvation structure for stable NCM811 cathode under high temperature

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Journal of Energy Chemistry 2025年第5期104卷 111-117页

作者： Dawei Xu Chao Yang Ailing Yang Xiaowei Liu Meilong Wang Jin Han Tiefeng Liu Ya You State Key Laboratory of Advanced Technology for Materials Synthesis and Processing Wuhan University of Technology International School of Materials Science and Engineering School of Materials Science and Microelectronics Wuhan University of Technology College of Chemical and Biological Engineering Zhejiang University Quzhou Institute of Power Battery and Grid Energy Storage

High-nickel cathode LiNi0.8Co0.1Mn0.1O2（NCM811） could enable lithium-ion batteries （LIBs） with high energy ***,excessive decomposition of the electrolyte would happen in the high operating voltage *** addition,the utilization of flammable organic solvents would increase safety risks in the high temperature ***,an electrolyte consisting of flame-retardant solvents with lower highest occupied molecular orbital （HOMO） level and LiDFOB salt is proposed to address above two *** a result,a thin and robust cathode-electrolyte interface containing rich LiF and Li-B-O compounds is formed on the cathode to effectively suppress electrolyte decomposition in the high operating *** NCM811||Li cell paired with this designed electrolyte possesses a capacity retention of 72% after 300 cycles at 55℃.This work provides insights into developing electrolyte for stable high-nickel cathode operated in the high temperature.

关键词： Electrolyte engineering High temperature High-nickel cathode Safety Weak solvation

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