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Double-Cable Conjugated Polymers with Pendent Near-Infrared Electron Acceptors for Single-Component Organic Solar Cells

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Angewandte Chemie 2022年第35期134卷

作者： Shijie Liang Baiqiao Liu Dr. Safakath Karuthedath Jing Wang Dr. Yakun He Wen Liang Tan Hao Li Prof. Yunhua Xu Prof. Ning Li Prof. Jianhui Hou Prof. Zheng Tang Prof. Frédéric Laquai Prof. Christopher R. McNeill Prof. Christoph J. Brabec Prof. Weiwei Li Beijing Advanced Innovation Center for Soft Matter Science and Engineering & State Key Laboratory of Organic-Inorganic Composites Beijing University of Chemical Technology Beijing 100029 China Contribution: Data curation (lead) Formal analysis (lead) Investigation (equal) Writing - original draft (supporting) Writing - review & editing (supporting) Department of Chemistry School of Science Beijing Jiaotong University Beijing 100044 P. R. China KAUST Solar Center (KSC) Physical Sciences and Engineering Division (PSE) Material Science and Engineering Program (MSE) King Abdullah University of Science and Technology (KAUST) Thuwal 23955-6900 Kingdom of Saudi Arabia Contribution: Data curation (supporting) Formal analysis (supporting) Investigation (supporting) Writing - original draft (supporting) Writing - review & editing (supporting) Center for Advanced Low-dimension Materials College of Materials Science and Engineering Donghua University Shanghai 201620 P. R. China Contribution: Data curation (supporting) Formal analysis (supporting) Investigation (supporting) Methodology (supporting) Writing - review & editing (supporting) Institute of Materials for Electronics and Energy Technology (i-MEET) Friedrich-Alexander-Universität Erlangen-Nürnberg Martensstrasse 7 91058 Erlangen Germany Contribution: Data curation (supporting) Formal analysis (supporting) Investigation (supporting) Methodology (supporting) Writing - original draft (supporting) Writing - review & editing (supporting) Department of Materials Science and Engineering Monash University Wellington Road Clayton Victoria 3800 Australia State Key Laboratory of Polymer Physics and Chemistry Beijing National Laboratory for Molecular Sciences Institute of Chemistry Chinese Academy of Sciences Beijing 100190 P. R. China Contribution: Data curation (supporting) Formal analysis (supporting) Writing - review & editing (supporting) Contribution: Funding acquisition (supporting) Writing - review & editing (supportin

Double-cable conjugated polymers with near-infrared (NIR) electron acceptors are synthesized for use in single-component organic solar cells (SCOSCs). Through the development of a judicious synthetic pathway, the highly sensitive nature of the 2-(3-oxo-2,3-dihydroinden-1-ylidene)malononitrile (IC)-based electron acceptors in basic and protonic solvents is overcome. In addition, an asymmetric design motif is adopted to optimize the packing of donor and acceptor segments, enhancing charge separation efficiency. As such, the new double-cable polymers are successfully applied in SCOSCs, providing an efficiency of over 10 % with a broad photo response from 300 to 850 nm and exhibiting excellent thermal/light stability. These results demonstrate the powerful design of NIR-acceptor-based double-cable polymers and will enable SCOSCs to enter a new stage.

关键词： Double-Cable Conjugated Polymers Electron Acceptors Near Infrared Single Component Solar Cells

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A Charge-Switchable Zwitterionic Peptide for Rapid Detection of SARS-CoV-2 Main Protease

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Angewandte Chemie 2021年第9期134卷

作者： Dr. Zhicheng Jin Yash Mantri Dr. Maurice Retout Dr. Yong Cheng Dr. Jiajing Zhou Alec Jorns Dr. Pavla Fajtova Wonjun Yim Colman Moore Dr. Ming Xu Matthew N. Creyer Raina M. Borum Dr. Jingcheng Zhou Zhuohong Wu Tengyu He Prof. William F. Penny Prof. Anthony J. O'Donoghue Prof. Jesse V. Jokerst Department of NanoEngineering University of California San Diego 9500 Gilman Drive La Jolla CA 92093 USA Department of Bioengineering University of California San Diego 9500 Gilman Drive La Jolla California 92093 USA Skaggs School of Pharmacy and Pharmaceutical Sciences University of California San Diego 9500 Gilman Drive La Jolla California 92093 USA Materials Science and Engineering Program University of California San Diego 9500 Gilman Drive La Jolla California 92093 USA Department of Medicine University of California San Diego 9500 Gilman Drive La Jolla California 92093 USA Department of Radiology University of California San Diego 9500 Gilman Drive La Jolla California 92093 USA

The transmission of SARS-CoV-2 coronavirus has led to the COVID-19 pandemic. Nucleic acid testing while specific has limitations for mass surveillance. One alternative is the main protease (M pro ) due to its functional importance in mediating the viral life cycle. Here, we describe a combination of modular substrate and gold colloids to detect M pro via visual readout. The strategy involves zwitterionic peptide that carries opposite charges at the C-/N-terminus to exploit the specific recognition by M pro . Autolytic cleavage releases a positively charged moiety that assembles the nanoparticles with rapid color changes ( t <10 min). We determine a limit of detection for M pro in breath condensate matrices <10 nM. We further assayed ten COVID-negative subjects and found no false-positive result. In the light of simplicity, our test for viral protease is not limited to an equipped laboratory, but also is amenable to integrating as portable point-of-care devices including those on face-coverings.

关键词： Colorimetric analysis Covid-19 mpro/3clpro/nsp5 Smart mask Zwitterionic peptide

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Degradation of Bioresorbable Mg-4Zn-1Sr Intramedullary Pins and Associated Biological Responses in Vitro and in Vivo

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ACS APPLIED materialS & INTERFACES 2017年第51期9卷 44332-44355页

作者： Cipriano, Aaron F. Lin, Jiajia Lin, Alan Sallee, Amy Le, Belinda Alcaraz, Mayra Celene Cortez Guan, Ren-Guo Botimer, Gary Inceoglu, Serkan Liu, Huinan [†] Department of Bioengineering University of California Riverside California 92521 United States[‡] Materials Science & Engineering University of California Riverside California 92521 United States[§] School of Materials Science and Engineering Northeastern University Shenyang 110819 China[∥] Department of Orthopedic Surgery Loma Linda University Loma Linda California 92354 United States[⊥] Stem Cell Center University of California Riverside California 92521 United States[#] Cell Molecular and Developmental Biology Program University of California Riverside California 92521 United States

This article reports the degradation and biological properties of as-drawn Mg-4Zn-1Sr (designated as ZSr41) and pure Mg (P-Mg) wires as bioresorbable intramedullary pins for bone repair. Specifically, their cytocompatibility with bone marrow derived mesenchymal stem cells (BMSCs) and degradation in vitro, and their biological effects on peri-implant tissues and in vivo degradation in rat tibiae were studied. The as-drawn ZSr41 pins showed a significantly faster degradation than P-Mg in vitro and in vivo. The in vivo average daily degradation rates of both ZSr41 and P-Mg intramedullary pins were significantly greater than their respective in vitro degradation rates, likely because the intramedullary site of implantation is highly vascularized for removal of degradation products. Importantly, the concentrations of Mg2+, Zn2+, and Sr2+ ions in the BMSC culture in vitro and their concentrations in rat blood in vivo were all lower than their respective therapeutic dosages, i.e., in a safe range. Despite of rapid degradation with a complete resorption time of 8 weeks in vivo, the ZSr41 intramedullary pins showed a significant net bone growth because of stimulatory effects of the metallic ions released. However, proportionally released OH- ions and hydrogen gas caused adverse effects on bone marrow cells and resulted in cavities in surrounding bone. Thus, properly engineering the degradation properties of Mg-based implants is critical for harvesting the bioactivities of beneficial metallic ions, while controlling adverse reactions associated with the release of OH- ions and hydrogen gas. It is necessary to further optimize the alloy processing conditions and/or modify the surfaces, for example, applying coatings onto the surface, to reduce the degradation rate of ZSr41 wires for skeletal implant applications.

关键词： biodegradable magnesium zinc strontium (Mg-Zn-Sr) alloy bioresorbable intramedullary pin implant in rat tibia biodegradation in vitro and in vivo cytocompatibility and biocompatibility bone remodeling microcomputed tomography (micro CT or mu CT)

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A Participant-Derived Xenograft Model of HIV Enables Long-Term Evaluation of Autologous Immunotherapies

SSRN

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SSRN 2020年

作者： McCann, Chase D. van Dorp, Christiaan H. Ward, Adam R. Danesh, Ali Dilling, Thomas R. Mota, Talia M. Zale, Elizabeth Patel, Shabnum Brumme, Chanson J. Dong, Winnie Jones, Douglas S. Andresen, Thomas L. Walker, Bruce D. Brumme, Zabrina L. Bollard, Catherine M. Perelson, Alan S. Irvine, Darrell J. Jones, R. Brad Weill Cornell Medicine Belfer Research Building Room 550 413 E 69th Street New YorkNY10021 United States Infectious Diseases Division Department of Medicine Weill Cornell Medical College New YorkNY United States Immunology & Microbial Pathogenesis Graduate Program Weill Cornell Graduate School of Medical Sciences New YorkNY United States Los Alamos National Laboratory Los AlamosNM United States Department of Microbiology Immunology & Tropical Medicine The George Washington University School of Medicine and Health Sciences WashingtonDC United States Milken Institute School of Public Health The George Washington University WashingtonDC United States Center for Cancer and Immunology Research Children’s National Health System WashingtonDC United States GW Cancer Center George Washington University WashingtonDC United States British Columbia Centre for Excellence in HIV/AIDS VancouverBC Canada Repertoire Immune Medicines CambridgeMA United States Ragon Institute of Massachusetts General Hospital MIT & Harvard University BostonMA United States Institute for Medical and Engineering Sciences MIT CambridgeMA United States Howard Hughes Medical Institute Chevy ChaseMD United States Faculty of Health Sciences Simon Fraser University BurnabyBC Canada Department of Material Science and Engineering MIT CambridgeMA United States Koch Institute for Integrative Cancer Research MIT CambridgeMA United States Department of Biological Engineering MIT CambridgeMA United States

HIV-specific CD8 + T-cells partially control viral replication and delay disease progression, but rarely provide lasting protection – largely due to immune escape. We show that engrafting mice with memory CD4+ T-cells from HIV + donors uniquely allows for the in vivo evaluation of autologous T-cell responses, while avoiding graft-versus-host disease and the need for human fetal tissues that limit other models. Treating HIV-infected mice with clinically-relevant HIV-specific T-cell products resulted in substantial reductions in viremia, which were augmented by engineering with IL-15 superagonist-containing nanogels. Ultimately, in vivo activity was limited by the selection of diverse escape mutations, recapitulating patterns seen in humans. By applying mathematical modeling, we show that the kinetics of the CD8 + T-cell response have a profound impact on the emergence and persistence of escape mutations. This ‘participant-derived xenograft’ model of HIV provides a powerful tool for studying HIV-specific immunological responses and facilitating the development of effective cell-based therapies. © 2020, The Authors. All rights reserved.

关键词： T-cells

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Multifunctional stimuli responsive polymer-gated iron and gold-embedded silica nano golf balls:Nanoshuttles for targeted on-demand theranostics

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Bone Research 2017年第4期5卷 343-356页

作者： Liping Wang Grace Jang Deependra Kumar Ban Vrinda Sant Jay Seth Sami Kazmi Nirav Patel Qingqing Yang Joon Lee Woraphong Janetanakit Shanshan Wang Brian P Head Gennadi Glinsky Ratneshwar Lai School of Biomedical Engineering Shanghai Jiaotong UniverityShanghaiChina Department of Mechanical and Aerospace Engineering La JollaCAUSA Materials Science and Engineering Program La JollaCAUSA Department of Nanoengineering La JollaCAUSA Department of Chemical Engineering University of California San DiegoLa JollaCAUSA Departrnenf of Bioengineering La JollaCAUSA Department of Anesthesiology La JollaCAUSA Veterans Affairs San Diego Healthcare System San DiegoCAUSA Institute of Engineering in Medicine La JollaCAUSA

Multi-functional nanoshuttles for remotely targeted and on-demand delivery of therapeutic molecules and imaging to defined tissues and organs hold great potentials in personalized medicine, including precise early diagnosis, efficient prevention and therapy without toxicity. Yet, in spite of 25 years of research, there are still no such shuttles available. To this end, we have designed magnetic and gold nanoparticles （NP）-embedded silica nanoshuttles （MGNSs） with nanopores on their surface. Fluorescently labeled Doxombicin （DOX）, a cancer drug, was loaded in the MGNSs as a payload. DOX loaded MGNSs were encapsulated in heat and pH sensitive polymer P（NIPAM-co- MAA） to enable controlled release of the payload. Magnetically-guided transport of MGNSs was examined in：（a） a glass capillary tube to simulate their delivery via blood vessels; and （b） porous hydrogels to simulate their transport in composite human tissues, including bone, cartilage, tendon, muscles and blood-brain barrier {BBB）. The viscoelastic properties of hydrogels were examined by atomic force microscopy （AFM）. Cellular uptake of DOX- loaded MGNSs and the subsequent pH and temperature-mediated release were demonstrated in differentiated human neurons derived from induced pluripotent stem cells （iPSCs） as well as epithelial HeLa cells. The presence of embedded iron and gold NPs in silica shells and polymer-coating are supported by SEM and TEM. Fluorescence spectroscopy and microscopy documented DOX loading in the MGNSs. Time-dependent transport of MGNSs guided by an external magnetic field was observed in both glass capillary tubes and in the porous hydrogel. AFM results affirmed that the stiffness of the hydrogels model the rigidity range from soft tissues to bone. pH and temperature-dependent drug release analysis showed stimuli responsive and gradual drug release. Cells＇ viability MTT assays showed that MGNSs are non-toxic. The cell death from on-demand DOX release was observed in both neurons and ep

关键词： Multifunctional stimuli responsive polymer-gated iron

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Morphology and filtration performances of polyether sulfone membrane modified with carbon and Fe2O3

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IOP Conference Series: materials science and engineering 2020年第1期845卷

作者： R. Arisandi A Fathurrahman A. Fahrina F Razi Z Jalil N Arahman Department of Chemical Engineering Universitas Syiah Kuala Banda Aceh 23111 Indonesia Magister Program of Chemical Engineering Department of Chemical Engineering Universitas Syiah Kuala Banda Aceh 23111 Indonesia Doctor of Engineering Graduate School of Engineering Universitas Syiah Kuala Banda Aceh 23111 Indonesia Material Physics Laboratory Department of Physics Faculty of Mathematics and Natural Science SyiahKuala University Banda Aceh Indonesia Graduate School of Environmental Management Universitas Syiah Kuala Jl. Tgk Chik Pante Kulu No. 5 Darussalam Banda Aceh 23111 Indonesia Research center for environmental and natural resources Universitas Syiah Kuala Jl. Hamzah Fansuri No. 4 Darussalam Banda Aceh 23111 Indonesia Atsiri Research Center Universitas Syiah Kuala Banda Aceh 23111 Indonesia

Membrane separation technology has been widely applied in various industrial sectors. Some modification on membrane composition and structure is conducted to improve membrane filtration performance and mitigate fouling phenomena. Fouling on membrane surfaces lead to decrease permeabilty, increase energy consumtion, and shorten membrane life time. The aim of this study is to manufacture PES membrane which involved inorganic additives consits of Carbon and Fe2O3 particles to mitigate fouling tendency. All of membranes were prepared using phase inversion method with dissolving PES polymer into dimethyl formamide (DMF). The result membranes were characterized using Scanning Electron Microscopy (SEM) to investigate morphological structure and breaking strength to determine mechanical property. Membrane filtration performance were tested using soy protein solution in cross-flow system. The results showed that the addition of inorganic particles in PES membrane caused the increasing of pores which lead to increase pure water flux from 15.14 L/m2.h to 58.67 L/m2.h. Fouling mitigation test towards soy protein also showed that carbon and Fe2O3 particles enhanced membrane flux recovery ratio from 64.5 to 76%. Furthermore, the inorganic particles presence in PES membrane also improved the tensile strength of membrane up to 128 Mpa.

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Signatures of electronic nematicity in (111) LaAlO3/SrTiO3 interfaces

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Physical Review B 2018年第4期97卷 041408(R)-041408(R)页

作者： S. Davis Z. Huang K. Han Ariando T. Venkatesan V. Chandrasekhar Graduate Program in Applied Physics and Department of Physics and Astronomy Northwestern University 2145 Sheridan Road Evanston Illinois 60208 USA NUSNNI-Nanocore National University of Singapore 117411 Singapore Department of Physics National University of Singapore 117551 Singapore NUS Graduate School for Integrative Sciences & Engineering National University of Singapore 117456 Singapore Department of Electrical and Computer Engineering National University of Singapore 117576 Singapore Department of Material Science and Engineering National University of Singapore 117575 Singapore

The two-dimensional conducting gas (2DCG) that forms at the interface between LaAlO3 (LAO) and SrTiO3 (STO) has been widely studied due to the multitude of in situ tunable phenomena that exist at the interface. Recently it has been shown that nearly every property of the 2DEG that forms at the interface of (111) oriented LAO/STO is strongly anisotropic with respect to the in-plane crystal direction. This in-plane rotational symmetry breaking points to the existence of an electronic nematic phase at the interface that can be modified by an in situ electrostatic back-gate potential. Here we show that the onset temperature of the anisotropy in the longitudinal resistance is T≈22K, which does not match up with any known structural transition, and coincides with the onset of anisotropy in the Hall response of the system. Furthermore, below 22 K, charge transport is activated in nature with different activation energies along the two in-plane crystal directions. Such a response implies that the band edges along the two directions are different and provides further evidence of an electronic nematic state at the interface.

关键词： Electrical properties Hall effect Nematic order Transport phenomena Hall bar Resistivity measurements Transport techniques

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Room-temperature relaxor ferroelectricity and photovoltaic effects in tin titanate directly deposited on a silicon substrate

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Physical Review B 2018年第5期97卷 054109-054109页

作者： Radhe Agarwal Yogesh Sharma Siliang Chang Krishna C. Pitike Changhee Sohn Serge M. Nakhmanson Christos G. Takoudis Ho Nyung Lee Rachel Tonelli Jonathan Gardner James F. Scott Ram S. Katiyar Seungbum Hong Department of Physics and Institute for Functional Nanomaterials University of Puerto Rico San Juan Puerto Rico 00931 USA Material Science Division Argonne National Laboratory Lemont Illinois 60439 USA Oak Ridge National Laboratory Oak Ridge Tennessee 37831 USA Department of Chemical Engineering University of Illinois at Chicago Chicago Illinois 60607 USA Department of Materials Science and Engineering Institute of Materials Science University of Connecticut Storrs Connecticut 06269 USA Department of Bioengineering University of Illinois at Chicago Chicago Illinois 60607 USA School of Chemistry University of St. Andrews St. Andrews KY16 9ST United Kingdom School of Physics and Astronomy University of St. Andrews St. Andrews KY16 9SS United Kingdom Department of Materials Science and Engineering KAIST Daejeon 34141 Republic of Korea

Tin titanate (SnTiO3) has been notoriously impossible to prepare as a thin-film ferroelectric, probably because high-temperature annealing converts much of the Sn2+ to Sn4+. In the present paper, we show two things: first, perovskite phase SnTiO3 can be prepared by atomic-layer deposition directly onto p-type Si substrates; and second, these films exhibit ferroelectric switching at room temperature, with p-type Si acting as electrodes. X-ray diffraction measurements reveal that the film is single-phase, preferred-orientation ferroelectric perovskite SnTiO3. Our films showed well-saturated, square, and repeatable hysteresis loops of around 3μC/cm2 remnant polarization at room temperature, as detected by out-of-plane polarization versus electric field and field cycling measurements. Furthermore, photovoltaic and photoferroelectricity were found in Pt/SnTiO3/Si/SnTiO3/Pt heterostructures, the properties of which can be tuned through band-gap engineering by strain according to first-principles calculations. This is a lead-free room-temperature ferroelectric oxide of potential device application.

关键词： Band gap Density of states Dielectric properties Ferroelectricity Relaxor ferroelectrics

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Anisotropic superconductivity and frozen electronic states at the (111) LaAlO3/SrTiO3 interface

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Physical Review B 2018年第2期98卷 024504-024504页

作者： S. Davis Z. Huang K. Han Ariando T. Venkatesan V. Chandrasekhar Graduate Program in Applied Physics and Department of Physics and Astronomy Northwestern University 2145 Sheridan Road Evanston Illinois 60208 USA NUSNNI-Nanocore National University of Singapore 117411 Singapore Department of Physics National University of Singapore 117551 Singapore NUS Graduate School for Integrative Sciences & Engineering National University of Singapore 117456 Singapore Department of Physics National University of Singapore 117542 Singapore Department of Electrical and Computer Engineering National University of Singapore 117576 Singapore Department of Material Science and Engineering National University of Singapore 117575 Singapore

We report measurements of the superconducting properties of the two-dimensional (2D) gas that forms at the interface between LaAlO3 (LAO) and SrTiO3 (STO) in the (111) crystal orientation, a system that permits in situ tuning of carrier density and disorder by means of a back-gate voltage Vg. Like the (001) oriented LAO/STO interface, superconductivity at the (111) LAO/STO interface can be tuned by Vg. The 2D superconductivity in these (111) LAO/STO samples shows an in-plane anisotropy, being different along different interface crystal directions, and “remembers” the disorder landscape at which they are cooled through the superconducting transition. The low energy scale and other characteristics of this memory effect distinguish it from charge-trapping effects previously observed in (001) interface samples.

关键词： Electrical conductivity Impurities in superconductors Superconducting phase transition Superconductivity Interfaces Solid-solid interfaces Superconductors Two-dimensional electron gas Type-II superconductors Hall bar Resistivity measurements

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Author Correction: Enhancing untargeted metabolomics using metadata-based source annotation

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Nature biotechnology 2023年第11期41卷 1656页

作者： Julia M Gauglitz Kiana A West Wout Bittremieux Candace L Williams Kelly C Weldon Morgan Panitchpakdi Francesca Di Ottavio Christine M Aceves Elizabeth Brown Nicole C Sikora Alan K Jarmusch Cameron Martino Anupriya Tripathi Michael J Meehan Kathleen Dorrestein Justin P Shaffer Roxana Coras Fernando Vargas Lindsay DeRight Goldasich Tara Schwartz MacKenzie Bryant Gregory Humphrey Abigail J Johnson Katharina Spengler Pedro Belda-Ferre Edgar Diaz Daniel McDonald Qiyun Zhu Emmanuel O Elijah Mingxun Wang Clarisse Marotz Kate E Sprecher Daniela Vargas-Robles Dana Withrow Gail Ackermann Lourdes Herrera Barry J Bradford Lucas Maciel Mauriz Marques Juliano Geraldo Amaral Rodrigo Moreira Silva Flavio Protasio Veras Thiago Mattar Cunha Rene Donizeti Ribeiro Oliveira Paulo Louzada-Junior Robert H Mills Paulina K Piotrowski Stephanie L Servetas Sandra M Da Silva Christina M Jones Nancy J Lin Katrice A Lippa Scott A Jackson Rima Kaddurah Daouk Douglas Galasko Parambir S Dulai Tatyana I Kalashnikova Curt Wittenberg Robert Terkeltaub Megan M Doty Jae H Kim Kyung E Rhee Julia Beauchamp-Walters Kenneth P Wright Maria Gloria Dominguez-Bello Mark Manary Michelli F Oliveira Brigid S Boland Norberto Peporine Lopes Monica Guma Austin D Swafford Rachel J Dutton Rob Knight Pieter C Dorrestein Collaborative Mass Spectrometry Innovation Center University of California San Diego La Jolla CA USA. Skaggs School of Pharmacy and Pharmaceutical Sciences University of California San Diego La Jolla CA USA. Beckman Center for Conservation Research San Diego Zoo Wildlife Alliance Escondido CA USA. Center for Microbiome Innovation Joan and Irwin Jacobs School of Engineering University of California San Diego La Jolla CA USA. Division of Biological Sciences University of California San Diego La Jolla CA USA. Department of Pediatrics School of Medicine University of California San Diego La Jolla CA USA. Bioinformatics and Systems Biology Program University of California San Diego La Jolla CA USA. Division of Rheumatology Allergy & Immunology Department of Medicine University of California San Diego La Jolla CA USA. Division of Epidemiology and Community Health School of Public Health University of Minnesota Minneapolis MN USA. Department of Integrative Physiology University of Colorado Boulder Boulder CO USA. Department of Population Health Sciences University of Wisconsin-Madison Madison WI USA. Servicio Autónomo Centro Amazónico de Investigación y Control de Enfermedades Tropicales Simón Bolívar Puerto Ayacucho Amazonas Venezuela. Department of Pediatrics Billings Clinic Billings MT USA. Department of Animal Science Michigan State University East Lansing MI USA. Department of Pharmacology Ribeirão Preto Medicinal School Center of Research in Inflammatory Diseases University of São Paulo Ribeirão Preto Sao Paolo Brazil. Multidisciplinary Health Institute Federal University of Bahia Vitória da Conquista Bahia Brazil. NPPNS Department of Biomolecular Sciences School of Pharmaceutical Sciences of Ribeirão Preto University of São Paulo Ribeirão Preto Sao Paolo Brazil. Department of Internal Medicine Ribeirão Preto Medical School Center of Research in Inflammatory Diseases University of São Paulo Ribeirão Preto Sao Paolo Brazil. Department

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