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Stacking-fault networks with Lomer-Cottrell locks induced by carbon addition in a severely strained Cr-Co-Ni alloy

Journal of Alloys and Compounds 2025年 1033卷

作者： Guilherme Cardeal Stumpf Gustavo Bertoli Francisco Gil Coury Augusta Cerceau Isaac Neta Luciano Andrey Montoro Roberto Braga Figueiredo Witor Wolf Graduate Program in Metallurgical Materials and Minning Engineering Federal University of Minas Gerais Belo Horizonte MG 31270-901 Brazil Graduate Program in Materials Science and Engineering Federal University of São Carlos Rod. Washington Luiz Km 235 São Carlos SP 13565-905 Brazil Department of Materials Engineering Federal University of São Carlos São Carlos SP 13565-905 Brazil Department of Metallurgical and Materials Engineering Federal University of Minas Gerais Av. Antônio Carlos 6627 Belo Horizonte MG 31270-901 Brazil Department of Chemistry Federal University of Minas Gerais Av. Antônio Carlos 6627 Belo Horizonte MG 31270-901 Brazil Department of Materials Engineering São Carlos School of Engineering University of São Paulo (EESC–USP) São Carlos SP 13563-120 Brazil

Face-centered cubic (FCC) Cr-Co-Ni multi-principal element alloys are among the toughest materials ever designed. The optimal trade-off between strength and ductility shown by these materials is tied with their deformation evolution. Typically, their plastic deformation starts with dislocation slip, followed by mechanical twinning (i.e., twinning induced plasticity, TWIP) and, as strain levels further increase, phase transformation induced by plasticity (TRIP). This work evaluates the deformation substructure of a highly strained (achieved with high-pressure torsion) Cr 40 Co 30 Ni 30 (at%) alloy with and without carbon alloying. After processing, the carbon-free alloy developed a typical substructure observed in FCC Medium/High-entropy alloys at later stages of straining, characterized by the presence of nanotwins and HCP lamellae, resulting in a 5.9 GPa hardness. In contrast, carbon addition induced grain refinement and suppression of the TWIP and TRIP effects. Notably, the Cr 39.6 Co 30 Ni 30 C 0.4 alloy developed networks of stacking faults with partial dislocations and Lomer-Cottrell locks, which primarily contributed to a stronger hardening capability, resulting in an increased hardness of 7.3 ± 0.8 GPa, 22 % (1.3 GPa) higher than the base alloy. These findings have important implications for better understanding the deformation substructure evolution of FCC multi-principal element alloys and can pave the way forward in regard to the design approaches for carbon-alloying in these materials.

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Culture of mesenchymal stem cells in a collagen sponge to reduce the cell leak

Culture of mesenchymal stem cells in a collagen sponge to re...

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55th Society of Polymer science Japan Symposium on Macromolecules

作者： Kawazoe, Naoki Akahane, Daisuke Chen, Guoping Shirasaki, Yoshio Yamamoto, Katsuyuki Tateishi, Tetsuya Biomaterials Center National Institute for Materials Science Namiki 1-1 Tyukuba Ibaraki 305-0044 Division of Bioengineering and Bioinformatics Graduate School of Information Science and Technology Institute for Human and Science Biomedical Engineering Advanced Indusrial Science and Technology

Collagen sponges have been used in tissue engineering to provide three dimensional scaffolds. However, it was difficult to distribute cells uniformly throughout the scaffolds because the seeded cells leak from the scaffolds. Here we prepared a collagen scaffold surrounded by a 10 micrometer mesh to prevent cell leakage from the scaffold and seeded human mesenchymal stem cells onto the scaffold. From the results of the high seed efficiency, the collagen/mesh scaffold in this study was useful for a culture of mesenchymal stem cells.

关键词： Cell culture

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Study on chemotaxis and chemokinesis of bone marrow-derived mesenchymal stem cells in hydrogel-based 3D microfluidic devices

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biomaterials Research 2016年第1期20卷 1-8页

作者： Yoon, Dayoung Kim, Hyerim Lee, Eojin Park, Min Hee Chung, Seok Jeon, Hojeong Ahn, Cheol-Hee Lee, Kangwon Center for Biomaterials Korea Institute of Science and Technology Seoul South Korea Research Institute of Advanced Materials (RIAM) Department of Materials Science and Engineering Seou National University Seoul South Korea Program in Nanoscience and Technology Graduate School of Convergence Science and Technology Seou National University Seoul South Korea School of Mechanical Engineering Korea University Seoul South Korea Advanced Institutes of Convergence Technology Gyeonggi-do South Korea

Background: Controlling the fate of mesenchymal stems cells (MSCs) including proliferation, migration and differentiation has recently been studied by many researchers in the tissue engineering field. Especially, recruitment of stem cells to injury sites is the first and crucial step in tissue regeneration. Although significant progress has been made in the chemotactic migration of MSCs, MSC migration in three dimensional environments remains largely unknown. We developed a 3D hydrogel-based microfluidic-device to study the migration behavior of human MSCs in the presence of stromal-cell derived factor-1α (SDF-1α), interleukin 8 (IL-8) and Substance P (SP) which have been utilized as chemoattractant candidates of human mesenchymal stem cells (hMSCs). Results: We systematically investigated the chemotactic migration behaviors of hMSCs and their responses to SDF-1a, IL-8, and SP. SDF-1α was shown to be the most fascinating chemoattractant candidate among those factors at a certain time point. We also found that each chemokine showed different chemoattractant abilities according to their concentration. In the case of SP, this factor showed chemokinesis not chemotaxis. Especially at a 7-8×10^-8 M concentration range, the chemokinesis ability driven by SP was further increased. The data suggest that some factors at the optimal concentration exhibit chemokinesis or chemotaxis in a 3D hydrogel-based microfluidic device. Conclusion: In this study on chemotaxis and chemokinesis of hMSCs, the system parameters such as chemokine concentration, system stability, and 2D or 3D microenvironment are critically important to obtain meaningful results. © 2016 The Author(s).

关键词： Chemokinesis Chemotaxis Mesenchymal stem cells Microfluidic device

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Curved copper nanowires-based robust flexible transparent electrodes via all-solution approach

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Nano Research 2017年第9期10卷 3077-3091页

作者： Zhenxing Yin Seung Keun Song Sanghun Cho Duck-Jae You Jeeyoung Yoo Suk Tai Chang Youn Sang Kim Program in Nano Science and Technology Graduate School of Convergence Science and Technology Seoul National University Seoul 08826 Republic of Korea School of Chemical Engineering and Materials Science Chung-Ang University Seou106974 Republic of Korea Advanced Institutes of Convergence Technology 145 Gwanggyo-ro Yeongtong-gu Suwon-si Gyeonggi-do 16229 Republic of Korea

Curved Cu nanowire (CCN)-based high-performance flexible transparent conductive electrodes (FTCEs) were fabricated via a fully solution-processed approach, involving synthesis, coating, patterning, welding, and transfer. Each step involved an innovative technique for completing the all-solution processes. The high-quality and well-dispersed CCNs were synthesized using a multi-polyol method through the synergistic effect of specific polyol reduction. To precisely control the optoelectrical properties of the FTCEs, the CCNs were uniformly coated on a polyimide (PI) substrate via a simple meniscus-dragging deposition method by tuning several coating parameters. We also employed a polyurethane (PU)-stamped patterning method to effectively produce 20 μm patterns on CCN thin films. The CCN thin films exhibited high electrical performance, which is attributed to the deeply percolated CCN network formed via a solvent-dipped welding method. Finally, the CCN thin films on the PI substrate were partially embedded and transferred to the PU matrix to reduce their surface roughness. Through consecutive processes involving the proposed methods, a highly percolated CCN thin film on the PU matrix exhibited high optoelectrical performance (R s = 53.48 Ω/□ at T = 85.71%), excellent mechanical properties (R/R 0 < 1.10 after the 10th repetition of tape peeling or 1,000 bending cycles), and a low root-mean-square surface roughness (R rms = 14.36 nm).

关键词： curved Cu nanowires all-solution processes 20 μm patterns high performance transparent electrode

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Water viscosity and hydrodynamic flow in nanopillar chips

Water viscosity and hydrodynamic flow in nanopillar chips

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9th International Conference on Miniaturized Systems for Chemistry and Life sciences, MicroTAS 2005

作者： Kaji, N. Oki, A. Ogawa, R. Horiike, Y. Baba, Y. Department of Applied Chemistry Graduate School of Engineering Nagoya University Japan Biomaterials Center National Institute for Materials Science Japan Health Technology Research Center National Institute of Advanced Industrial Science and Technology Japan

ISBN: (纸本)0974361119

Here we report an anomalous behavior of water, especially viscosity and hydrodynamic flow, in nanopillar chips. These physicochemical properties of water were investigated by single-particle tracking (SPT) technique. The results of diffusion constants of nanospheres indicated that a higher viscosity and a less hydrodynamic flow in nanopillar chips compared with a bulk solution. Copyright © 2005 by the Transducer Research Foundation, Inc.

关键词： Hydrodynamics

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Microcellular Al2O3 ceramics from wood for filter applications

Microcellular Al2O3 ceramics from wood for filter applicatio...

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作者： Rambo, Carlos Renato Andrade, Tarcisio Fey, Tobias Sieber, Heino Martinelli, Antônio Eduardo Greil, Peter Materials Science and Engineering Graduate Program-PGMAT Chemical Engineering Department-EQA Federal University of Santa Catarina 88040-900 Florianópolis SC Brazil Materials Science and Engineering Graduate Program-PPGCEM UFRN-Federal University of Rio Grande Do Norte 59072-970 Natal RN Brazil Department of Materials Science Glass and Ceramics University of Erlangen-Nuremberg D-91058 Erlangen Germany American Ceramic Society

Microcellular biomorphous Al2O3 was produced by Al-vapor infiltration in pyrolyzed rattan and pine wood-derived biocarbon preforms. At 1600°C the biocarbon preforms reacted with gaseous aluminum to form Al4C3. After oxidation in air at temperatures between 1550° and 1650°C, for 3 h, the biocarbon preforms were fully converted into α-Al2O3. Owing to the high anisotropy of biomorphous Al2O3, the compressive strength behavior was strongly dependent on the loading direction. The compressive strength of the specimens (0.1-11 MPa) is strongly dependent on their overall porosity and their behavior could be explained using the Gibson-Ashby model. The Darcian permeability (k1), as well as the non-Darcian permeability (k 2), increased with an increase of the total porosity. The Darcian permeability of biomorphous Al2O3 was found to be in the range of 1-8 × 10-9 m2, which is in the order of magnitude of gas filters, and, therefore, suitable for several technological applications. © 2008 The American Ceramic Society.

关键词： Wood products

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Bioactive coatings by vaterite deposition on polymer substrates of different composition and morphology

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materials science and engineering C 2007年第4期27卷 741-745页

作者： Maeda, H. Maquet, V. Chen, Q.Z. Kasuga, T. Jawad, H. Boccaccini, A.R. Department of Materials Science and Engineering Graduate School of Engineering Nagoya Institute of Technology Gokiso-cho Showa-ku Nagoya 466-8555 Japan and Interfaculty Centre for Biomaterials University of Liege B-4000 Liege Belgium Department of Materials Imperial College London Prince Consort Road London SW7 2BP United Kingdom

Calcium carbonate particles of vaterite crystalline structure were deposited on the surface of polymer substrates of different chemistry and morphology by a slurry dipping technique using ethanol as a solvent. Artificial prosthetic fibrous ligaments (polyester-based) and poly(Ε-caprolactone) (PCL) 3-dimensional foams of high porosity were selected as model polymer substrates. The vaterite coated polymers were immersed in simulated body fluid to induce the formation of homogeneous hydroxycarbonate apatite (HCA) layers on the polymer surfaces, which were detected by SEM and XRD. The method offers great potential for inducing bioactive behaviour to normally bioinert polymers. In this investigation, fibrous structures for orthopaedic ligaments and 3-D porous tissue engineering scaffolds were considered and the application of the vaterite coating technique demonstrated. © 2006 Elsevier B.V. All rights reserved.

关键词： Biodegradable polymers

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Improving hydroxyapatite coating ability on biodegradable metal through laser-induced hydrothermal coating in liquid precursor:Application in orthopedic implants

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Bioactive materials 2023年第7期25卷 796-806页

作者： Jaeho Park Seung-Hoon Um Youngmin Seo Jaehong Lee Yu-Chan Kim Myoung-Ryul Ok Suk-Won Hwang Jeong-Yun Sun Hyung-Seop Han Hojeong Jeon Biomaterials Research Center Biomedical Research DivisionKorea Institute of Science and Technology(KIST)Seoul02792South Korea Department of Materials Science and Engineering Seoul National University(SNU)Seoul08826South Korea Division of Biomedical Science and Technology KIST SchoolKorea University of Science and TechnologySeoul02792South Korea KU-KIST Graduate School of Converging Science and Technology Korea UniversitySeoul02841South Korea

During the past decade,there has been extensive research toward the possibility of exploring magnesium and its alloys as biocompatible and biodegradable materials for implantable *** practical medical application,however,has been limited to specific areas owing to rapid corrosion in the initial stage and the consequent *** coatings can significantly reduce the initial corrosion of Mg alloys,and several studies have been carried out to improve the adhesion strength of the coating to the surfaces of the *** composition of hydroxyapatite(HAp)is very similar to that of bone tissue;it is one of the most commonly used coating materials for bone-related implants owing to favorable osseointegration *** this study,HAp was coated on Mg using nanosecond laser coating,combining the advantages of chemical and physical *** heat generated in the liquid precursor by the laser improved the adhesion of the coating through the precipitation and growth of HAp at the localized nanosecond laser focal area and increased the corrosion resistance and cell adhesion of *** physical,crystallographic,and chemical bondings were analyzed to explore the mechanism through which the surface adhesion between Mg and the HAp coating layer *** applicability of the coating to Mg screws used for clinical devices and improvement in its corrosion property were *** liquid environment-based laser surface coating technique offers a simple and quick process that does not require any chemical ligands,and therefore,overcomes a potential obstacle in its clinical use.

关键词： Biodegradable metal HAp coating Nanosecond laser Photothermal synthesis Soret effect(thermophoresis)

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A novel collagen sponge for cartilage tissue engineering

A novel collagen sponge for cartilage tissue engineering

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作者： Chen, Guoping Akahane, Daisuke Kawazoe, Naoki Shirasaki, Yoshio Tanaka, Junzo Yamamoto, Katsuyuki Tateishi, Tateishi Biomaterials Center National Institute for Materials Science 1-1 Namiki Tsukuba Japan Division of Bioengineering and Bioinformatics Graduate School of Information Science and Technology Hokkaido University Japan Institute for Human and Science Biomedical Engineering Advanced Industrial Science and Technology Japan Department of Metallurgy and Ceramics Science Graduate School of Science and Engineering Tokyo Institute of Technology Japan

A novel collagen sponge that can protect cell leakage during cell seeding was developed by wrapping all the surfaces except the upside of a collagen sponge with membrane that has pores smaller than cell. The collagen sponge was used for three-dimensional culture of human bone marrow-derived mesenchymal stem cells (MSCs). The cells adhered to the collagen, and proliferated to fill the spaces in the sponge. The cell seeding efficiency was higher than 95%. The MSCs cultured in the collagen sponge in the chondrogenic induction medium supplemented with TGF-3 and BMP6 expressed genes encoding type II collagen, SOX9 and aggrecan. HE staining indicated the round morphology of differentiated cells and the extracelluler matrices were positively stained by safranin O and toluidine blue. Type II collagen and cartilage proteoglycan were detected by immunostaining with anti-type II collagen and anti-cartilage proteoglycan. These results suggest the chondrogenic differentiation of MSCs. The collagen sponge facilitated cell seeding and chondrogenic differentiation of MSCs, and will be useful for cartilage tissue engineering.

关键词： Collagen

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Flexible cellulose-carbon nanotube paper substrate decorated with PZT: sensor properties

Flexible cellulose-carbon nanotube paper substrate decorated...

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MRS Advances

作者： Silva, Ricardo M. Noremberg, Bruno S. Marins, Natália H. Alano, Jose H. Santana, Luiza R. Valentini, Antoninho Lukowiec, Dariusz Tański, Tomasz Carreño, Neftalí L.V. Graduate Program in Materials Science and Engineering Technology Development Center Federal University of Pelotas PelotasRS96010-000 Brazil Federal University of Ceará Department of Analytical Chemistry and Chemical Physics FortalezaCE Brazil Institute of Engineering Materials and Biomaterials Silesian University of Technology Gliwice Poland Center for Nanotechnology Silesian University of Technology Gliwice Poland

Composite of PZT (lead zirconate titanate) and PLZT (lead lanthanum zirconate titanate) along an organic, renewable, conductive, and flexible matrix have been developed. The conductive paper was obtained through the reaction between the cellulose extracted from banana stem and functionalized MWCNT. This reaction was made in the presence of hydrogen (from H2SO4), which reduced the size of the cellulose by acid hydrolysis and promotes the interaction between its hydroxyls and the carboxyl groups of nanotubes. Afterward, the PZT particles were synthesized and grown up on the conductive paper by microwaves-assisted hydrothermal synthesis (MHS). The composite material was characterized by structure and morphology. Moreover, gas-sensing in the presence of methanol and electrical resistance as a function of temperature were also investigated. In this way, a simple, low-cost and successful synthesis was reported. Also, a promising flexible was obtained using a chemical transformation process from banana residue as source of cellulose. Copyright © materials Research Society 2018.

关键词： Cellulose

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