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Flexible electrochemical fiber sensor for intracranial nitric oxide monitoring

science China Chemistry 2024年第8期67卷 2431-2433页

作者： Ziwei Liu Huisheng Peng State Key Laboratory of Molecular Engineering of Polymers Department of Macromolecular ScienceInstitute of Fiber Materials and Devicesand Laboratory of Advanced MaterialsFudan UniversityShanghai 200438China

Real-time and accurate monitoring of vital biomarkers in vivo forms a crucial foundation for health assessment,early intervention,and disease ***,continuous monitoring of intracranial nitric oxide(NO)levels plays a pivotal role in promptly assessing immune responses,neurovirulence,and cerebrovascular diseases[1].Differing from non-real-time monitoring methods like chemiluminescence[2]and fluorescent probes[3],implantable electrochemical sensors excel in simultaneously high temporal resolution,sensitivity,and cost-effectiveness[4].

关键词： prompt electrochemical monitoring

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Deep insight of unique phase transition behaviors and mechanism in Zr_(2)Co-H isotope system with ultra-low equilibrium pressure

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Rare Metals 2024年第1期43卷 212-224页

作者： Yang Liu Pan-Pan Zhou Xue-Zhang Xiao Jia-Cheng Qi Jia-Peng Bi Tiao Ying Xing-Wen Feng Yan Shi Wen-Hua Luo Li-Xin Chen State Key Laboratory of Silicon Materials School of Materials Science and EngineeringZhejiang UniversityHangzhou 310027China Institute of Materials China Academy of Engineering PhysicsMianyang 621907China Key Laboratory of Advanced Materials and Applications for Batteries of Zhejiang Province Hangzhou 310013China

Efficient capture,safe storage and release of tritium from the international thermonuclear experimental reactor(ITER) reaction exhaust gas is a perplexing problem,and the development of an efficient tritium-getter material with ultra-low hydrogenation equilibrium pressure is considered as a reliable *** this work,Zr_(2)Co alloy was selected as a tritium-getter material and prepared through induction levitation *** performance test results show that Zr_(2)Co exhibits an ultra-low hydrogenation equilibrium pressure of 3.22 × 10^(-6) Pa at 25℃ and excellent hydriding kinetics under a low hydrogen pressure of 0.005 ***,unique phase transition behaviors were presented in Zr_(2)Co-H ***,Zr_(2)CoH_(5) formed by Zr_(2)Co hydrogenated at room temperature is initially decomposed into ZrH_(2) and ZrCoH_(3) at200 ℃.With the temperature increasing to 350 ℃,ZrCoH_(3)is dehydrogenated to ZrCo,and then ZrCo further reacts with ZrH_(2) at 650 ℃ to reform Zr_(2)Co and *** the staged phase transition pathways during dehydrogenation,the decomposition of Zr_(2)CoH_(5) occurs preferentially,which is well accordance with both the smallest reaction energy barrier and the maximum reaction spontaneity that are determined respectively from kinetics activation energy and thermodynamics Gibbs free ***,first principles calculation results indicate that the stronger binding of hydrogen in interstitial environments of ZrCoH_(3)and ZrH_(2) triggers the hydrogen-stabilized phase transformation of Zr_(2)CoH_(5).The unique phase transition mechanisms in Zr_(2)Co-H system can shed light on the further exploration and regulation of analogous staged phase transition of hydrogen storage materials.

关键词： Zr_(2)Co alloy Tritium-getter materials Ultralow equilibrium hydrogen pressure Phase transition mechanism

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Machine learning-based performance predictions for steels considering manufacturing process parameters:a review

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Journal of Iron and Steel Research International 2024年第7期31卷 1555-1581页

作者： Wei Fang Jia-xin Huang Tie-xu Peng Yang Long Fu-xing Yin Tianjin Key Laboratory of Materials Laminating Fabrication and Interface Control Technology School of Materials Science and EngineeringHebei University of TechnologyTianjin 300132China Institute of New Materials Guangdong Academy of ScienceGuangzhou 510651GuangdongChina

Steels are widely used as structural materials,making them essential for supporting our lives and ***,further improving the comprehensive properties of steel through traditional trial-and-error methods becomes challenging due to the continuous development and numerous processing parameters involved in steel *** address this challenge,the application of machine learning methods becomes crucial in establishing complex relationships between manufacturing processes and steel *** review begins with a general overview of machine learning methods and subsequently introduces various performance predictions in steel *** classification of performance pre-diction was used to assess the current application of machine learning model-assisted *** important issues,such as data source and characteristics,intermediate features,algorithm optimization,key feature analysis,and the role of environmental factors,were summarized and *** insights will be beneficial and enlightening to future research endeavors in this field.

关键词： Steel Manufacturing process Machine learning Performance prediction Algorithm

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Cooperative enhancement of mechanical and tribological properties through tailoring TiN transition interface in boron nitride nanosheets reinforced copper composites

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Rare Metals 2024年第10期43卷 5202-5215页

作者： Zhong-Hua Li Liang Liu Xin You Jian-Hong Yi Rui Bao Ming-Yi Zhu Song Lu Jun-Jun Pai Faculty of Materials Science and Engineering Kunming University of Science and TechnologyKunming 650093China Key Laboratory of Advanced Materials of Yunnan Province Kunming University of Science and TechnologyKunming 650093China

Strengthening interface bonding between boron nitride nanosheets(BNNS)and copper matrix is an essential prerequisite for exploiting a new generation of copper matrix composites(CMCs)with high strength and wear ***,BNNS/Cu composites were fabricated by the powder metallurgy route,matrix-alloying(adding 1.0 wt%Ti)strategy was adopted to improve the interfacial wettability and strengthen interface adhesion.A typical"sandwich"-like multiply interface structure involving TiN transition layers,BNNS and Cu matrix had been well constructed through the rational heat treatment(900℃ for 120 min).Additionally,nano-sized TiB whisker was in situ formed in the vicinity of the interface,it had linked the BNNS-Cu-TiN multiply interface,which played a role of"threading the needle"and significantly strengthened the multi-interfaces *** specific interface structure was finely characterized,and the formation mechanism of solid-state interfacial reaction feature was *** results demonstrated that the ultimate tensile strength(UTS)of BNNS/Cu-(Ti)-900℃ increased from 248 to 530 MPa(increased by 114%),and the coefficient of friction(COF)decreased from 0.51 to 0.28 than pure *** work highlights the importance of interface configuration design,which contributes to the development of CMCs with prominent comprehensive properties.

关键词： Copper matrix composites Boron nitride nanosheets interface structure Mechanical and frictional properties

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Investigating the Absorption and Desorption Behavior of Methylene Chloride in the Poly(aryl ether ketone) Film with Different Crystallinities

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Chinese Journal of Polymer science 2024年第2期42卷 239-246,I0009页

作者： Hong-Ru Yang Jin-Dong Zhang Dong-Ting Gao Gang Liu Chun-Hai Chen Jia-Nan Yao Center for Advanced Low-Dimension Materials State Key Laboratory for Modification of Chemical Fibers and Polymer MaterialsCollege of Materials Science and EngineeringDonghua UniversityShanghai201620China

Poly(aryl ether keton e)(PAEK) films with different crystallinities were obtained by controlling the cooling rate,which were subjected to the absorption and desorption of methylene chloride(CH_(2)Cl_(2)).We employed attenuated total reflection Fourier transform infrared(ATR-FTIR)spectroscopy analyses to investigate the diffusion behavior of CH_(2)Cl_(2) in PAEK films with different *** to the Fickian diffusion model,the calculated diffu sion coefficients of CH_(2)Cl_(2) in PAEK films were observed to decrease with increasing *** effect of CH_(2)Cl_(2)absorption and desorption on the mechanical properties of PAEK films with different crystallinity was further analyzed using tensile *** tensile tests exhibited that CH_(2)Cl_(2) has two concurrent effects:plasticization and solvent-induced *** scanning calorimetry(DSC) and wide-angle X-ray diffraction(WXRD) techniques further confirmed solvent-induced crystallization *** results would be beneficial to understand the solvent resistance of PAEK materials and consequently provide the practical application conditions of PAEK with a theoretical basis.

关键词： Poly(aryl ether ketone) Diffusion behavior Infrared spectra Solvent-induced crystallization Mechanical properties

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Atomic-scale insights of indium segregation and its suppression by GaAs insertion layer in InGaAs/AlGaAs multiple quantum wells

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Chinese Physics B 2023年第3期32卷 544-548页

作者：马淑芳李磊孔庆波徐阳刘青明张帅张西数韩斌仇伯仓许并社郝晓东 Materials Institute of Atomic and Molecular Science Shaanxi University of Science and TechnologyXi'an 710021China School of Materials Science and Engineering Shaanxi University of Science and TechnologyXi'an 710021China Key Laboratory of Interface Science and Engineering in Advanced Materials Taiyuan University of TechnologyTaiyuan 030024China

The In segregation and its suppression in InGaAs/AlGaAs quantum well are investigated by using high-resolution x-ray diffraction(XRD)and photoluminescence(PL),combined with the state-of-the-art aberration corrected scanning transmission electron microscopy(Cs-STEM)*** facility our study,we grow two multiple quantum wells(MQWs)samples,which are almost identical except that in sample B a thin GaAs layer is inserted in each of the InGaAs well and AlGaAs barrier layer comparing to pristine InGaAs/AlGaAs MQWs(sample A).Our study indeed shows the direct evidences that In segregation occurs in the InGaAs/AlGaAs interface,and the effect of the Ga As insertion layer on suppressing the segregation of In atoms is also demonstrated on the ***,the atomic-scale insights are provided to understand the segregation behavior of In atoms and to unravel the underlying mechanism of the effect of GaAs insertion layer on the improvement of crystallinity,interface roughness,and further an enhanced optical performance of InGaAs/AlGaAs QWs.

关键词： InGaAs/AlGaAs quantum well GaAs insertion layer In segregation scanning transmission electron microscopy

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Designing interstitial boron-doped tunnel-type vanadium dioxide cathode for enhancing zinc ion storage capability

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Carbon Energy 2023年第8期5卷 78-86页

作者： Shiwen Wang Hang Zhang Kang Zhao Wenqing Liu Nairui Luo Jianan Zhao Shide Wu Junwei Ding Shaoming Fang Fangyi Cheng Henan Provincial Key Laboratory of Surface&Interface Science College of Materials and Chemical EngineeringZhengzhou University of Light IndustryZhengzhouChina Key Laboratory of Advanced Energy Materials Chemistry(Ministry of Education) College of ChemistryNankai UniversityTianjinChina

Chemical doping is a powerful method to intrinsically tailor the electrochemical properties of electrode ***,an interstitial boron-doped tunnel-type VO_(2)(B)is constructed via a facile hydrothermal *** analysis techniques demonstrate that boron resides in the interstitial site of VO_(2)(B)and such interstitial doping can boost the zinc storage kinetics and structural stability of VO_(2)(B)cathode during ***,we found that the boron doping level has a saturation limit peculiarity as proved by the quantitative ***,the 2 at.%boron-doped VO_(2)(B)shows enhanced zinc ion storage performance with a high storage capacity of 281.7 mAh g^(-1) at 0.1 A g^(-1),excellent rate performance of 142.2 mAh g^(-1) at 20 A g^(-1),and long cycle stability up to 1000 cycles with the capacity retention of 133.3 mAh g^(-1) at 5 A g^(-1).Additionally,the successful preparation of the boron-doped tunneltype α-MnO_(2) further indicates that the interstitial boron doping approach is a general strategy,which supplies a new chance to design other types of functional electrode materials for multivalence batteries.

关键词： cathode interstitial boron doping tunnel-type VO_(2)(B) zinc ion battery

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Recent advances and perspectives in MXene-based cathodes for aqueous zinc-ion batteries

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International Journal of Minerals,Metallurgy and materials 2024年第7期31卷 1752-1765页

作者： Aiduo Wu Tianhao Wang Long Zhang Chen Chen Qiaomin Li Xuanhui Qu Yongchang Liu Beijing Advanced Innovation Center for Materials Genome Engineering Institute for Advanced Materials and TechnologyState Key Laboratory for Advanced Metals and MaterialsUniversity of Science and Technology BeijingBeijing 100083China School of Materials Science and Engineering University of Science and Technology BeijingBeijing 100083China School of Economics and Management University of Science and Technology BeijingBeijing 100083China

Aqueous zinc-ion batteries(AZIBs)show great potential for applications in grid-scale energy storage,given their intrinsic safety,cost effectiveness,environmental friendliness,and impressive electrochemical ***,strong electrostatic interactions exist between zinc ions and host materials,and they hinder the development of advanced cathode materials for efficient,rapid,and stable Zn-ion *** and their derivatives possess a large interlayer spacing,excellent hydrophilicity,outstanding electronic conductivity,and high redox *** materials are considered“rising star”cathode candidates for *** comprehensive review discusses recent advances in MXenes as AZIB cathodes from the perspectives of crystal structure,Zn-storage mechanism,surface modification,interlayer engineering,and conductive network design to elucidate the correlations among their composition,structure,and electrochemical *** work also outlines the remaining challenges faced by MXenes for aqueous Zn-ion storage,such as the urgent need for improved toxic preparation methods,exploration of potential novel MXene cathodes,and suppression of layered MXene restacking upon cycling,and introduces the prospects of MXene-based cathode materials for high-performance AZIBs.

关键词： aqueous zinc-ion batteries MXenes terminal groups interlayer engineering conductive network design

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Improving mechanical properties of Mg-Sn alloys by co-addition of Li and Al

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Progress in Natural science:materials International 2023年第3期33卷 355-363页

作者： Zhen Pan Hucheng Pan Yu Huang Zhihao Zeng Zhang-Zhi Shi Chubin Yang Yuping Ren Lu-Ning Wang Gaowu Qin Key Laboratory for Anisotropy and Texture of Materials (Ministry of Education) College of Materials Science and Engineering Northeastern University Beijing Advanced Innovation Center for Materials Genome Engineering Key Laboratory for Advanced Materials Processing of Ministry of Education School of Materials Science and Engineering University of Science and Technology Beijing Jiangxi Provincial Engineering Research Center for Magnesium Alloy Gannan Normal University

In this work, a novel low-alloyed Mg-Sn-Li-Al alloy with high-strength has been developed. The addition of ～1 wt% Li into the Mg-2Sn wt.% binary alloy can change the type of strengthening phases in Mg-2Sn-1Li sample(TL21),involving the formation of both Li2Mg Sn and Mg2Sn phases. The co-addition of ～1 wt% Al and ～1 wt% Li can further induce the higher density of both micron-sized phases and nano-precipitations in the Mg-2Sn-1Li-1Al sample(TLA211). The nano-precipitations can inhibit the grain growth, which thus lead to the fine grain size of ～1.38 μm in TLA211 sample, and ～1.59 μm in the TL21 sample. Besides, the profuse nano-phases would improve the yield strength via Orowan hardening effect. Consequently, the TL21 sample can exhibit the high yield strength of ～204 MPa, and elongation of ～6.6%. The TLA211 sample exhibits the much higher yield strength of～250 MPa, ultimate tensile strength of ～291 MPa, and also high elongation of ～9.0%. The high strength-ductility synergy, together with the low-Sn content, make the present Mg-Sn based alloy to be potential for the wider industrial applications.

关键词： Mg wrought alloy Nano-precipitations Strengthening Grain refinement Mechanical properties

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Effect of titanium on the wettability between Fe-P-Ti alloy and Al2O3 substrate

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Progress in Natural science:materials International 2024年第3期34卷 555-561页

作者： Rui Wang Shengjie Bai Xu Chen Likui Xie Zhiqiang Yu Yang Kang Yihong Li Yong Hu Zhiyue Shi Zhijie Yan School of Materials Science and Engineering North University of China Shanxi Key Laboratory of Advanced Metal Materials for Special Environments North University of China CISDI Engineering CO. LTD. School of Materials Science and Engineering Taiyuan University of Science and Technology

It is of significance that the wettability between the molten alloy and the Al2O3affects the inclusion removal,nozzle clogging and refractory erosion. In the present work, the wettability between the Al2O3substrate and Fe–P–Ti alloys with different Ti content was investigated by using the sessile droplets method. The interfacial characteristics were investigated by scanning electron microscope（SEM）. The contact angles between the sintered Al2O3substrate and Fe–P–Ti alloys with 0, 0.05, 0.10 and 0.15 wt% Ti are 100.1°, 97.3°, 94.5°and 90.5°,respectively. The oxidation of [Al] and [Ti] in the molten alloys leads to the formation of the oxides on the droplets. With the increase of Ti content in the Fe–P–Ti alloys, the formed oxides change from Al2O3to Ticontaining oxides. The reaction between [Ti] and Al2O3substrate in the interface results in the formation of Ti-containing oxides. The quantity of the interfacial oxides increases with the increase of Ti content in the *** a result, the synergetic effect of the formation of the interfacial products and the oxides on the surface of droplets leads to the decrease of the contact angles between the Al2O3substrate and Fe–P–Ti alloys due to the increase of Ti content.

关键词： Wettability Contact angle Interfacial reaction Fe–P–Ti alloys Al2O3 substrate

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