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Effect of lanthanum on microstructure of a nickel-based single crystal superalloy

China Foundry 2025年第1期22卷 55-64页

作者： Hong Gao Kai Guan Ren-jie Cui Jian-chao Qin Zi-han Zhao Zhao-hui Huang Science and Technology on Advanced High Temperature Structural Materials Laboratory Beijing Institute of Aeronautical MaterialsBeijing 100095China

To enhance the high-temperature oxidation resistance and mechanical properties of a secondgeneration nickel-based superalloy,various concentrations of lanthanum(La)ranging from 5.0×10^(-5)wt.%to 3.4×10^(-4)wt.%are added to the *** microstructure of the nickel-based single crystal superalloy with trace of La was examined by means of SEM,EDS and *** show the addition of La decreases the segregation of elements and increases the amount ofγ/γ′eutectics of the as-cast alloy,and in the interdendritic region,the growth of eutectics is accompanied by the growth of strip clusters composed of Ni_(5)La and Ni_(3)*** the La content in the alloy increases,the proportion of Ni_(5)La in the cluster *** heat treatment,incipient melting occurs in the cluster regions,leading to an increase in microporosity compared to the original as-cast ***,the heat treatment alters the shape of the clusters from a strip morphology to an elliptical one,and it changes their composition from Ni_(5)La and Ni_(3)Ta to a combination of Ni_(5)La,Ni_(3)Ta,and MC carbides.

关键词： single crystal superalloy lanthanum microstructure heat-treatment precipitate phase

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Multi-region calcium imaging in freely behaving mice with ultra-compact head-mounted fluorescence microscopes

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National science Review 2024年第1期11卷 161-173页

作者： Feng Xue Fei Li Ke-ming Zhang Lufeng Ding Yang Wang Xingtao Zhao Fang Xu Danke Zhang Mingzhai Sun Pak-Ming Lau Qingyuan Zhu Pengcheng Zhou Guo-Qiang Bi Department of Precision Machinery and Precision Instruments University of Science and Technology of China Hefei National Laboratory for Physical Sciences at the Microscale University of Science and Technology of China Interdisciplinary Center for Brain Information the Brain Cognition and Brain Disease Institute Shenzhen Institute of Advanced Technology Chinese Academy of Sciences Faculty of Life and Health Sciences Shenzhen Institutes of Advanced Technology Chinese Academy of Sciences School of Life Sciences University of Science and Technology of China Institute of Semiconductors Chinese Academy of Sciences Department of Modern Life Sciences and Biotecnology Xiongan Institute of Innovation Xiongan New Area Shenzhen-Hong Kong Institute of Brain Science-Shenzhen Fundamental Research Institutions Suzhou Institute for Advanced Research University of Science and Technology of China Institute of Artiflcial Intelligence Hefei Comprehensive National Science Center

To investigate the circuit-level neural mechanisms of behavior, simultaneous imaging of neuronal activity in multiple cortical and subcortical regions is highly desired. Miniature head-mounted microscopes offer the capability of calcium imaging in freely behaving animals. However, implanting multiple microscopes on a mouse brain remains challenging due to space constraints and the cumbersome weight of the ***, we present TINIscope, a Tightly Integrated Neuronal Imaging microscope optimized for electronic and opto-mechanical design. With its compact and lightweight design of 0.43 g, TINIscope enables unprecedented simultaneous imaging of behavior-relevant activity in up to four brain regions in ***-of-concept experiments with TINIscope recorded over 1000 neurons in four hippocampal subregions and revealed concurrent activity patterns spanning across these regions. Moreover, we explored potential multi-modal experimental designs by integrating additional modules for optogenetics, electrical stimulation or local field potential recordings. Overall, TINIscope represents a timely and indispensable tool for studying the brain-wide interregional coordination that underlies unrestrained behaviors.

关键词： miniature microscope multiple sites calcium imaging multimodal integration hippocampus

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Galerkin-based quasi-smooth manifold element(QSME)method for anisotropic heat conduction problems in composites with complex geometry

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Applied Mathematics and Mechanics(English Edition) 2024年第1期45卷 137-154页

作者： Pan WANG Xiangcheng HAN Weibin WEN Baolin WANG Jun LIANG School of Civil Engineering Central South UniversityChangsha 410083China Institute of Advanced Structure Technology Beijing Institute of TechnologyBeijing 100081China School of Science Harbin Institute of TechnologyShenzhen 518055Guangdong ProvinceChina

The accurate and efficient analysis of anisotropic heat conduction problems in complex composites is crucial for structural design and performance evaluation. Traditional numerical methods, such as the finite element method(FEM), often face a trade-off between calculation accuracy and efficiency. In this paper, we propose a quasi-smooth manifold element(QSME) method to address this challenge, and provide the accurate and efficient analysis of two-dimensional(2D) anisotropic heat conduction problems in composites with complex geometry. The QSME approach achieves high calculation precision by a high-order local approximation that ensures the first-order derivative *** results demonstrate that the QSME method is robust and stable, offering both high accuracy and efficiency in the heat conduction analysis. With the same degrees of freedom(DOFs), the QSME method can achieve at least an order of magnitude higher calculation accuracy than the traditional FEM. Additionally, under the same level of calculation error, the QSME method requires 10 times fewer DOFs than the traditional FEM. The versatility of the proposed QSME method extends beyond anisotropic heat conduction problems in complex composites. The proposed QSME method can also be applied to other problems, including fluid flows, mechanical analyses, and other multi-field coupled problems, providing accurate and efficient numerical simulations.

关键词： anisotropic heat conduction quasi-smooth manifold element(QSME) composite with complex geometry numerical simulation finite element method(FEM)

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Hyperreflective photonic crystals created by shearing colloidal dispersions at ultrahigh volume fraction

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Microsystems & Nanoengineering 2024年第1期10卷 161-173页

作者： Minji Kim Jong Bin Kim Shin-Hyun Kim Department of Chemical and Biomolecular Engineering Korea Advanced Institute of Science and Technology(KAIST)Daejeon 34141Republic of Korea

Colloidal crystallization serves as one of the most economic and scalable production methods for photonic ***,insufficient optical performance,nonuniformity and low reproducibility remain challenges for advanced high-value *** this study,we optimally formulate a photocurable dispersion of silica particles and apply shear flow to unify the orientation of the colloidal crystals,ensuring high optical performance and *** silica particles experience strong repulsion at ultrahigh volume fractions of 50%but demonstrate low mobility,leading to polycrystalline *** shear flow to the dispersions allows the silica particles to rearrange into larger crystalline domains with a unidirectional orientation along the *** shear-induced structural change produces absolute reflectivity at the stopband as high as 90%and a high transparency of 90%at off-resonant wavelengths with minimal diffusive ***,the strong interparticle repulsion ensures a uniform volume fraction of particles throughout the dispersion,reducing deviations in the optical *** intricately micropattern the photocurable dispersions using ***,the photonic films and patterns can be stacked to form multiple layers,displaying mixed structural colors and multiple reflectance peaks without sacrificing *** superior photonic materials hold promise for various optical applications,including optical components and anticounterfeiting patches.

关键词： properties. dispersion reflectivity

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14-Bit SAR ADC with on-Chip Digital Bubble Sorting Calibration technology

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Chinese Journal of Electronics 2025年第1期34卷 125-136页

作者： Hua Fan Zhuorui Chen Tongrui Xu Franco Maloberti Qi Wei Quanyuan Feng School of Integrated Circuit Science and Engineering(Exemplary School of Microelectronics) University of Electronic Science and Technology of China Shenzhen Institute for Advanced Study University of Electronic Science and Technology of China Chongqing Institute of Microelectronics Industry Technology University of Electronic Science and Technology of China Department of Electrical Computer and Biomedical Engineering University of Pavia Department of Precision Instrument Tsinghua University Institute of Microelectronics Southwest Jiaotong University

This article designs a 14-bit successive approximation register analog-to-digital converter（SAR ADC）.A novel digital bubble sorting calibration method is proposed and applied to eliminate the effect of capacitor mismatch on the linearity of the SAR ADC. To reduce the number of capacitors, a hybrid architecture of a high 8-bit binary-weighted capacitor array and a low 6-bit resistor array is adopted by the digital-to-analog（DAC）. The common-mode voltage VCM-based switching scheme is chosen to reduce the switching energy and area of the DAC. The time-domain comparator is employed to obtain lower power consumption. Sampling is performed through a gate voltage bootstrapped switch to reduce the nonlinear errors introduced when sampling the input signal. Moreover, the SAR logic and the whole calibration is totally implemented on-chip through digital integrated circuit（IC） tools such as design compiler, IC compiler, etc. Finally, a prototype is designed and implemented using 0.18 μm bipolar-complementary metal oxide semiconductor（CMOS）-double-diffused MOS 1.8 V CMOS technology. The measurement results show that the SAR ADC with on-chip bubble sorting calibration method achieves the signal-to-noise-and-distortion ratio of 69.75 dB and the spurious-free dynamic range of 83.77 dB.

关键词： Semiconductor device measurement Capacitors Linearity Switches Calibration System-on-chip Frequency measurement Time-domain analysis Sorting Signal to noise ratio

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Polyethylene Oxide-Based Composite Solid Electrolytes for Lithium Batteries:Current Progress,Low-Temperature and High-Voltage Limitations,and Prospects

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Electrochemical Energy Reviews 2024年第1期7卷 53-90页

作者： Xin Su Xiao-Pei Xu Zhao-Qi Ji Ji Wu Fei Ma Li-Zhen Fan Advanced Battery Technology Center School of New EnergyHarbin Institute of TechnologyWeihai 264209ShandongChina Advanced Battery Technology Center School of Marine Science and TechnologyHarbin Institute of TechnologyWeihai 264209ShandongChina Advanced Battery Technology Center School of Automotive EngineeringHarbin Institute of TechnologyWeihai 264209ShandongChina R&D Center Shanghai Shanshan Technology Co.Ltd.Shanghai 201209China Department of Chemistry and Biochemistry Georgia Southern UniversityStatesboro GA30460USA Beijing Advanced Innovation Center for Materials Genome Engineering University of Science and Technology BeijingBeijing 100083China

Lithium-ion batteries(LIBs)are considered to be one of the most promising power sources for mobile electronic products,portable power devices and vehicles due to their superior environmental friendliness,excellent energy density,negligible memory effect,good charge/discharge rates,stable cycling life,and efficient electrochemical energy conversion,which distinguish it from other power ***,the flammable and volatile organic solvents in carbonate-containing liquid electrolytes can leach,resulting in thermal runaway and interface reactions,thus significantly limiting its *** use of polymer solid electrolytes is an effective way to solve this safety issues,among which poly(ethylene oxide)(PEO)-based solid polymer electrolytes(SPEs)have attracted much attention because of their stable mechanical properties,ease of fabrication,excellent electrochemical and thermal ***,PEO-SPEs with their low room-temperature ionic conductivity,narrow electrochemical windows,poor interface stability,and uncontrollable growth of lithium dendrites cannot meet the demand for high energy density in future ***,this review firstly describes the ion transport mechanisms and challenges that are crucial for PEO-SPEs,and then provides a comprehensive review of current approaches to address the challenges,including novel and efficient lithium salts,additives,composite electrolytes,stable solid electrolyte interfaces,3-D lithium metals and alloys,cathode protection layers and multi-layer ***,future research directions are proposed for the stable operation of PEO-SPEs at room temperature and high voltage,which is imperative for the commercialization of safe and high energy density LIBs.

关键词： Solid polymer electrolytes Polyethylene oxide Ionic conductivity Electrochemical window Lithium-ions batteries Additives

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Direct high-resolution X-ray imaging exploiting pseudorandomness

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Light(science & Applications) 2023年第5期12卷 776-788页

作者： KyeoReh Lee Jun Lim Su Yong Lee YongKeun Park Department of Physics Korea Advanced Institute of Science and TechnologyDaejeon 34141Republic of Korea KAIST Institute for Health Science and Technology Korea Advanced Institute of Science and TechnologyDaejeon 34141Republic of Korea Pohang Accelerator Laboratory Pohang University of Science and TechnologyPohangKyungbuk 37637Republic of Korea Tomocube Inc Daejeon 34051Republic of Korea

Owing to its unique penetrating power and high-resolution capability,X-ray imaging has been an irreplaceable tool since its *** the significance,the resolution of X-ray imaging has largely been limited by the technical difficulties on X-ray lens *** lensless imaging methods have been proposed,but are yet relying on multiple measurements or additional constraints on measurements or *** we present coherent specklecorrelation imaging(CSI)using a designed X-ray *** has no prerequisites for samples or ***,from a single shot measurement,the complex sample field is retrieved based on the pseudorandomness of the speckle intensity pattern,ensured through a *** achieve a spatial resolution of 13.9 nm at 5.46 keV,beating the feature size of the diffuser used(300 nm).The high-resolution imaging capability is theoretically explained based on fundamental and practical *** expect the CSI to be a versatile tool for navigating the unexplored world of nanometer.

关键词： resolution speckle replace

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Effect of samarium on the N_(2) selectivity of Sm_(x)Mn_(0.3-x)Ti catalysts during selective catalytic reduction of NO_(x) with NH_(3)

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International Journal of Minerals,Metallurgy and Materials 2023年第4期30卷 642-652页

作者： Shengyang Zhang Bolin Zhang Boyu Wu Bo Liu Shengen Zhang Institute for Advanced Materials and Technology University of Science and Technology BeijingBeijing 100083China Shunde Innovation School University of Science and Technology BeijingFoshan 528399China

This work aims to study the improvement effect of Sm on Mn-based catalysts for selective catalytic reduction (SCR) of NO with NH3.A series of Sm_(x)Mn_(0.3-x)-xTi catalysts (x=0,0.1,0.15,0.2,and 0.3) were prepared by *** tests indicated that the Sm_(0.15)Mn_(0.15)Ti catalyst showed superior performances,with a NO conversion of 100%and N_(2)selectivity above 87%at 180–300℃.The characterizations showed that Sm doping suppressed the crystallization of TiO_(2)and Mn2O3phases and increased the specific surface area and *** particular,the surface area increased from 152.2 m^(2)·g^(-1)for Mn0.3Ti to 241.7 m^(2)·g^(-1)for Sm_(0.15)Mn_(0.15)*** effects contributed to the high catalytic *** X-ray photoelectron spectroscopy (XPS) results indicated that the relative atomic ratios of Sm^(3+)/Sm and Oβ/O of Sm_(0.15)Mn_(0.15)Ti were 76.77at%and 44.11at%,*** presence of Sm contributed to an increase in surface-absorbed oxygen (Oβ) and a decrease in Mn^(4+)surface concentration,which improved the catalytic *** the results of hydrogen temperature-programmed reduction(H_(2)-TPR),the presence of Sm induced a higher reduction temperature and lower H_(2)consumption (0.3 mmol·g^(-1)) for the Sm_(0.15)Mn_(0.15)Ti catalyst compared to the Mn0.3Ti *** decrease in Mn^(4+)weakened the redox property of the catalysts and increased the N_(2)selectivity by suppressing N_(2)O formation from NH3oxidation and the nonselective catalytic reduction *** in situ diffuse reflectance infrared Fourier transform spectra (DRIFTs) revealed that NH3-SCR of NO over the Sm_(0.15)Mn_(0.15)Ti catalyst mainly followed the Eley–Rideal *** doping increased surface-absorbed oxygen and weakened the redox property to improve the NO conversion and N_(2)selectivity of the Sm_(0.15)Mn_(0.15)Ti catalyst.

关键词： manganese oxides nitric oxide nitrous oxide samarium selective catalytic reduction nitrogen selectivity

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Pushing working voltage of nickel-rich cathode to 4.6 V by stabilizing lattice oxygen redox via spinel Li_(4)Mn_5O_(12)coating

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Journal of Energy Chemistry 2025年第4期103卷 692-702页

作者： Yunting Wang Gaohui Du Di Han Jiahao Deng Weihao Shi Huayu Li Yongle Wang Siyao Wang Zhan Gao Youqing Wang Shixian Chen Wenqi Zhao Qingmei Su Bingshe Xu Materials Institute of Atomic and Molecular Science Shaanxi University of Science and TechnologyXi’an 710021ShaanxiChina Shanxi-Zheda Institute of Advanced Materials and Chemical Engineering Taiyuan 030024ShanxiChina Key Laboratory of Interface Science and Engineering in Advanced Materials Taiyuan University of TechnologyTaiyuan 030024ShanxiChina

Augmenting the working voltage is an effective way to maximize the energy density of Ni-rich layered Li[Ni_(0.8)Co_(0.1)Mn_(0.1)]O_(2)(NCM)to approach its theoretical ***,NCM suffers from structural degradation in deep delithiation state,which is often accompanied by severe surface lattice oxygen loss and transition metal dissolution,leading to restricted cycle ***,a facile and effective surfacestrengthening strategy is proposed,in which Mn(OH)_(2)nanoshells are uniformly grown on the NCM surface as a Li~+capturer and then converted to thin spinel Li_(4)Mn_(5)O_(12)layers during subsequent hightemperature *** resultant Li_(4)Mn_(5)O_(12)layers can enhance cathode-electrolyte interface electrochemical stability with inhibited electrolyte corrosion and accelerated Li~+*** theoretical calculations confirms that the Mn-O bonds formed at the interfaces can effectively decrease the oxygen activity,thereby further inhibiting the lattice oxygen release and structural degradation caused by the irreversible phase ***,the Li_(4)Mn_(5)O_(12)-coated NCM displays high capacity retention of 80.3%and 94.9%at 1 C and 5 C compared to the pristine NCM(52.5%and 10.1%)after 200 cycles and can operate stably at 2.7-4.6 V and 60℃.The spinel Li_(4)Mn_(5)O_(12)-coating demonstrates an effective route to enhance the structural/electrochemical stability of NCM for next-generation advanced lithium-ion batteries.

关键词： Ni-rich cathode Interfacial stability Li_(4)Mn_5O_(12)coating High voltage stability

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Enhanced strength and ductility in a powder metallurgy Ti material by the oxygen scavenger of CaB_(6)

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Journal of Materials science & technology 2023年第6期137卷 132-142页

作者： Yu Pan Jinshan Zhang Jianzhuo Sun Yanjun Liu Ce Zhang Rui Li Fan Kuang Xinxin Wu Xin Lu Beijing Advanced Innovation Center for Materials Genome Engineering Institute of Engineering TechnologyNational Engineering Research Center for Advanced Rolling TechnologyUniversity of Science and Technology BeijingBeijing 100083China School of Materials Science and Engineering Nanjing Institute of TechnologyNanjing 211167China

The challenge of producing a high-ductility titanium(Ti)material using inexpensive high-oxygen hydride-dehydride(HDH)Ti powder is hereby addressed by the incorporation of CaB_(6)*** oxygen-scavenging behavior,microstructure evolution,mechanical behavior and improvement mechanism were systematically investigated.A continuous TiO_(2)oxide layer with a thickness of approximately 9.3 nm is presented on the HDH Ti powder *** oxide layer will dissolve into Ti matrix during sintering,making the increase of c/a value and leading to the Ti-Ti bonds developing from plastic metal bonds to-ward brittle covalent *** CaB_(6)addition can scavenge O impurity and make a significant increase in tensile ductility forα-Ti matrix.A small addition of 0.2 wt.%CaB_(6)provides a superior tensile elongation of 22.2%for Ti material,almost three times as high as that of pure Ti(7.5%).The increase of defor-mation twining activity and grain refinement are responsible for the improved ***,the CaB_(6)oxygen-scavenger can react with the surface oxide layer to in-situ form rod-like TiB and granular CaTiO_(3)reinforcements,refining the coarse near equiaxed grain ofα-Ti matrix into fine equiaxed *** multiple mechanisms of grain-boundary strengthening,load-bearing strengthening of TiB and Orowan strengthening of CaTiO_(3)nanoparticles work together to increase the tensile strength of Ti/CaB_(6)*** work offers an effective method to fabricate high-performance Ti material using inex-pensive high-oxygen HDH Ti powder.

关键词： Titanium Powder metallurgy Sintering Oxygen Mechanical properties

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